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1. 发明申请

US20070225458A1 Novel Fluorinated Alkyl Fluorophosphoric Acid Salts of Onium and Ttransition Metal Complex 有权
标题翻译：新型氟化烷基氟磷酸盐的鎓和过渡金属络合物
公开(公告)号：US20070225458A1
公开(公告)日：2007-09-27
申请号：US11597616
申请日：2005-05-27
申请人： Hideki Kimura , Jiro Yamamoto , Shinji Yamashita , Mitsuo Kurumaya , Takaaki Sonoda
发明人： Hideki Kimura , Jiro Yamamoto , Shinji Yamashita , Mitsuo Kurumaya , Takaaki Sonoda
IPC分类号： C07F9/02 , C08F4/46
CPC分类号： C08G59/68 , B33Y70/00 , C07C25/18 , C07C381/12 , C07F9/28 , C07F15/025 , C07F17/02 , C08F4/00 , C08G65/18
摘要： To obtain a polymerization initiator (acid generating agent) having excellent power for initiation of cationic polymerization without containing arsenic or antimony. [Means for solution] Provided is a specific onium salt or transition metal complex salt of a fluorinated alkyl fluorophosphoric acid.
摘要翻译：得到不含砷或锑的阳离子聚合引发功能优异的聚合引发剂（酸产生剂）。 [解决方案]提供氟化烷基氟磷酸的特定的鎓盐或过渡金属络合盐。

2. 发明申请

US20100305345A1 PROCESS FOR PRODUCING FLUORINE-CONTAINING COMPOUNDS 失效
标题翻译：生产含氟化合物的方法
公开(公告)号：US20100305345A1
公开(公告)日：2010-12-02
申请号：US12734842
申请日：2008-11-28
申请人： Mitsuo Kurumaya , Tsunetoshi Honda , Kota Omori
发明人： Mitsuo Kurumaya , Tsunetoshi Honda , Kota Omori
IPC分类号： C07C51/60
CPC分类号： C07C51/60 , C07B39/00 , C07C51/62 , C07C67/14 , C07C55/40 , C07C55/36 , C07C53/50 , C07C69/63 , C07C53/42
摘要： This process for producing fluorine-containing compounds includes liquid-phase fluorination by introducing a raw material compound and fluorine gas into a solvent to replace hydrogen atoms in the raw material compound with fluorine atoms. More specifically, the process for producing fluorine-containing compounds includes (1) promoting fluorination by dissolving the raw material compound in anhydrous hydrofluoric acid and introducing into a liquid-phase fluorination solvent, or (2) promoting fluorination by dissolving the raw material compound in a perfluoro compound having a plurality of polar groups in a molecule thereof and introducing into a liquid-phase fluorination solvent. According to these processes, a fluorination reaction can be carried out at high yield and without containing hardly any isomers while using a hydrocarbon compound as is for the raw material.
摘要翻译：该含氟化合物的制造方法包括通过将原料化合物和氟气引入溶剂中来代替原料化合物中的氢原子用氟原子进行液相氟化。更具体地说，制造含氟化合物的方法包括：（1）通过将原料化合物溶解在无水氢氟酸中并引入液相氟化溶剂来促进氟化，或（2）通过将原料化合物溶解于在其分子中具有多个极性基团并引入液相氟化溶剂的全氟化合物。根据这些方法，氟化反应可以以高产率进行，并且在使用原料的烃化合物的同时不含有几乎任何异构体。

3. 发明授权

US08350082B2 Process for producing fluorine-containing compounds 失效
标题翻译：含氟化合物的制造方法
公开(公告)号：US08350082B2
公开(公告)日：2013-01-08
申请号：US12734842
申请日：2008-11-28
申请人： Mitsuo Kurumaya , Tsunetoshi Honda , Kota Omori
发明人： Mitsuo Kurumaya , Tsunetoshi Honda , Kota Omori
IPC分类号： C07C51/58
CPC分类号： C07C51/60 , C07B39/00 , C07C51/62 , C07C67/14 , C07C55/40 , C07C55/36 , C07C53/50 , C07C69/63 , C07C53/42
摘要： This process for producing fluorine-containing compounds includes liquid-phase fluorination by introducing a raw material compound and fluorine gas into a solvent to replace hydrogen atoms in the raw material compound with fluorine atoms. More specifically, the process for producing fluorine-containing compounds includes (1) promoting fluorination by dissolving the raw material compound in anhydrous hydrofluoric acid and introducing into a liquid-phase fluorination solvent, or (2) promoting fluorination by dissolving the raw material compound in a perfluoro compound having a plurality of polar groups in a molecule thereof and introducing into a liquid-phase fluorination solvent. According to these processes, a fluorination reaction can be carried out at high yield and without containing hardly any isomers while using a hydrocarbon compound as is for the raw material.
摘要翻译：该含氟化合物的制造方法包括通过将原料化合物和氟气引入溶剂中来代替原料化合物中的氢原子用氟原子进行液相氟化。更具体地说，制造含氟化合物的方法包括：（1）通过将原料化合物溶解在无水氢氟酸中并引入液相氟化溶剂来促进氟化，或（2）通过将原料化合物溶解于在其分子中具有多个极性基团并引入液相氟化溶剂的全氟化合物。根据这些方法，氟化反应可以以高产率进行，并且在使用原料的烃化合物的同时不含有几乎任何异构体。

4. 发明授权

US07709598B2 Fluorinated alkyl fluorophoshoric acid salts of onium and transition metal complex 有权
标题翻译：鎓和过渡金属络合物的氟化烷基氟磷酸盐
公开(公告)号：US07709598B2
公开(公告)日：2010-05-04
申请号：US11597616
申请日：2005-05-27
申请人： Hideki Kimura , Jiro Yamamoto , Shinji Yamashita , Mitsuo Kurumaya , Takaaki Sonoda
发明人： Hideki Kimura , Jiro Yamamoto , Shinji Yamashita , Mitsuo Kurumaya , Takaaki Sonoda
IPC分类号： C08G59/68
CPC分类号： C08G59/68 , B33Y70/00 , C07C25/18 , C07C381/12 , C07F9/28 , C07F15/025 , C07F17/02 , C08F4/00 , C08G65/18
摘要： To obtain a polymerization initiator (acid generating agent) having excellent power for initiation of cationic polymerization without containing arsenic or antimony.Provided is a specific onium salt or transition metal complex salt of a fluorinated alkyl fluorophosphoric acid.
摘要翻译：得到不含砷或锑的阳离子聚合引发功能优异的聚合引发剂（酸产生剂）。提供氟化烷基氟磷酸的特定鎓盐或过渡金属络合盐。

5. 发明申请

US20120184763A1 METHOD FOR PRODUCING PERFLUOROSULFONIC ACID HAVING ETHER STRUCTURE AND DERIVATIVE THEREOF, AND SURFACTANT CONTAINING FLUORINE-CONTAINING ETHER SULFONIC ACID COMPOUND AND DERIVATIVE THEREOF 审中-公开
标题翻译：生产具有其结构和衍生物的全氟代酸的方法，以及含有含氟的含硫磺酸化合物及其衍生物的表面活性剂
公开(公告)号：US20120184763A1
公开(公告)日：2012-07-19
申请号：US13498710
申请日：2010-09-29
申请人： Mitsuo Kurumaya , Tsunetoshi Honda , Kota Omori
发明人： Mitsuo Kurumaya , Tsunetoshi Honda , Kota Omori
IPC分类号： C07C303/28 , C07C303/02 , C25B3/08 , C07C309/68 , C07C309/10 , C07C303/22 , C07C309/82
CPC分类号： C07C303/22 , C07C303/02 , C07C303/28 , C07C303/32 , C07C303/44 , C25B3/08 , C07C309/82 , C07C309/10 , C07C309/68
摘要： In this method, RH2ORH1SO2F is added to hydrofluoric acid so as to form a thick solution (hydrogen bonded complex), and the solution is directly supplied to a liquid phase reaction system in which an F2 gas is used. Alternatively, RH2ORH1SO2Cl is added to hydrofluoric acid so as to be converted into RH1ORH2SO2F by discharging HCl, and the RH1ORH2SO2F is directly supplied to a liquid phase reaction system in which an F2 gas is used. Consequently, fluorination can be carried out safely and a compound having an objective structure can be produced at low cost without causing isomerization or the like.
摘要翻译：在该方法中，将RH2ORH1SO2F加入到氢氟酸中以形成稠溶液（氢键合复合物），并将溶液直接供给到使用F2气体的液相反应体系中。或者，将RH2ORH1SO2Cl加入氢氟酸中，通过排出HCl转化为RH1ORH2SO2F，将RH1ORH2SO2F直接供给到使用F2气体的液相反应体系中。因此，可以安全地进行氟化，可以以低成本制造具有目标结构的化合物，而不会引起异构化等。

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