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1. 发明申请

US20070280869A1 Methods for reversibly storing hydrogen 失效
标题翻译：氢可逆储存方法
公开(公告)号：US20070280869A1
公开(公告)日：2007-12-06
申请号：US11758114
申请日：2007-06-05
申请人： John Vajo , Florian Mertens , Sky Skeith , Michael Balogh , Frederick Pinkerton , Martin Meyer
发明人： John Vajo , Florian Mertens , Sky Skeith , Michael Balogh , Frederick Pinkerton , Martin Meyer
IPC分类号： C01B6/13 , C01B6/10
CPC分类号： C01B3/0078 , C01B3/0026 , C01B3/0031 , C01B3/065 , Y02E60/327 , Y02E60/362
摘要： The invention provides a method of reversibly storing hydrogen at industrially practicable temperature and pressure conditions. A stable hydrogen storage hydride is mixed with a destabilizing hydride. The stable hydride is capable of releasing hydrogen at a first energy level. When the stable hydride is in the presence of the destabilizing hydride, the stable hydride releases hydrogen at a second energy level. The second energy level is significantly reduced from the first energy level.
摘要翻译：本发明提供了一种在工业上可行的温度和压力条件下可逆地储存氢的方法。将稳定的储氢氢化物与不稳定的氢化物混合。稳定的氢化物能够在第一能级释放氢。当稳定的氢化物存在不稳定的氢化物时，稳定的氢化物在第二能级释放氢。第二个能源水平从第一个能源水平显着降低。

2. 发明授权

US3192138A Process for the production of hydrides and/or halogenated hydrides of the elements boron and silicon 失效
标题翻译：用于生产元素硼和硅的氢化物和/或卤代氢化物的方法
公开(公告)号：US3192138A
公开(公告)日：1965-06-29
申请号：US4087160
申请日：1960-07-05
申请人： WACKER CHEMIE GMBH
发明人： EDUARD ENK , JULIUS NICKL
IPC分类号： C01B6/10 , C01B6/11 , C01B6/13 , C01B33/04 , C01B35/02 , C01B35/06
CPC分类号： C01B33/04 , C01B6/00 , C01B6/10 , C01B6/11 , C01B6/13 , C01B33/107 , C01B35/02 , C01B35/026 , C01B35/06

3. 发明授权

US3094562A Process for the preparation of amine-borane complexes 失效
标题翻译：胺 - 硼烷络合物的制备方法
公开(公告)号：US3094562A
公开(公告)日：1963-06-18
申请号：US80407759
申请日：1959-04-06
申请人： ETHYL CORP
发明人： ASHBY EUGENE C
IPC分类号： C01B6/10 , C01B6/13 , C07F5/00 , C10L1/30
CPC分类号： C01B6/13 , C01B6/10 , C07F5/006 , C10L1/303

4. 发明申请

US20100160149A1 METHOD OF ACTIVATING OR REGENERATING A HYDROGEN STORAGE MATERIAL 有权
标题翻译：激活或再生氢储存材料的方法
公开(公告)号：US20100160149A1
公开(公告)日：2010-06-24
申请号：US12635315
申请日：2009-12-10
申请人： GAGIK BARKHORDARIAN , Claudio Pistidda , Martin Dornheim , Rüdiger Bormann
发明人： GAGIK BARKHORDARIAN , Claudio Pistidda , Martin Dornheim , Rüdiger Bormann
IPC分类号： B01J20/34 , C01B6/24 , C01B6/04 , C01B6/13
CPC分类号： C01B6/00 , C01B6/04 , C01B6/24 , C01B6/243 , Y02E60/324 , Y02E60/327
摘要： The present invention concerns a method of activating or regenerating a hydrogen storage material which contains at least one metal hydride. The at least one metal hydride is brought into contact with an inert solvent and the inert solvent is subsequently removed again. After contacting with and removal of the inert solvent, there is not only an increase in the reaction rate but surprisingly the hydrogenation also proceeds more completely.The present method is particularly advantageous when the hydrogen storage material contains at least components which interact with one another during absorption and desorption.
摘要翻译：本发明涉及活化或再生含有至少一种金属氢化物的储氢材料的方法。使至少一种金属氢化物与惰性溶剂接触，随后再次除去惰性溶剂。在与惰性溶剂接触并除去之后，反应速率不仅有所增加，而且令人惊奇的是氢化也更完全地进行。当吸收和解吸时，储氢材料至少含有彼此相互作用的组分时，本方法是特别有利的。

5. 发明授权

US07678356B2 Process for the preparation of crystalline magnesium borohydride 失效
标题翻译：制备结晶硼氢化镁的方法
公开(公告)号：US07678356B2
公开(公告)日：2010-03-16
申请号：US11807524
申请日：2007-05-29
申请人： Pierino Zanella , Laura Crociani , Giovanni Giunchi
发明人： Pierino Zanella , Laura Crociani , Giovanni Giunchi
IPC分类号： C01B6/13 , C01B6/10 , C01B3/00
CPC分类号： C01B3/065 , C01B6/04 , C01B6/21 , Y02E60/324 , Y02E60/362
摘要： A process is described for the preparation of magnesium borohydride having a high purity and crystallinity, which comprises the reaction of an orgenometallic compound of magnesium of the type MgX2, wherein X is an organic binder selected from alkyl, amide, alkoxide, cyclopentadienyl, aryl, with a derivative of a boron hydride, in a hydrocarbon solvent.
摘要翻译：描述了一种制备具有高纯度和结晶度的硼氢化镁的方法，其包括MgX 2型镁的金属间化合物的反应，其中X是选自烷基，酰胺，醇盐，环戊二烯基，芳基，与硼氢化物的衍生物在烃溶剂中反应。

6. 发明授权

US07608233B1 Direct synthesis of calcium borohydride 有权
标题翻译：直接合成硼氢化钙
公开(公告)号：US07608233B1
公开(公告)日：2009-10-27
申请号：US11807012
申请日：2007-05-24
申请人： Ewa Carin Ellinor Rönnebro , Eric H. Majzoub
发明人： Ewa Carin Ellinor Rönnebro , Eric H. Majzoub
IPC分类号： C01B6/13 , C01B6/24 , C01B6/00 , C01B6/04 , C01B3/02 , C01B3/08
CPC分类号： C01B6/21 , C01B3/0026 , C01B3/065 , Y02E60/327 , Y02E60/362
摘要： A method is disclosed for directly preparing an alkaline earth metal borohydride, i.e. Ca(BH4)2, from the alkaline earth metal hydride and the alkaline earth metal boride. The borohydride thus prepared is doped with a small portion of a metal chloride catalyst compound, such as RuCl3, TiCl3, or a mixture of TiCl3 and palladium metal. The process provides for mechanically mixing the dry reagents under an inert atmosphere followed by charging the mixed materials with high pressure hydrogen at about 70 MPa while heating the mixture to about 400° C. The method is relatively simple and inexpensive and provides reversible hydride compounds which are free of the usual contamination introduced by prior art wet chemical methods.
摘要翻译：公开了从碱土金属氢化物和碱土金属硼化物直接制备碱土金属硼氢化物即Ca（BH 4）2的方法。由此制备的硼氢化钠掺入少量的金属氯化物催化剂化合物，例如RuCl 3，TiCl 3或TiCl 3和钯金属的混合物。该方法提供了在惰性气氛下机械混合干试剂，然后在约70MPa的高压氢气下将混合物料加热，同时将混合物加热至约400℃。该方法相对简单且便宜，并提供可逆氢化物化合物，其中没有通过现有技术的湿化学方法引入的通常污染物。

7. 发明授权

US4152401A Chelated lithium aluminum compounds 失效
公开(公告)号：US4152401A
公开(公告)日：1979-05-01
申请号：US877354
申请日：1978-02-13
申请人： Arthur W. Langer, Jr. , Thomas A. Whitney
发明人： Arthur W. Langer, Jr. , Thomas A. Whitney
IPC分类号： C01B6/13 , C07F1/00 , C07F5/00 , C07F9/02 , C07F9/50 , C10L1/30 , C10M159/18
CPC分类号： C07F9/02 , C07F1/005 , C07F5/00 , C07F9/50 , C10L1/301 , C10M159/18 , C10M3/00 , C10M2207/125 , C10M2207/129 , C10M2215/04 , C10M2215/042 , C10M2215/044 , C10M2215/062 , C10M2215/064 , C10M2215/066 , C10M2215/14 , C10M2215/22 , C10M2215/221 , C10M2215/222 , C10M2215/225 , C10M2215/226 , C10M2215/26 , C10M2215/30 , C10M2217/046 , C10M2217/06 , C10M2219/04 , C10M2219/082 , C10M2219/087 , C10M2219/088 , C10M2219/089 , C10M2223/02 , C10M2223/049 , C10M2223/06 , C10M2223/061 , C10M2227/09 , C10N2210/01 , C10N2210/02 , C10N2210/03
摘要： Chelated lithium aluminum compounds are prepared by mixing a lithium aluminum compound such as a lithium aluminum hydride with a chelating agent wherein the agent contains at least one nitrogen atom. The chelating agent is a tertiary polyamine or aminoether. The resultant chelate is used for a variety of processes such as separations, catalytic reactions, substitution reactions, reductions, electrochemical reactions, and also as an oil and fuel additive.

8. 发明申请

US20060194695A1 Destabilized and catalyzed borohydrided for reversible hydrogen storage 审中-公开
标题翻译：不稳定和催化硼氢化用于可逆氢存储
公开(公告)号：US20060194695A1
公开(公告)日：2006-08-31
申请号：US11343048
申请日：2006-01-30
申请人： Ming Au
发明人： Ming Au
IPC分类号： C01B6/13
CPC分类号： B01J20/04 , B01J20/0211 , B01J20/0248 , B01J20/046 , B01J20/28007 , B01J20/3021 , B01J20/3078 , B01J21/063 , B01J21/066 , C01B3/0078 , C01B6/21 , Y02E60/324
摘要： A hydrogen storage material and process is provided in which catalyzed alkali borohydride materials and partially substituted borohydride materials are created and which may contain effective amounts of catalyst(s) which include transition metal oxides, halides, and chlorides of titanium, zirconium, tin, vanadium, iron, cobalt and combinations of the various catalysts and the destabilization agents which include metals, metal hydrides, metal chlorides and complex hydrides of magnesium, calcium, strontium, barium, aluminum, gallium, indium, thallium and combinations of the various destabilization agents. When the catalysts and destabilization agents are added to an alkali borodydride such as a lithium borohydride, the initial hydrogen release point of the resulting mixture is substantially lowered. Additionally, the hydrogen storage material may be rehydrided with weight percent values of hydrogen of at least about nine percent.
摘要翻译：提供了一种储氢材料和方法，其中产生了催化的碱金属硼氢化物材料和部分取代的硼氢化物材料，并且可以含有有效量的催化剂，其包括钛，锆，锡，钒的过渡金属氧化物，卤化物和氯化物，铁，钴以及各种催化剂和不稳定剂的组合，其包括镁，钙，锶，钡，铝，镓，铟，铊的金属，金属氢化物，金属氯化物和络合氢化物以及各种不稳定剂的组合。当将催化剂和去稳定剂加入硼氢化锂等碱金属硼化物中时，所得混合物的初始氢释放点显着降低。另外，储氢材料可以用至少约9％的重量百分比的氢气重新水解。

9. 发明申请

US20050226801A1 Process for production of a borohydride compound 失效
标题翻译：硼氢化合物的制备方法
公开(公告)号：US20050226801A1
公开(公告)日：2005-10-13
申请号：US11098734
申请日：2005-04-04
申请人： Arthur Chin
发明人： Arthur Chin
IPC分类号： C01B6/23 , B41J2/175 , C01B6/13 , C01B6/17 , C01B6/19 , C01B6/21 , H01M8/06
CPC分类号： C01B6/17 , C01B6/21 , C01B6/23
摘要： A process for production of a borohydride compound. The process comprises the steps of: (a) combining a boron-containing salt, at least one of a metal and its hydride; wherein the metal is Be, Mg, Ca, Sr, Ba, Al, Ga, Si or a transition metal; and a solvent in which the borohydride compound is soluble; (b) grinding a mixture formed in step (a) to form the borohydride compound; and (c) separating a solution comprising the borohydride compound.
摘要翻译：硼氢化合物的制造方法。该方法包括以下步骤：（a）将含硼盐，金属和其氢化物中的至少一种合并; 其中所述金属为Be，Mg，Ca，Sr，Ba，Al，Ga，Si或过渡金属; 和硼氢化合物可溶的溶剂; （b）研磨步骤（a）中形成的混合物以形成硼氢化合物; 和（c）分离包含硼氢化合物的溶液。

10. 发明授权

US4376782A Complexes of square planar platinum II compounds and N-methyl glucamine 失效
标题翻译：方形平面铂II化合物和N-甲基葡糖胺的复合物
公开(公告)号：US4376782A
公开(公告)日：1983-03-15
申请号：US151976
申请日：1980-05-21
申请人： John Turkevich , Joseph H. Burchenal
发明人： John Turkevich , Joseph H. Burchenal
IPC分类号： C07F15/00 , C01B6/13 , C01B6/22
CPC分类号： C07F15/0093 , Y10S514/908
摘要： Complexes or salts of square planar platinum(II) compounds and N-methyl glucamine, prepared by reacting a platinum(II) compound with N-methyl glucamine in an aqueous medium, are effective anti-tumor agents.
摘要翻译：通过在水性介质中使铂（II）化合物与N-甲基葡糖胺反应制备的正方形平面铂（II）化合物和N-甲基葡糖胺的配合物或盐是有效的抗肿瘤剂。

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