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1. 发明授权

US08883109B2 High capacity stabilized complex hydrides for hydrogen storage 有权
标题翻译：用于氢存储的高容量稳定复合氢化物
公开(公告)号：US08883109B2
公开(公告)日：2014-11-11
申请号：US13382751
申请日：2010-07-09
申请人： Ragaiy Zidan , Rana F. Mohtadi , Christopher Fewox , Premkumar Sivasubramanian
发明人： Ragaiy Zidan , Rana F. Mohtadi , Christopher Fewox , Premkumar Sivasubramanian
IPC分类号： C01B6/23 , C01B6/13 , C01B6/34
CPC分类号： C01B6/34 , C01B6/23 , Y02E60/327 , Y02E60/328 , Y02E60/364 , Y10S420/90
摘要： Complex hydrides based on Al(BH4)3 are stabilized by the presence of one or more additional metal elements or organic adducts to provide high capacity hydrogen storage material.
摘要翻译：基于Al（BH4）3的复合氢化物通过一种或多种另外的金属元素或有机加合物的存在来稳定，以提供高容量的储氢材料。

2. 发明授权

US08465715B1 Method for synthesizing metal bis(borano) hypophosphite complexes 有权
标题翻译：金属双（硼）次磷酸盐配合物的合成方法
公开(公告)号：US08465715B1
公开(公告)日：2013-06-18
申请号：US12829592
申请日：2010-07-02
申请人： Joseph G. Cordaro
发明人： Joseph G. Cordaro
IPC分类号： C01B6/21 , C01B6/00 , C01B35/026
CPC分类号： C01B3/001 , C01B3/04 , C01B6/00 , C01B6/21 , C01B6/23 , C01D13/00 , C01D15/00 , Y02E60/324 , Y02E60/364
摘要： The present invention describes the synthesis of a family of metal bis(borano) hypophosphite complexes. One procedure described in detail is the syntheses of complexes beginning from phosphorus trichloride and sodium borohydride. Temperature, solvent, concentration, and atmosphere are all critical to ensure product formation. In the case of sodium bis(borano) hypophosphite, hydrogen gas was evolved upon heating at temperatures above 150° C. Included in this family of materials are the salts of the alkali metals Li, Na and K, and those of the alkaline earth metals Mg and Ca. Hydrogen storage materials are possible. In particular the lithium salt, Li[PH2(BH3)2], theoretically would contain nearly 12 wt % hydrogen. Analytical data for product characterization and thermal properties are given.
摘要翻译：本发明描述了一族金属双（硼）次磷酸盐络合物的合成。详细描述的一个程序是从三氯化磷和硼氢化钠开始的络合物的合成。温度，溶剂，浓度和气氛对于确保产品形成至关重要。在二（硼）次亚磷酸钠的情况下，在高于150℃的温度下加热时放出氢气。该材料族包括碱金属Li，Na和K以及碱土金属的盐镁和钙储氢材料是可能的。特别是锂盐Li [PH2（BH3）2]在理论上将含有近12wt％的氢。给出了产品表征和热性能的分析数据。

3. 发明申请

US20100329974A1 HYDROGEN STORAGE MATERIAL AND A PROCESS FOR RELEASE OF HYDROGEN 审中-公开
标题翻译：氢储存材料和氢释放过程
公开(公告)号：US20100329974A1
公开(公告)日：2010-12-30
申请号：US12746386
申请日：2008-12-05
申请人： Ping Chen , Zhitao Xiong , Guotao Wu
发明人： Ping Chen , Zhitao Xiong , Guotao Wu
IPC分类号： C01B3/02 , B01J20/22 , B01J20/26
CPC分类号： C01B6/21 , C01B3/0026 , C01B3/0078 , C01B3/06 , C01B6/23 , C01B6/246 , Y02E60/327 , Y02E60/364
摘要： There is disclosed a hydrogen storage material which may comprise an optionally substituted M-amino-borane complex or a composite comprising: (i) at least one of a M-nitrogen compound; and (ii) a compound comprising (Y—Z)—R bonds. M is a metal or metalloid; Y is an element selected from Group 13 of the Periodic Table of Elements; Z is an element selected from Group 15 of the Periodic Table of Elements; and R is hydrogen (H) or a hydrocarbyl.
摘要翻译：公开了一种储氢材料，其可以包含任选取代的M-氨基 - 硼烷络合物或复合物，其包含：（i）至少一种M-氮化合物; 和（ii）包含（Y-Z）-R键的化合物。 M是金属或准金属; Y是选自元素周期表第13族的元素; Z是选自元素周期表第15族的元素; 和R是氢（H）或烃基。

4. 发明授权

US06586563B1 Processes for synthesizing alkali metal borohydride compounds 失效
标题翻译：碱金属硼氢化合物合成方法
公开(公告)号：US06586563B1
公开(公告)日：2003-07-01
申请号：US10022077
申请日：2001-12-18
申请人： Jeffrey V. Ortega , Ying Wu , Steven C. Amendola , Michael T. Kelly
发明人： Jeffrey V. Ortega , Ying Wu , Steven C. Amendola , Michael T. Kelly
IPC分类号： C08G7908
CPC分类号： C01B6/23 , C01B6/21
摘要： Processes for synthesizing borohydride compounds with reduced energy requirements and high efficiency are disclosed. The processes include the reaction of a base with a borane complex or diborane to produce a borohydride compound of formula YBH4, where Y is a monovalent cationic moiety.
摘要翻译：公开了具有降低的能量需求和高效率合成硼氢化合物的方法。该方法包括碱与硼烷络合物或乙硼烷的反应，生成式YBH4的硼氢化合物，其中Y是一价阳离子部分。

5. 发明授权

US09947947B2 Mixed metal borohydrides 有权
公开(公告)号：US09947947B2
公开(公告)日：2018-04-17
申请号：US14629317
申请日：2015-02-23
申请人： Intelligent Energy Inc.
发明人： Allison M. Fisher , Brian Elliot Hayden , Jean-Philipe Soulie
IPC分类号： C01B3/00 , H01M8/04082 , C01B35/00 , C01B6/23
CPC分类号： H01M8/04216 , C01B6/23 , C01B35/00
摘要： The invention relates to mixed metal borohydrides used for solid hydrogen storage. The mixed metal borohydrides are synthesized through solution synthesis using multiple metal borohydrides. First and second precursor solutions are prepared and combined to create a mixture in which the mixed metal borohydride is formed. The solvent is removed, leaving the mixed metal borohydride. The first precursor solution consisting essentially of lithium borohydride, and the second precursor solution consisting essentially of a borohydride compound containing one or more metal cations selected from the group of metals consisting of sodium, magnesium, calcium and titanium.

6. 发明申请

US20160280542A1 MULTI-ELEMENT ANIONIC REAGENT COMPLEXES 有权
标题翻译：多元素阴离子试剂复合物
公开(公告)号：US20160280542A1
公开(公告)日：2016-09-29
申请号：US15176313
申请日：2016-06-08
申请人： Toyota Motor Engineering & Manufacturing North America, Inc. , The University of Manitoba
发明人： Michael Paul Rowe , Elizabeth Marie Skoropata , Johan Alexander van Lierop
IPC分类号： C01B6/23 , C01B19/04
CPC分类号： C01B6/23 , C01B6/21 , C01B19/04 , H01F1/0311 , H01F3/00
摘要： Reagent complexes have two or more elements, formally in oxidation state zero, complexed with a hydride molecule. Complexation with the hydride molecule may be evidenced by shifts to lower binding energies, of one or more electrons in each of the two or more elements, as observed by x-ray photoelectron spectroscopy. The reagents can be useful for the synthesis of multi-element nanoparticles. Preparation of the reagents can be achieved by ball-milling a mixture that includes powders of two or more elements and a hydride molecule.
摘要翻译：试剂络合物具有两种或更多种正式氧化态为零的元素，与氢化物分子络合。与氢化物分子的络合可以通过X射线光电子能谱法观察到的两个或更多个元素中的一个或多个电子中的一个或多个电子的转移降低结合能来证明。这些试剂可用于合成多元素纳米颗粒。试剂的制备可以通过球磨研磨包含两种或更多种元素的粉末和氢化物分子的混合物来实现。

7. 发明申请

US20150259200A1 METHOD OF USE OF AN IONIC LIQUID FOR STORING HYDROGEN 有权
标题翻译：使用离子液体储存氢气的方法
公开(公告)号：US20150259200A1
公开(公告)日：2015-09-17
申请号：US14726248
申请日：2015-05-29
申请人： VTU Holding GmbH
发明人： Roland Kalb
IPC分类号： C01B3/08 , B01J41/08 , H01M8/06
CPC分类号： C01B3/08 , B01J41/09 , C01B3/001 , C01B3/065 , C01B6/23 , C07C211/63 , C07F9/5407 , H01M8/0606 , Y02E60/324 , Y02E60/327 , Y02E60/362
摘要： A method releases hydrogen by forming a second ionic liquid from a first ionic liquid by releasing hydrogen from the first ionic liquid by exposing the second ionic liquid to water and a catalyst. The first ionic liquid includes a cation and an anion including a borohydride. The release of the hydrogen forms a borate, which makes up the anion of the second ionic liquid. The cation of the first ionic liquid is the same as that of the second ionic liquid. A reaction system includes the first and second ionic liquids, water and a catalyst.
摘要翻译：一种方法是通过从第一离子液体形成第二离子液体来释放氢气，通过将第二离子液体暴露于水和催化剂中，从第一离子液体释放氢。第一离子液体包括阳离子和包含硼氢化物的阴离子。氢的释放形成硼酸盐，其构成第二离子液体的阴离子。第一离子液体的阳离子与第二离子液体的阳离子相同。反应体系包括第一和第二离子液体，水和催化剂。

8. 发明申请

US20150166336A1 MIXED METAL BOROHYDRIDES 审中-公开
标题翻译：混合金属硼氢化物
公开(公告)号：US20150166336A1
公开(公告)日：2015-06-18
申请号：US14629317
申请日：2015-02-23
申请人： INTELLIGENT ENERGY INC.
发明人： Allison M. Fisher , Brian Elliot Hayden , Jean-Philipe Soulie
IPC分类号： C01B3/00 , H01M8/04 , C01B35/00
CPC分类号： H01M8/04216 , C01B6/23 , C01B35/00
摘要： The invention relates to mixed metal borohydrides used for solid hydrogen storage. The mixed metal borohydrides are synthesized through solution synthesis using multiple metal borohydrides. First and second precursor solutions are prepared and combined to create a mixture in which the mixed metal borohydride is formed. The solvent is removed, leaving the mixed metal borohydride. The first precursor solution consisting essentially of lithium borohydride, and the second precursor solution consisting essentially of a borohydride compound containing one or more metal cations selected from the group of metals consisting of sodium, magnesium, calcium and titanium.
摘要翻译：本发明涉及用于固体储氢的混合金属硼氢化物。通过使用多种金属硼氢化物的溶液合成来合成混合金属硼氢化物。制备和组合第一和第二前体溶液以产生其中形成混合金属硼氢化物的混合物。除去溶剂，留下混合金属硼氢化物。基本上由硼氢化锂组成的第一前体溶液和基本上由含有一种或多种选自钠，镁，钙和钛的金属组成的金属阳离子的硼氢化合物组成的第二前体溶液。

9. 发明授权

US09051182B2 Method of use of an ionic liquid for storing hydrogen 有权
标题翻译：使用离子液体储存氢气的方法
公开(公告)号：US09051182B2
公开(公告)日：2015-06-09
申请号：US13144912
申请日：2010-01-08
申请人： Roland Kalb
发明人： Roland Kalb
IPC分类号： C01B6/23 , C01B3/06 , C01B3/00 , C07C211/63 , C07F9/54
CPC分类号： C01B3/08 , B01J41/09 , C01B3/001 , C01B3/065 , C01B6/23 , C07C211/63 , C07F9/5407 , H01M8/0606 , Y02E60/324 , Y02E60/327 , Y02E60/362
摘要： A method of storing hydrogen is provided, wherein the method comprises forming a first ionic liquid by inducing a borohydride into a second ionic liquid comprising cations and an anion comprising borate, in particular metaborate, and forming the second ionic liquid by releasing the hydrogen out of the first ionic liquid by using water and/or a catalyst.
摘要翻译：提供一种储存氢气的方法，其中所述方法包括通过将硼氢化物诱导到包含阳离子和包含硼酸盐，特别是偏硼酸盐的阴离子的第二离子液体中来形成第一离子液体，并通过将氢气从通过使用水和/或催化剂的第一离子液体。

10. 发明申请

US20120027669A1 METHOD OF USE OF AN IONIC LIQUID FOR STORING HYDROGEN 有权
标题翻译：使用离子液体储存氢气的方法
公开(公告)号：US20120027669A1
公开(公告)日：2012-02-02
申请号：US13144912
申请日：2010-01-08
申请人： Roland Kalb
发明人： Roland Kalb
IPC分类号： C01B3/02 , C09K3/00
CPC分类号： C01B3/08 , B01J41/09 , C01B3/001 , C01B3/065 , C01B6/23 , C07C211/63 , C07F9/5407 , H01M8/0606 , Y02E60/324 , Y02E60/327 , Y02E60/362
摘要： A method of storing hydrogen is provided, wherein the method comprises forming a first ionic liquid by inducing a borohydride into a second ionic liquid comprising cations and an anion comprising borate, in particular metaborate, and forming the second ionic liquid by releasing the hydrogen out of the first ionic liquid by using water and/or a catalyst.
摘要翻译：提供一种储存氢气的方法，其中所述方法包括通过将硼氢化物诱导到包含阳离子和包含硼酸盐，特别是偏硼酸盐的阴离子的第二离子液体中来形成第一离子液体，并通过将氢气从通过使用水和/或催化剂的第一离子液体。

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