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1. 发明申请

US20190185391A1 Graphene/Metal or Metalloid Core-Shell Composite and Manufacturing Method Thereof 审中-公开
公开(公告)号：US20190185391A1
公开(公告)日：2019-06-20
申请号：US15777371
申请日：2016-06-15
申请人： HUBEI INSTITUTE OF AEROSPACE CHEMOTECHNOLOGY
发明人： Jian Gu , Xiaoping Zhang , Aimin Pang
IPC分类号： C06B45/20 , B22F9/24 , B22F1/02 , C06B21/00
CPC分类号： C06B45/20 , B22F1/02 , B22F1/025 , B22F9/24 , C01B6/04 , C01B6/06 , C01G3/02 , C01G21/06 , C01G49/06 , C06B21/00 , C06B21/0008 , C06B21/0033 , C06B21/0083
摘要： The present invention relates to a manufactured graphene/metal or metalloid core-shell composite and manufacturing method thereof. The method comprising: using a modified graphene oxide as a base, then performing concentration and steam drying followed by organic solvent replacement to obtain a modified graphene oxide organic solvent; using a liquid-phase self-assembly method to coat the modified graphene oxide onto a surface of the metal or metalloid to form a graphene/metal or metalloid coated particle solution, then filtering and drying to obtain the graphene metal/metalloid core-shell composite. The method improves upon a conventional organic and inorganic material coating technique, and reduces an impact of a water-based solvent and high temperature on a highly reactive metal and metalloid, thereby expanding the feasibility of the coating technique and addressing a barrier of applicability of graphene and reactive metal or metalloid in the field of energetic materials.

2. 发明申请

US20110236300A1 PROCESS FOR PRODUCTION OF A METAL HYDRIDE 有权
标题翻译：生产金属氢化物的方法
公开(公告)号：US20110236300A1
公开(公告)日：2011-09-29
申请号：US13053350
申请日：2011-03-22
申请人： Nathan Tait Allen , Robert Butterick, III , Arthur Achhing Chin , Dean Michael Millar , David Craig Molzahn
发明人： Nathan Tait Allen , Robert Butterick, III , Arthur Achhing Chin , Dean Michael Millar , David Craig Molzahn
IPC分类号： C01B6/04
CPC分类号： C01B6/04
摘要： A process for production of a metal hydride compound MHx, wherein x is one or two and M is an alkali metal, Be or Mg. The process comprises combining a compound of formula (R1O)xM with aluminum, hydrogen and at least one metal selected from among titanium, zirconium, hafnium, niobium, vanadium, tantalum and iron to produce a compound of formula MHx. R1 is phenyl or phenyl substituted by at least one alkyl or alkoxy group. A mole ratio of aluminum to (R1O)xM is from 0.1:1 to 1:1. The catalyst is present at a level of at least 200 ppm based on weight of aluminum.
摘要翻译：一种制备金属氢化物化合物MHx的方法，其中x为一个或两个，M为碱金属Be或Mg。该方法包括将式（R1O）xM化合物与铝，氢和至少一种选自钛，锆，铪，铌，钒，钽和铁的金属组合以制备式MHx的化合物。 R 1是被至少一个烷基或烷氧基取代的苯基或苯基。铝与（R1O）xM的摩尔比为0.1:1至1:1。以铝的重量计，催化剂的含量至少为200ppm。

3. 发明授权

US08012453B2 Carbon sequestration and production of hydrogen and hydride 有权
标题翻译：碳封存和氢气和氢化物的生产
公开(公告)号：US08012453B2
公开(公告)日：2011-09-06
申请号：US12258886
申请日：2008-10-27
申请人： Surendra Saxena
发明人： Surendra Saxena
IPC分类号： C01D5/00 , C01B3/02
CPC分类号： C01D7/07 , C01B3/02 , C01B3/065 , C01B3/50 , C01B6/04 , C01B2203/0465 , C01B2203/0475 , C01B2203/86 , Y02E60/362 , Y02P20/134 , Y02P30/30
摘要： This invention describes a complete sequestration of carbon (CO2 and CO) from coal burning plants. In this process, hydrogen can be generated which in turn permits the reduction in the cost of hydride synthesis. The hydrides store hydrogen for on-board application for automobiles and fuel cells. Hydrogen generation and synthesis of hydrides is accomplished by using an integrated approach in which coal is used as a fuel and carbon is sequestered in the process. The CO and or CO2 produced in coal burning power plants and the heat is used when available for producing hydrogen and hydrides. Carbon is used both as a reactant and as a fuel. Economically hydrogen production cost is comparable to or less than the current price of hydrogen produced from fossil-fuel with the added benefit of carbon sequestration and reducing global warming. Specific processes for synthesizing important hydrogen storage materials, hydrides are described. A hydrogen based automobile becomes viable as the cost of the hydrogen production and hydride synthesis is reduced. Although coal-burning power plant is specified here, any power plant, coal- or natural gas-burning, can be subjected to similar treatment.
摘要翻译：本发明描述了来自燃煤设备的碳（CO 2和CO）的完全封存。在这个过程中，可以产生氢气，这又可以降低氢化物合成的成本。氢化物储存氢气用于车载和燃料电池的车载应用。氢化物的氢生成和合成通过使用其中使用煤作为燃料并且碳在该过程中螯合的综合方法来实现。在燃煤发电厂生产的CO和/或CO2可用于生产氢和氢化物。碳既用作反应物又用作燃料。经济上的氢气生产成本与化石燃料产生的氢气现在的价格相当甚至更低，另外还有碳封存的好处，并减少全球变暖。描述了合成重要储氢材料，氢化物的具体方法。随着氢气生产和氢化物合成的成本降低，氢基汽车变得可行。虽然这里规定了燃煤发电厂，但任何电厂，煤或天然气燃烧都可以进行类似的处理。

4. 发明授权

US07892521B2 Synthesis and use of metal hydrides for vehicular and other applications 有权
标题翻译：用于车辆和其他应用的金属氢化物的合成和使用
公开(公告)号：US07892521B2
公开(公告)日：2011-02-22
申请号：US11773286
申请日：2007-07-03
申请人： Surendra Saxena
发明人： Surendra Saxena
IPC分类号： C01B6/00 , C01B6/04 , C01B6/24 , C01B3/00 , C01B3/02 , C01B3/06 , C01B3/08 , C01B3/10
CPC分类号： B01J7/02 , C01B3/065 , C01B6/04 , Y02E60/362
摘要： The invention provides for the synthesis of a hydride directly from metal and water or metal and hydroxide or metal and aqueous hydrogen chloride. The hydride generated may be used as metal hydride slurry for on-board generation of hydrogen by reaction with water or with aqueous HCl.
摘要翻译：本发明提供直接从金属和水或金属和氢氧化物或金属和氯化氢水溶液合成氢化物。产生的氢化物可以用作金属氢化物浆液，用于通过与水或HCl水溶液反应来生成氢。

5. 发明申请

US20100323253A1 Systems and Methods for Hydrogen Storage and Generation from Water Using Lithium Based Materials 审中-公开
标题翻译：使用锂基材料从水中储氢和生成的系统和方法
公开(公告)号：US20100323253A1
公开(公告)日：2010-12-23
申请号：US12280232
申请日：2007-02-22
申请人： Zhigang Zak Fang , Jun Lu , Hong Yong Sohn
发明人： Zhigang Zak Fang , Jun Lu , Hong Yong Sohn
IPC分类号： H01M8/06 , C01B6/04 , C01B3/04
CPC分类号： C01B3/065 , C01B3/0026 , C01B6/04 , C01D15/02 , C01F5/04 , C22B5/04 , C22B26/12 , Y02E60/327 , Y02E60/362
摘要： A process for forming lithium hydride for use in storing and producing hydrogen is presented. The process includes reacting lithium oxide with water to form a regenerated lithium hydroxide and reacting the regenerated lithium hydroxide with magnesium to form magnesium oxide and a regenerated lithium hydride. The magnesium oxide can be regenerated to form magnesium. The process can further include reacting lithium hydride to form hydrogen and lithium oxide. Such hydrogen production can include reaction between lithium hydride and lithium hydroxide, and/or reaction between lithium hydride and water.
摘要翻译：提出了一种形成用于储存和生产氢的氢化锂的方法。该方法包括使氧化锂与水反应以形成再生的氢氧化锂，并使再生的氢氧化锂与镁反应形成氧化镁和再生的氢化锂。氧化镁可再生以形成镁。该方法还可以包括使氢化锂反应形成氢和氧化锂。这种氢气生成可以包括氢化锂和氢氧化锂之间的反应，和/或氢化锂与水之间的反应。

6. 发明申请

US20100239495A1 Hydride composite and preparation process of hydrogen gas 审中-公开
标题翻译：氢化物复合和氢气制备工艺
公开(公告)号：US20100239495A1
公开(公告)日：2010-09-23
申请号：US12659122
申请日：2010-02-25
申请人： Mitsuru Matsumoto
发明人： Mitsuru Matsumoto
IPC分类号： C01B3/04 , B01J20/04
CPC分类号： C01B3/065 , C01B3/0078 , C01B6/04 , Y02E60/324 , Y02E60/362 , Y02E60/364
摘要： The present invention is: a hydride composite containing NaH and a metal salt containing an alkali earth metal or a transition metal; and a preparation process of a hydrogen gas including a reaction process to react such a hydride composite with an ammonia gas. Further, the present invention is: a hydride composite containing NaH, a metal salt containing an alkali earth metal or a transition metal, and an ammonia source that is a solid at ordinary temperatures and generates an ammonia gas by decomposition; and a preparation process of a hydrogen gas including a reaction process to heat such a hydride composite.
摘要翻译：本发明是：含有NaH和含有碱土金属或过渡金属的金属盐的氢化物复合物; 以及包括使这种氢化物复合物与氨气反应的反应过程的氢气的制备方法。另外，本发明是含有NaH，含有碱土类金属或过渡金属的金属盐的氢化物复合体和在常温下为固体并通过分解而产生氨气的氨源，以及包括加热这种氢化物复合物的反应过程的氢气的制备方法。

7. 发明申请

US20100068134A1 METHODS OF ENHANCING KINETIC PROPERTIES OF HYDROGEN STORAGE MATERIALS BY SELF-CATALYSIS 审中-公开
标题翻译：通过自催化增强氢储存材料的动力学性质的方法
公开(公告)号：US20100068134A1
公开(公告)日：2010-03-18
申请号：US12233246
申请日：2008-09-18
申请人： Andrea Sudik , Jun Yang , Donald J. Siegel , Christopher Mark Wolverton
发明人： Andrea Sudik , Jun Yang , Donald J. Siegel , Christopher Mark Wolverton
IPC分类号： C01B3/00
CPC分类号： C01B3/0078 , C01B3/001 , C01B6/04 , C01B6/21 , Y02E60/324
摘要： Methods of enhancing the kinetic properties of solid-state hydrogen storage materials are disclosed. The methods of the present invention comprise a process of utilizing built-in, ancillary reactions to effectually catalyze primary hydrogen storage reactions. This self-catalysis process gives rise to novel mechanisms for solid-state hydrogen storage compositions that benefit from enhanced kinetic properties, thereby increasing the usefulness of hydrogen storage technologies. The methods of enhancing the kinetic properties of hydrogen storage compositions by implementing a self-catalyzing reaction mechanism generally include formulating a hydrogen desorption pathway in a hydrogen storage composition, the pathway including a hydrogen releasing reaction and an ancillary reaction; and selecting the ancillary reaction to produce a product that serves to enhance the kinetic properties of the hydrogen releasing reaction.
摘要翻译：公开了增强固态储氢材料的动力学性质的方法。本发明的方法包括利用内置的辅助反应来有效地催化初级储氢反应的方法。这种自催化过程为固态储氢组合物提供了新的机理，其受益于增强的动力学性质，从而增加储氢技术的有用性。通过实施自催化反应机理来提高储氢组合物的动力学性质的方法通常包括在储氢组合物中配制氢解吸途径，该途径包括氢释放反应和辅助反应; 并选择辅助反应以产生用于增强氢释放反应的动力学性质的产物。

8. 发明授权

US07678362B2 High density hydrogen storage material 有权
标题翻译：高密度储氢材料
公开(公告)号：US07678362B2
公开(公告)日：2010-03-16
申请号：US11471443
申请日：2006-06-20
申请人： Christopher Mark Wolverton , Gregory J. Lewis , John J. Low
发明人： Christopher Mark Wolverton , Gregory J. Lewis , John J. Low
IPC分类号： C01B3/04 , C09K3/00
CPC分类号： C01B3/0078 , C01B6/04 , C01B35/04 , H01M8/04216 , H01M8/065 , Y02E60/324
摘要： A hydrogen storage material. The hydrogen storage material is a combination of LiBH4 with MHx, wherein greater than about 50% of M comprises Al.
摘要翻译：储氢材料。储氢材料是LiBH4与MHx的组合，其中大于约50％的M包括Al。

9. 发明申请

US20090162709A1 Inorganic-hydrogen-polymer and hydrogen-polymer compounds and applications thereof 审中-公开
公开(公告)号：US20090162709A1
公开(公告)日：2009-06-25
申请号：US12155944
申请日：2008-06-11
申请人： Randell L. Mills
发明人： Randell L. Mills
IPC分类号： H01M8/18 , C01B6/00 , C01B3/02 , B01J19/08 , H01M8/04
CPC分类号： H01M4/48 , C01B3/00 , C01B6/04 , C01B6/24 , C01B15/00 , H01B1/122 , H01M4/383 , H01M4/86 , H01M10/46 , Y02E60/327 , Y02E60/328
摘要： Compounds are provided comprising at least one neutral, positive, or negative hydrogen species having a binding energy greater than its corresponding ordinary hydrogen species, or greater than any hydrogen species for which the corresponding ordinary hydrogen species is unstable or is not observed. Compounds comprise at least one increased binding energy hydrogen species and at least one other atom, molecule, or ion other than an increased binding energy hydrogen species. One group of such compounds contains one or more increased binding energy hydrogen species selected from the group consisting of Hn, Hn−, and Hn+ where n is a positive integer, with the proviso that n is greater than 1 when H has a positive charge. Another group of such compounds may have the formula [MHmM′X]n wherein m and n are each an integer, M and M′ are each an alkali or alkaline earth cation, X is a singly or doubly negative charged anion, and the hydrogen content Hm of the compound comprises at least one increased binding energy hydrogen species. Applications of the compounds include use in batteries, fuel cells, cutting materials, light weight high strength structural materials and synthetic fibers, corrosion resistant coatings, heat resistant coatings, xerographic compounds, proton source, photoluminescent compounds, phosphors for lighting, ultraviolet and visible light source, photoconductors, photovoltaics, chemiluminescent compounds, fluorescent compounds, optical coatings, optical filters, extreme ultraviolet laser media, fiber optic cables, magnets and magnetic computer storage media, superconductors, and etching agents, masking agents, agents to purify silicon, dopants in semiconductor fabrication, cathodes for thermionic generators, fuels, explosives, and propellants. Increased binding energy hydrogen compounds are useful in chemical synthetic processing methods and refining methods. The increased binding energy hydrogen ion has application as the negative ion of the electrolyte of a high voltage electrolytic cell. The selectivity of increased binding energy hydrogen species in forming bonds with specific isotopes provides a means to purify desired isotopes of elements.

10. 发明申请

US20070009425A1 Method for producing alkali metal hydrides and hydrogen 审中-公开
标题翻译：制备碱金属氢化物和氢的方法
公开(公告)号：US20070009425A1
公开(公告)日：2007-01-11
申请号：US10558585
申请日：2004-05-26
申请人： Wolf Johnssen
发明人： Wolf Johnssen
IPC分类号： C01B6/04
CPC分类号： C01B3/065 , C01B3/34 , C01B6/04 , C01B2203/0227 , C01B2203/0283 , Y02E60/362 , Y02E60/364 , Y02P20/133
摘要： The invention relates to a method for producing hydrogen, comprising: (i) reacting an alkali metal compound with a carbon-containing substance and hydrogen to obtain an alkali metal hydride; and (ii) reacting the alkali metal hydride that has been obtained with water to obtain hydrogen and alkali metal hydroxide. The invention also relates to a method comprising the steps of: (a) reacting a carbon source with water to obtain a carbon-containing substance; and (b) reacting the carbon-containing substance that has been obtained with hydrogen and an alkali metal compound to obtain an alkali metal hydride. In another embodiment a method is described comprising the steps of: (a) reacting a carbon source with water to obtain hydrogen; and (b) reacting the hydrogen that has been obtained with a carbon-containing substance and an alkali metal compound to obtain an alkali metal hydride.
摘要翻译：本发明涉及一种生产氢的方法，包括：（i）使碱金属化合物与含碳物质和氢反应，得到碱金属氢化物; 和（ii）使所得到的碱金属氢化物与水反应得到氢和碱金属氢氧化物。本发明还涉及一种方法，其包括以下步骤：（a）使碳源与水反应以获得含碳物质; 和（b）使所获得的含碳物质与氢和碱金属化合物反应，得到碱金属氢化物。在另一个实施方案中，描述了一种方法，其包括以下步骤：（a）使碳源与水反应以获得氢; 和（b）使所获得的氢与含碳物质和碱金属化合物反应，得到碱金属氢化物。

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