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    • 5. 发明申请
    • Quartz member for semiconductor manufacturing equipment and method for metal analysis in quartz member
    • 石英构件用于半导体制造设备和金属分析方法的石英构件
    • US20030000458A1
    • 2003-01-02
    • US10181980
    • 2002-07-24
    • Yoshinori MarumoKaname SuzukiTeruyuki HayashiTakashi Tanahashi
    • C30B001/00
    • C30B35/00C30B31/10G01N1/32G01N1/4044Y10T117/10
    • Quartz member such as a quartz tube for semiconductor manufacturing equipment capable of heat treating a substrate to be treated without causing contamination, a manufacturing method of such quartz member, thermal treatment equipment furnished with such quartz member, and an analysis method of metal in quartz member are provided. A quartz specimen is immersed in hydrofluoric acid to expose a layer to be analyzed located at a prescribed depth. On an exposed surface, a decomposition liquid such as hydrofluoric acid or nitric acid is dripped to decompose only an extremely thin layer to be analyzed, followed by recovering of the decomposition liquid. The decomposition liquid is quantitatively analyzed by use of atomic absorption spectroscopy (AAS) or the like to measure an amount of metal contained in the decomposition liquid. From a difference of thicknesses before and after the decomposition and an area of dripped decomposition liquid, a volume of a decomposed layer to be analyzed is obtained. From this and the amount of metal contained in the decomposition liquid, a concentration of metal contained in the layer to be analyzed, in addition a diffusion coefficient of a layer to be analyzed is calculated. With thus obtained diffusion coefficient as an index, quartz material in which metal diffuses with difficulty is sorted out. With thus sorted quartz material, a quartz member used for semiconductor manufacturing equipment such as a quartz tube is manufactured.
    • 石英部件,例如能够对被处理基板进行热处理而不引起污染的半导体制造设备的石英管,这种石英部件的制造方法,配备有这种石英部件的热处理设备以及石英部件中的金属分析方法 被提供。 将石英样品浸入氢氟酸中以暴露位于规定深度的被分析层。 在暴露的表面上,滴加氢氟酸或硝酸等分解液,仅分解极薄的待分析层,然后回收分解液。 通过使用原子吸收光谱法(AAS)等对分解液进行定量分析,以测量分解液中所含的金属的量。 根据分解前后的厚度差和滴落分解液的面积,得到待分析体积的分解层。 由此和分解液中所含的金属的量,计算待分析层中所含的金属的浓度,另外计算待分析层的扩散系数。 以这样获得的扩散系数作为指标,分析难以扩散金属的石英材料。 通过这样排列的石英材料,制造了用于诸如石英管的半导体制造设备的石英部件。
    • 6. 发明授权
    • Vertical heat-treating apparatus and heat insulator
    • 立式热处理装置和隔热材料
    • US5601428A
    • 1997-02-11
    • US540136
    • 1995-10-06
    • Shinichi OkoshiHiroyuki Kimura
    • Shinichi OkoshiHiroyuki Kimura
    • C30B31/10C30B31/12C30B33/00F27B17/00F27D7/02F27D3/12
    • C30B33/00C30B31/10F27B17/0025F27D7/02
    • It is an object of the present invention to provide a vertical heat treatment apparatus having a heat insulator, which has sufficient heat insulation, heat retention and high load pressure bearing properties to cope with increased size dimensions and number of layers of wafer workpieces and can be particularly advantageously used as a semiconductor and TFT substrate heat treatment apparatus. The apparatus features the use of a heat insulator casing 40 supporting a substrate holder 3 on its top and receiving a heat insulator 50 having numerous inner microspaces in its lower space, and defining a substrate holder or boat insulator receiving space A and a heat insulator receiving space B such that these spaces are hermetically sealed with respect to each other by the heat insulator casing. It is also a feature of the apparatus that the heat insulator receiving space B is in communication with the exterior or that the pressure in the heat insulator receiving space B can be reduced or increased through a contact section of a closure member 70 which supports the heat insulator casing 40 or a heat insulator casing flange 41.
    • 本发明的目的是提供一种具有绝热体的立式热处理装置,其具有足够的隔热性,保温性和高负载压力承载性能,以应对尺寸增加的尺寸和晶片工件的层数,并且可以 特别有利地用作半导体和TFT基板热处理装置。 该装置的特征在于使用在其顶部上支撑衬底保持器3的绝热器壳体40,并且在其下部空间中容纳具有多个内部微型体的隔热件50,并且限定衬底保持器或舟形绝缘体容纳空间A和隔热件接收 空间B,使得这些空间通过绝热壳体相对于彼此气密密封。 绝热体接收空间B与外部连通的装置的特征还在于,能够通过支撑热量的封闭构件70的接触部来减小或增加绝热体容纳空间B中的压力 绝缘体套管40或绝热体套管凸缘41。