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1. 发明授权

US09409825B2 Granulation of fine powder 有权
标题翻译：造粒细粉
公开(公告)号：US09409825B2
公开(公告)日：2016-08-09
申请号：US13971157
申请日：2013-08-20
申请人： Los Alamos National Security, LLC
发明人： Ching-Fong Chen
IPC分类号： C04B35/51 , C04B35/626
CPC分类号： C04B35/51 , C01F15/00 , C01F17/0043 , C01G43/00 , C01G43/01 , C01G56/00 , C01G56/005 , C01P2004/03 , C01P2004/50 , C01P2004/60 , C01P2004/61 , C01P2004/82 , C01P2006/10 , C01P2006/12 , C04B35/6262 , C04B35/62695 , C04B2235/3229 , C04B2235/5409 , C04B2235/604 , C04B2235/608 , C04B2235/77
摘要： A mixture of fine powder including thorium oxide was converted to granulated powder by forming a first-green-body and heat treating the first-green-body at a high temperature to strengthen the first-green-body followed by granulation by crushing or milling the heat-treated first-green-body. The granulated powder was achieved by screening through a combination of sieves to achieve the desired granule size distribution. The granulated powder relies on the thermal bonding to maintain its shape and structure. The granulated powder contains no organic binder and can be stored in a radioactive or other extreme environment. The granulated powder was pressed and sintered to form a dense compact with a higher density and more uniform pore size distribution.
摘要翻译：将包括氧化钍在内的细粉末的混合物通过形成第一生体并在高温下热处理第一生体而将其转化成粒状粉末，以加强第一生体，然后通过粉碎或研磨制粒热处理的第一生体。颗粒粉末通过筛选组合来实现，以获得所需的颗粒尺寸分布。造粒粉末依赖于热粘合以保持其形状和结构。造粒粉末不含有机粘合剂，可放置在放射性或其他极端环境中。将造粒粉末压制并烧结以形成具有更高密度和更均匀孔径分布的致密成型体。

2. 发明授权

US09260767B2 Processes for recovering rare earth elements from aluminum-bearing materials 有权
标题翻译：从含铝材料回收稀土元素的工艺
公开(公告)号：US09260767B2
公开(公告)日：2016-02-16
申请号：US14005885
申请日：2012-03-19
申请人： Richard Boudreault , Denis Primeau , Heinz Krivanec , Carsten Dittrich , Joel Fournier , Raymond Simoneau , Maria Christina Garcia
发明人： Richard Boudreault , Denis Primeau , Heinz Krivanec , Carsten Dittrich , Joel Fournier , Raymond Simoneau , Maria Christina Garcia
IPC分类号： C22B21/00 , C22B59/00 , C22B3/10 , C22B3/44 , C22B58/00 , C22B26/12 , C22B34/34 , C22B3/06 , C22B3/46 , C22B34/12 , C01G1/02 , C01F7/06 , C01F7/30 , C01F7/22 , C01G23/04 , C01G3/02 , C01G5/00 , C01G7/00 , C01G49/02 , C01G9/02 , C01G51/04 , C01G39/02 , C01G43/01 , C01G53/04 , C01G45/02 , C01G55/00 , C01B13/18 , C01D1/00 , C01F5/02 , C01F15/00 , C01F17/00
CPC分类号： C22B59/00 , C01B13/18 , C01D1/00 , C01F5/02 , C01F7/066 , C01F7/22 , C01F7/306 , C01F15/00 , C01F17/0043 , C01G1/02 , C01G3/02 , C01G5/00 , C01G7/00 , C01G9/02 , C01G23/04 , C01G39/02 , C01G43/01 , C01G45/02 , C01G49/02 , C01G51/04 , C01G53/04 , C01G55/004 , C21B15/00 , C22B3/06 , C22B3/10 , C22B3/22 , C22B3/24 , C22B3/42 , C22B3/44 , C22B3/46 , C22B21/0015 , C22B21/0023 , C22B26/12 , C22B34/1245 , C22B34/34 , C22B58/00 , C25D3/54 , Y02P10/234
摘要： The present disclosure relates to processes for recovering rare earth elements from an aluminum-bearing material. The processes can comprise leaching the aluminum-bearing material with an acid so as to obtain a leachate comprising at least one aluminum ion, at least one iron ion, at least one rare earth element, and a solid, and separating the leachate from the solid. The processes can also comprise substantially selectively removing at least one of the at least one aluminum ion and the at least one iron ion from the leachate and optionally obtaining a precipitate. The processes can also comprise substantially selectively removing the at least one rare earth element from the leachate and/or the precipitate.
摘要翻译：本公开涉及从含铝材料回收稀土元素的方法。所述方法可以包括用酸浸出含铝材料，以便获得包含至少一种铝离子，至少一种铁离子，至少一种稀土元素和固体的渗滤液，并将浸出液与固体分离。所述方法还可以包括基本上选择性地从渗滤液中除去至少一种铝离子和至少一种铁离子中的至少一种，并任选地获得沉淀物。所述方法还可以包括基本上选择性地从渗滤液和/或沉淀物中除去至少一种稀土元素。

3. 发明授权

US5494648A Process for removing thorium and recovering vanadium from titanium chlorinator waste 失效
标题翻译：从钛氯化物废物中去除钍和回收钒的方法
公开(公告)号：US5494648A
公开(公告)日：1996-02-27
申请号：US188863
申请日：1994-01-31
申请人： Richard S. Olsen , John T. Banks
发明人： Richard S. Olsen , John T. Banks
IPC分类号： C01F15/00 , C01G49/00 , C22B34/12 , C22B34/22 , C22B60/02
CPC分类号： C01F15/00 , C01G49/0018 , C22B34/1213 , C22B34/22 , C22B60/02 , C01P2006/80
摘要： A process for removal of thorium from titanium chlorinator waste comprising: (a) leaching an anhydrous titanium chlorinator waste in water or dilute hydrochloric acid solution and filtering to separate insoluble minerals and coke fractions from soluble metal chlorides; (b) beneficiating the insoluble fractions from step (a) on shaking tables to recover recyclable or otherwise useful TiO.sub.2 minerals and coke; and (c) treating filtrate from step (a) with reagents to precipitate and remove thorium by filtration along with acid metals of Ti, Zr, Nb, and Ta by the addition of the filtrate (a), a base and a precipitant to a boiling slurry of reaction products (d); treating filtrate from step (c) with reagents to precipitate and recover an iron vanadate product by the addition of the filtrate (c), a base and an oxidizing agent to a boiling slurry of reaction products; and (e) treating filtrate from step (d) to remove any remaining cations except Na by addition of Na.sub.2 CO.sub.3 and boiling.
摘要翻译：一种从钛氯化物废料中除去钍的方法，包括：（a）将无水氯化钛废物浸入水或稀盐酸溶液中并过滤以从可溶性金属氯化物中分离出不溶性矿物和焦炭馏分; （b）从摇台上挑选步骤（a）中的不溶级分，以回收可回收或以其他方式使用的二氧化钛矿物和焦炭; 和（c）用试剂处理来自步骤（a）的滤液，通过加入滤液（a），碱和沉淀剂将其与Ti，Zr，Nb和Ta的酸性金属一起过滤沉淀并除去钍沸腾的反应产物浆液（d）; 用试剂处理来自步骤（c）的滤液，通过向反应产物的沸腾浆液中加入滤液（c），碱和氧化剂来沉淀并回收钒酸铁产物; 和（e）处理来自步骤（d）的滤液，通过加入Na 2 CO 3并煮沸除去Na外的任何剩余的阳离子。

4. 发明授权

US4971734A Method of making nuclear fuel pellets, comprising producing and using pourable, frittable powders obtained directly by precipitation of peroxides 失效
标题翻译：制备核燃料颗粒的方法，包括生产和使用直接通过沉淀过氧化物获得的可倾倒的易碎粉末
公开(公告)号：US4971734A
公开(公告)日：1990-11-20
申请号：US377117
申请日：1989-07-10
申请人： Antoine Floreancig , Paul Mollard
发明人： Antoine Floreancig , Paul Mollard
IPC分类号： C01B15/047 , C01F15/00 , C01F17/00 , C01G27/02 , C01G43/01 , C01G56/00 , C04B35/64 , G21C3/62
CPC分类号： C01F17/0043 , C01B15/0475 , C01F15/00 , C01F17/0012 , C01G27/02 , C01G43/01 , C01G56/005 , G21C3/623 , C01P2004/40 , C01P2004/61 , C01P2006/10 , C01P2006/12 , C01P2006/20 , C01P2006/60 , C01P2006/80 , C01P2006/82 , Y02E30/38
摘要： A method of obtaining pellets of MxOy oxide, where M represents one or more elements used to make nuclear fuel pellets, as a means of obtaining very high density fritted pellets directly, i.e. without the intermediate powders being conditioned, comprising starting with a solution of soluble salts of the M elements, and treating them with hydrogen peroxide with the pH kept at from 2 to 2.5, in a continuous fluidized bed reactor comprising at least 3 superposed cylindrical sections of different diameters, the solutions in the central section being agitated vigorously, to obtain a precipitate which is subsequently calcined reduced, pressed then fritted.
摘要翻译：获得M x O y氧化物颗粒的方法，其中M表示用于制造核燃料颗粒的一种或多种元素，作为直接获得非常高密度烧结颗粒的方法，即不调节中间体粉末，包括从可溶性溶液在含有至少3个重叠的不同直径的圆柱形切片的连续流化床反应器中，将pH值保持在2至2.5的过氧化氢处理它们，并将中心部分的溶液剧烈搅拌，至得到沉淀，随后煅烧还原，然后烧结。

5. 发明授权

US4615834A Process and apparatus for producing microspheres of fissile and/or fertile materials 失效
标题翻译：用于生产易裂变和/或可育材料微球的方法和装置
公开(公告)号：US4615834A
公开(公告)日：1986-10-07
申请号：US578615
申请日：1984-02-13
申请人： Shigeru Yamagishi , Yoshihisa Takahashi , Koreyuki Shiba
发明人： Shigeru Yamagishi , Yoshihisa Takahashi , Koreyuki Shiba
IPC分类号： B01J2/08 , C01F15/00 , C01G43/00 , C01G56/00 , G21C3/62 , G21C19/00 , G21C21/00
CPC分类号： C01G43/00 , B01J2/08 , C01F15/00 , C01G56/004 , G21C3/623 , Y02E30/38
摘要： A process and an apparatus are, herein, disclosed for producing microspheres of fissile and/or fertile materials with a high degree of sphericity from a feed solution starter containing at least one metal salt selected from among thorium, uranium and plutonium by using as a gelling medium an organic solvent that has a higher density and a greater interfacial tension with water than the feed solution and which is capable of dissolving ammonia.
摘要翻译：本文公开了一种方法和装置，用于从含有选自钍，铀和钚中的至少一种金属盐的进料溶液起动器中制备具有高度球形度的易裂变和/或可育材料的微球，通过使用作为凝胶介质与进料溶液相比具有更高的密度和更大的与水的界面张力并且能够溶解氨的有机溶剂。

6. 发明授权

US3761563A Reacting metal oxides with a sulfate and pyrosulfate mixture 失效
标题翻译：用硫酸和磷酸盐混合物反应金属氧化物
公开(公告)号：US3761563A
公开(公告)日：1973-09-25
申请号：US3761563D
申请日：1971-04-20
申请人： KERNFORSCHUNGSANLAGE JUELICH
发明人： KAISER G , ZIMMER E
IPC分类号： C01F15/00 , C01G25/02 , C01G43/00 , C22B3/08 , C22B34/10 , C22B60/02 , C22B60/04 , C01G56/00
CPC分类号： C22B3/08 , C01F15/00 , C01G25/02 , C01G43/00 , C01P2004/82 , C22B34/10 , C22B60/0208 , C22B60/0213 , C22B60/0291 , C22B60/04 , Y02P10/234
摘要： The invention relates to a process for converting oxides to sulfates. The contemplated oxides are slowly soluble or insoluble in acids and/or lyes, particularly the oxides found in nuclear fuel and/or breeder material. The oxides are mixed with a sulfate and a disulfate (pyrosulfate) and heated to between about 650* C and 800* C for a comparatively short time. The amount of disulfate should be at least stoichiometric.
摘要翻译：本发明涉及将氧化物转化为硫酸盐的方法。预期的氧化物缓慢溶解或不溶于酸和/或碱液，特别是在核燃料和/或育种材料中发现的氧化物。将氧化物与硫酸盐和二硫酸盐（焦硫酸盐）混合并加热至约650℃至800℃相对较短的时间。二硫酸盐的量应至少为化学计量。

7. 发明授权

US3700416A Extraction of vanadium and copper with fluorinated beta-diketones 失效
标题翻译：用氟化的白蛋白提取钒和铜
公开(公告)号：US3700416A
公开(公告)日：1972-10-24
申请号：US3700416D
申请日：1970-09-04
申请人： KERR MC GEE CHEM CORP
发明人： LUCID MICHAEL F
IPC分类号： B01D11/04 , C01F15/00 , C01G3/00 , C01G31/00 , C01G49/00 , C07C45/45 , C07C49/80 , C07C49/813 , C07C49/84 , C22B3/26 , C23G1/36
CPC分类号： C22B3/0021 , C01F15/00 , C01G3/00 , C01G31/003 , C01G49/0009 , C07C45/455 , C07C49/80 , C07C49/813 , C07C49/84 , Y02P10/234
摘要： A METHOD FOR THE EXTRACTION OF METALS FROM AQUEOUS ACIDIC SOLUTIONS IS PROVIDED WHICH COMPRISES EXTRACTING THE METALS WITH A FLUORINATED B-DIKETONE IN AN ORGANIC SOLVENT, THE METAL BEING EXTRACTED INTO THE ORGANIC PHASE.

8. 发明授权

US3678100A 2-haloperfluoro-1-cycloalken-1-yl phosphoryl compounds and process for the preparation thereof 失效
标题翻译： 2-卤代环戊烯-1-环烯酮-1-YL磷化合物及其制备方法
公开(公告)号：US3678100A
公开(公告)日：1972-07-18
申请号：US87080169
申请日：1969-09-05
申请人： BORG WARNER
发明人： FRANK ARLEN W , BARANAUCKAS CHARLES F
IPC分类号： C01F15/00 , C07F9/30 , C07F9/32 , C07F9/38 , C07F9/40 , C07F9/42 , C08J9/00 , C22B3/38 , C22B60/02 , C11D1/34
CPC分类号： C01F15/00 , C07F9/303 , C07F9/3223 , C07F9/383 , C07F9/4018 , C07F9/4025 , C07F9/42 , C08J9/0038 , C08J2375/04 , C08K5/53 , C22B3/0077 , C22B60/026 , C22B60/0291 , Y02P10/234 , C08L75/04 , C08L27/06
摘要： A PROCESS FOR THE PREPARTION OF A COMPOUND SELECTED FROM THE GROUP CONSISTING OF 2-HALOPERFLUORO-1-CYCLOALKEN-1YLPHOSPHONIC ACID AND 2-HALOPERFLUORO-1-CYCLOALKEN-1-YL PHOSPHINIC ACID, WHICH COMPRISES HYDROLYZING THE CORRESPONDING COMPOUND OF THE FORMULA

X-C
WHEREIN X IS SELECTED FROM THE GROUP CONSISTING OF CHLORINE AND BROMINE, R AND R'' ARE ORGANIC RADICALS, M IS FROM 2 TO 4, AND N IS FROM 0 TO 1.

9. 发明授权

US3676081A Removal of titanium from monazite ores 失效
标题翻译：从MONAZITE ORES去除钛
公开(公告)号：US3676081A
公开(公告)日：1972-07-11
申请号：US3676081D
申请日：1968-12-31
申请人： JOSEPH PETER MAZZA
发明人： MAZZA JOSEPH PETER
IPC分类号： C01F15/00 , C22B34/12 , C22B61/04 , C22B53/00
CPC分类号： C22B34/1245 , C01F15/00
摘要： TITANIUM OCCURRING AS AN IMPURITY IN MONAZITE ORES IS REMOVED BY TREATMENT OF A THORIUM CHLORIDE SOLUTION DERIVED FROM SAID ORES WHICH CONTAINS SAID TITANIUM WITH TANNIC ACID TO PRECIPITATE THE TITANIUM, THEREBY REMOVING 90% OR MORE OF THE LATTER.

10. 发明授权

US3495954A Precipitation processes for metalcontaining materials 失效
标题翻译：金属材料的降解过程
公开(公告)号：US3495954A
公开(公告)日：1970-02-17
申请号：US3495954D
申请日：1967-03-27
申请人： ATOMIC ENERGY AUTHORITY UK
发明人： GRIMES JOHN HERBERT , DRESS WILLIAM
IPC分类号： B01J2/02 , B01J2/04 , B01J2/08 , B01J2/20 , B22F3/00 , B22F9/20 , C01B25/26 , C01B31/30 , C01B33/20 , C01F7/34 , C01F15/00 , C01G56/00 , C03C17/25 , C04B41/50 , C22C1/02 , C22C1/10 , C22C32/00 , C22B61/04
CPC分类号： C22C32/00 , B01J2/02 , B01J2/04 , B01J2/08 , B01J2/20 , B22F3/00 , B22F9/20 , C01B25/26 , C01B32/90 , C01B33/20 , C01F7/34 , C01F15/00 , C01G56/004 , C01G56/005 , C01P2004/32 , C01P2006/60 , C01P2006/80 , C03C17/25 , C03C2217/229 , C03C2218/111 , C04B41/5025 , C22C1/02 , C22C1/1026 , C04B41/4505 , C04B41/4584

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