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1. 发明申请

US20210027905A1 SYSTEMS, APPARATUS AND METHODS FOR SEPARATING ACTINIUM, RADIUM, AND THORIUM 有权
公开(公告)号：US20210027905A1
公开(公告)日：2021-01-28
申请号：US17040652
申请日：2019-03-26
申请人： Andrew Kyle Henderson ROBERTSON , TRIUMF, A JOINT VENTURE OF THE GOVERNORS OF THE UNIVERSITY OF ALBERTA, THE UNIVERSITY OF BRITISH
发明人： Andrew Kyle Henderson ROBERTSON , Hua YANG , Stefan ZEISLER , Paul SCHAFFER
IPC分类号： G21G1/00 , C01F17/13 , C01B15/047 , C01B11/22 , B01D15/36 , B01D15/18 , G21G1/10
摘要： A method of separating actinium and/or radium from proton-irradiated thorium metal. The thorium metal is irradiated to produce isotopes including thorium, actinium and/or radium. The resultant product is dissolved in solution and a selective precipitant is used to precipitate a bulk portion of the thorium. The precipitated thorium can be recovered. Chromatography is carried out on the remaining solution to remove residual thorium and to separate the actinium from the radium.

2. 发明授权

US10119036B2 Process for the formation of metal oxide nanoparticles coating of a solid substrate 有权
公开(公告)号：US10119036B2
公开(公告)日：2018-11-06
申请号：US13821279
申请日：2011-09-07
申请人： Ovadia Lev , Sergey Sladkevich , Petr Prikhodchenko , Genia Gun
发明人： Ovadia Lev , Sergey Sladkevich , Petr Prikhodchenko , Genia Gun
IPC分类号： B05D3/02 , C09D5/24 , B01J23/14 , B01J23/18 , B01J27/057 , B01J35/00 , B01J37/02 , B05D1/00 , B82Y30/00 , C01B15/04 , C01B15/047 , C04B41/00 , C23C18/00 , C23C18/12 , C01B32/00 , B01J21/08 , B01J21/16
摘要： The present invention provides a process for the formation of a coating comprising peroxynanoparticles of metals selected from the group consisting of: Ga, Ge, As, Se, In, Sn, Sb, Te, Tl, Pb and Bi on a solid substrate, comprising providing a basic solution containing at least a first metal selected from said group and hydrogen peroxide, and contacting said solution with a solid substrate having oxygen-containing chemically reactive groups on its surface.

3. 发明授权

US10106409B2 Method for activating U3O8 with a view to converting same into hydrated UO4 有权
公开(公告)号：US10106409B2
公开(公告)日：2018-10-23
申请号：US15119906
申请日：2015-02-19
申请人： AREVA NC
发明人： Mehdi Arab , Bertrand Morel , Murielle Rivenet
IPC分类号： C01G43/01 , C01B15/047 , C01G43/00 , C22B3/00
摘要： A method to activate U3O8 for conversion of this uranium oxide to hydrated UO4 via reaction with hydrogen peroxide H2O2, wherein the following successive steps are performed: a) an aqueous suspension is prepared containing a powder of U3O8 and hydrogen peroxide; b) the aqueous suspension containing a powder of U3O8 and hydrogen peroxide is contacted with ozone, whereby an aqueous suspension is obtained of a powder of activated U3O8; c) optionally the powder of activated U3O8 is separated from the aqueous suspension. A method to convert U3O8 to hydrated UO4 of formula UO4, nH2O where n is 2 or 4, comprising at least one step at which hydrogen peroxide H2O2 is added to the aqueous suspension of a powder of activated U3O8 obtained at the end of step b) of the activation method or to an aqueous suspension prepared by placing in suspension in water the powder of activated U3O8 obtained at the end of step c) of the activation method.

4. 发明授权

US09045350B2 Method for converting UO3 or U3O8 into hydrated UO4 有权
标题翻译：将UO3或U3O8转化为水合UO4的方法
公开(公告)号：US09045350B2
公开(公告)日：2015-06-02
申请号：US13995277
申请日：2011-12-16
申请人： Bertrand Morel , David Amaraggi , Mehdi Arab , Rudy Thomas , Murielle Rivenet , Francis Abraham
发明人： Bertrand Morel , David Amaraggi , Mehdi Arab , Rudy Thomas , Murielle Rivenet , Francis Abraham
IPC分类号： C01G43/01 , C01B15/047 , C01G43/06
CPC分类号： C01G43/01 , C01B15/0475 , C01G43/06 , C01P2002/72 , C01P2004/03 , C01P2004/10 , C01P2004/54 , C01P2006/12
摘要： A method for converting UO3 and/or U3O8 into hydrated UO4 of formula UO4.nH2O wherein n is 2 or 4, comprising the following successive steps: a) preparing an aqueous suspension of a UO3 powder and/or a U3O8 powder; b) adding hydrogen peroxide H2O2 to the aqueous suspension of a UO3 and/or U3O8 powder, converting the UO3 and/or U3O8 into hydrated UO4 and precipitating, crystallizing the hydrated UO4 in the suspension; c) recovering the precipitate, crystals of UO4 hydrate; d) optionally, washing the recovered UO4 hydrate precipitate, crystal(s); e) optionally, repeating step d); f) optionally, drying the precipitate, the crystals; wherein the addition of H2O2 to the aqueous suspension is carried out so that the suspension contains a stoichiometric excess of H2O2 relatively to the stoichiometry of the reaction from UO3: UO3+nH2O+H2O2→UO4.nH2O+H2O (1) or of the reaction from U3O8 UO2.67+1.33H2O2+nH2O→UO4.nH2O+1.33H2O (2), and the pH of the suspension is maintained in steps a) and b) at a value comprised between 2 and 3.
摘要翻译：将UO 3和/或U 3 O 8转化为式UO·4H 2 O的水合UO 4的方法，其中n为2或4，包括以下连续步骤：a）制备UO 3粉末和/或U 3 O 8粉末的水性悬浮液; b）向UO 3和/或U 3 O 8粉末的水性悬浮液中加入过氧化氢H 2 O 2，将UO 3和/或U 3 O 8转化为水合UO 4并沉淀，使悬浮液中的水合UO4结晶; c）回收沉淀物，UO4水合物晶体; d）任选地，洗涤回收的UO4水合物沉淀物，晶体; e）任选地，重复步骤d）; f）任选地，干燥沉淀物，晶体; 其中向含水悬浮液中加入H 2 O 2使得悬浮液相对于来自UO 3 :OO 3 + nH 2 O + H 2 O 2→UO 4·n H 2 O + H 2 O（1）或反应的反应的化学计量比含有化学计量过量的H 2 O 2 从U3O8 UO2.67 + 1.33H2O2 + nH2O→UO4·nH2O + 1.33H2O（2），并且悬浮液的pH在步骤a）和b）中保持在2和3之间的值。

5. 发明授权

US09034169B2 Method for detection of cyanide in water 有权
标题翻译：水中氰化物检测方法
公开(公告)号：US09034169B2
公开(公告)日：2015-05-19
申请号：US13827999
申请日：2013-03-14
申请人： KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
发明人： Mohammed Ashraf Gondal , Qasem Ahmed Qasem Drmosh , Z. H. Yamani , Tawfik Abdo Saleh
IPC分类号： G01N27/26 , G01N27/30 , G01N27/416 , G01N33/18 , C01B15/047
CPC分类号： G01N27/30 , C01B15/047 , G01N27/4166 , G01N33/182 , Y10S977/773 , Y10T436/172307
摘要： The method for detection of cyanide in water is a method for the detection of a highly toxic pollutant, cyanide, in water using ZnO2 nanoparticles synthesized locally by an elegant Pulsed Laser Ablation technique. ZnO2 nanoparticles having a median size of 4 nm are synthesized from pure zinc metal target under UV laser irradiation in a 1-10% H2O2 environment in deionized water. The synthesized ZnO2 nanoparticles are suspended in dimethyl formamide in the presence of Nafion, and then ultrasonicated to create a homogenous suspension, which is used to prepare a thin film of ZnO2 nanoparticles on a metal electrode. The electrode is used for cyanide detection.
摘要翻译：氰化物在水中的检测方法是使用典型的脉冲激光烧蚀技术局部合成的ZnO 2纳米颗粒，检测水中高毒性污染物氰化物的方法。中性粒径为4nm的ZnO 2纳米粒子在纯化学金属靶材中，在去离子水中，在1-10％H 2 O 2环境下，在UV激光照射下合成。合成的ZnO 2纳米颗粒在Nafion存在下悬浮于二甲基甲酰胺中，然后进行超声波处理，产生均匀的悬浮液，用于在金属电极上制备ZnO2纳米粒子薄膜。电极用于氰化物检测。

6. 发明授权

US6113861A Photocatalyst sheet 失效
标题翻译：光触媒片
公开(公告)号：US6113861A
公开(公告)日：2000-09-05
申请号：US29393
申请日：1998-02-27
申请人： Shiro Ogata
发明人： Shiro Ogata
IPC分类号： B32B7/02 , B01D53/86 , B01J35/00 , B32B9/00 , C01B15/047 , C01G23/047 , A61L9/16
CPC分类号： B01D53/86 , B01J35/002 , B01J35/004 , B01D2255/802 , Y10T428/2927 , Y10T428/2949 , Y10T428/2967
摘要： A photocatalytic sheet which has a base made of polymeric organic compound, that is not decomposed by a photocatalytic function, and also hardly loses the photocatalytic function after washing and is capable of providing the photocatalytic function even in an environment without sufficient ultraviolet radiation from outside. Using a fiber, a filament, a yarn made of fibers or filaments, a ribbon, a knitted fabric, a woven fabric, a nonwoven fabric, or a film as the base, a base protective layer is formed on a part of the base, which is made of the polymeric organic compound, and a photocatalytic semiconductor layer is formed on the entire surface of the base including the base protective layer.
摘要翻译： PCT No.PCT / JP97 / 02242 Sec。 371日期1998年2月27日 102（e）1998年2月27日PCT 1997年6月27日PCT公布。公开号WO98 / 00290 日期1998年1月8日一种具有由聚合有机化合物制成的基底的光催化片，其不被光催化功能分解，并且在洗涤后几乎不失去光催化功能，并且即使在没有足够的环境的环境中也能够提供光催化功能紫外线辐射从外面。使用纤维，长丝，由纤维或长丝制成的纱线，丝带，针织物，机织织物，无纺布或膜作为基底，在基底的一部分上形成基底保护层，其由聚合有机化合物制成，并且在包括基底保护层的基底的整个表面上形成光催化半导体层。

7. 发明授权

US5114606A Bleaching composition comprising as a bleaching catalyst a complex of manganese with a non-carboxylate polyhydroxy ligand 失效
标题翻译：漂白组合物作为漂白催化剂复合锰与非羧酸聚氧乙烯基配合物
公开(公告)号：US5114606A
公开(公告)日：1992-05-19
申请号：US657582
申请日：1991-02-19
申请人： Marten R. P. van Vliet , Jan E. Iburg
发明人： Marten R. P. van Vliet , Jan E. Iburg
IPC分类号： B01J31/02 , B01J31/22 , C01B15/043 , C01B15/047 , C10B15/00 , C11D3/39 , C11D3/395 , C11D7/54 , D06L3/02
CPC分类号： C11D3/3932
摘要： A stable and effective manganese complex for use as a peroxy compound bleach catalyst is disclosed, the catalyst being a water-soluble complex of manganese (II), (III), or (IV) or mixtures thereof with a ligand which is a non-carboxylate polyhydroxy compound having at least three consecutive C--OH groups in its molecular structure. Bleaching composition comprising a peroxy compound and the catalyst, as well as process for bleaching substrates using said catalyst are also disclosed. Preferred ligand is sorbitol and preferred catalyst is Mn-sorbitol complex.

8. 发明授权

US4793978A Method and apparatus for producing uranyl peroxide (U0.sub.4.2H.sub.2 O) from uranium and uranium alloy pieces 失效
标题翻译：从铀和铀合金片制造过氧化二铀酰（U04.2H2O）的方法和装置
公开(公告)号：US4793978A
公开(公告)日：1988-12-27
申请号：US5083
申请日：1987-01-20
申请人： Eugene N. Pollock
发明人： Eugene N. Pollock
IPC分类号： C01B15/047 , C22B60/02 , C01G43/01
CPC分类号： C01B15/0475 , C22B60/0226 , C22B60/0278
摘要： A method and apparatus are provided for producing uranyl peroxide (UO.sub.4.2H.sub.2 O) from uranium-bearing metal pieces. The uranium-bearing metal pieces are dissolved in a first aqueous solution containing nitric acid and between 0.5% and 5.0% fluoboric acid to provide a second aqueous solution which includes uranyl ions (UO.sub.2.sup.+2) and nitric and fluoboric acids. Hydrogen peroxide is added to the second aqueous solution to precipitate uranyl peroxide out of that solution and provide a third aqueous solution which contains nitric and fluoboric acids. The uranyl peroxide is then separated from the third aqueous solution.
摘要翻译：提供了一种从含铀金属片制备过氧化二烷基（UO4.2H2O）的方法和装置。将含铀金属片溶解在含有硝酸和0.5％至5.0％氟硼酸的第一水溶液中以提供包含铀酰离子（UO 2 + 2）和硝酸和氟硼酸的第二水溶液。向第二水溶液中加入过氧化氢，使该溶液中的二氧化铀过氧化物沉淀出来，并提供含有硝酸和氟硼酸的第三水溶液。然后将二氧化铀过氧化物与第三水溶液分离。

9. 发明授权

US4026910A Oxidation process using nickel peroxide oxidizing agents 失效
标题翻译：氧化工艺使用过氧化镍氧化剂
公开(公告)号：US4026910A
公开(公告)日：1977-05-31
申请号：US598307
申请日：1975-07-23
申请人： Roman Marbet
发明人： Roman Marbet
IPC分类号： C07C69/738 , C01B15/047 , C01G53/04 , C07C45/00 , C07C45/29 , C07C45/34 , C07C45/37 , C07C47/00 , C07C47/21 , C07C47/277 , C07C67/00 , C07C401/00 , C07C403/14 , C07C403/16 , C11C3/02 , C07C45/16
CPC分类号： C07C403/14 , C01B15/047 , C07C403/16 , C07C45/29 , C07C47/277 , C07C2101/16
摘要： Preparation of a nickel peroxide oxidizing agent from nickel hydroxide and its use in oxidizing .alpha.,.beta.-unsaturated alcohols to the corresponding carbonyl compounds.
摘要翻译：从氢氧化镍制备过氧化镍氧化物及其在将α，β-不饱和醇氧化成相应羰基化合物的用途。

10. 发明授权

US4024215A Production of uranium peroxide 失效
标题翻译：生产过氧化铀
公开(公告)号：US4024215A
公开(公告)日：1977-05-17
申请号：US571089
申请日：1975-04-24
申请人： Frank E. Caropreso , Donald F. Kreuz
发明人： Frank E. Caropreso , Donald F. Kreuz
IPC分类号： C01G43/01 , C01B15/047 , C22B60/02 , G21C3/62 , C01G43/00
CPC分类号： C22B60/0278 , C01B15/0475
摘要： A process of recovering uranium values as uranium peroxide from an aqueous uranyl solution containing dissolved vanadium and sodium impurities by treating the uranyl solution with hydrogen peroxide in an amount sufficient to have an excess of at least 0.5 parts H.sub.2 O.sub.2 per part of vanadium (V.sub.2 O.sub.5) above the stoichiometric amount required to form the uranium peroxide, the hydrogen peroxide treatment being carried out in three sequential phases consisting of I, a precipitation phase in which the hydrogen peroxide is added to the uranyl solution to precipitate the uranium peroxide and the pH of the reaction medium maintained in the range of 2.5 to 5.5 for a period of from about 1 to 60 minutes after the hydrogen peroxide addition; II, a digestion phase in which the pH of the reaction medium is maintained in the range of 3.0 to 7.0 for a period of about 5 to 180 minutes and III, a final phase in which the pH of the reaction medium is maintained in the range of 4.0 to 7.0 for a period of about 1 to 60 minutes during which time the uranium peroxide is separated from the reaction solution containing the dissolved vanadium and sodium impurities. The excess hydrogen peroxide is maintained during the entire treatment up until the uranium peroxide is separated from the reaction medium.
摘要翻译：一种从含有溶解的钒和钠杂质的水性铀酰溶液中回收铀值作为过氧化铀的方法，该方法是用足以使上述每部分钒（V 2 O 5）含有至少0.5份H 2 O 2过量的过氧化氢处理铀酰溶液形成铀过氧化物所需的化学计量量，过氧化氢处理在三个连续的阶段中进行，这三个阶段由I组成，其中过氧化氢加入到铀酰溶液中以沉淀过氧化铀和反应的pH 培养基保持在2.5至5.5的范围内，加入过氧化氢后约1至60分钟; II，消化阶段，其中反应介质的pH保持在3.0至7.0的范围内约5至180分钟的时间和III，其中反应介质的pH保持在该范围内的最后阶段为4.0〜7.0，时间约为1〜60分钟，在此期间，从含有溶解的钒和钠杂质的反应溶液中分离出铀过氧化物。在整个处理期间保持过量的过氧化氢直到从反应介质中分离出过氧化二铀。

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