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    • 4. 发明授权
    • Evaporator and concentrator in reactor and loading system
    • 蒸发器和浓缩器在反应堆和装载系统中
    • US07998418B1
    • 2011-08-16
    • US11754623
    • 2007-05-29
    • Joseph C. Matteo
    • Joseph C. Matteo
    • B01L99/10G01N15/06G01N33/00G01N33/48
    • B01J19/0093B01J2219/00795B01J2219/00822B01J2219/00831B01J2219/00833B01J2219/0086B01J2219/00867B01J2219/00873B01J2219/0088Y10T436/11Y10T436/25Y10T436/25375Y10T436/2575Y10T436/25875
    • An evaporator and concentrator in a reactor and loading system concentrates ions such as fluoride ions in some embodiments, and evaporates micro- to milliliter volumes of liquid solutions including intermediate and final product in other embodiments. It efficiently re-dissolves the evaporated solution generating a product, which is transferred to an external system as desired. The external system may be a micro-fluidic reactor system and/or loading system. The evaporator/concentrator has an input port for introducing liquids and solids. A capillary tube introduces gas, such as nitrogen gas, into a volume of solution contained within a v-vial, which produces an evaporating micro bubbler. A concentric tube, surrounding the capillary tube in some embodiments, introduces gas into the empty volume above the solution inside the v-vial, which is referred to as a vapor sweep. The vapor sweep assists in removing the evaporated solution from the v-vial through a vacuum tube.
    • 在一些实施方案中,反应器和负载系统中的蒸发器和浓缩器集中离子如氟离子,并且在其它实施方案中蒸发微至数毫升的液体溶液,包括中间体和最终产物。 它有效地重新溶解产生产品的蒸发溶液,根据需要将其转移到外部系统。 外部系统可以是微流体反应器系统和/或加载系统。 蒸发器/浓缩器具有用于引入液体和固体的输入端口。 毛细管将诸如氮气的气体引入包含在v型小瓶内的一定体积的溶液中,其产生蒸发的微型起泡器。 在一些实施例中,围绕毛细管的同心管将气体引入V型瓶内溶液上方的空体积,这被称为蒸气扫描。 蒸汽扫描有助于通过真空管从V型瓶中除去蒸发的溶液。