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1. 发明授权

US08324324B2 Composition and process for preparing curable organofluorine-modified polysilazanes, and polysilazanes prepared thereby 有权
标题翻译：制备可固化的有机氟改性聚硅氮烷的组合物和方法，以及由此制备的聚硅氮烷
公开(公告)号：US08324324B2
公开(公告)日：2012-12-04
申请号：US12792065
申请日：2010-06-02
申请人： Yu Yang , George G. I. Moore , Thomas P. Klun
发明人： Yu Yang , George G. I. Moore , Thomas P. Klun
IPC分类号： C08F283/00 , C08G77/62
CPC分类号： C08L83/04 , B05D3/0254 , B05D5/083 , B05D2202/25 , C08G77/24 , C08G77/62 , C08L83/16 , C08L83/00
摘要： A composition for preparing curable organofluorine-modified polysilazanes comprises (a) at least one curable oligomeric or polymeric polysilazane comprising at least one chemically reactive site; and (b) at least one fluorochemical compound comprising (1) at least one organofluorine or heteroorganofluorine moiety, and (2) at least one functional group that is capable of reacting with the curable oligomeric or polymeric polysilazane through at least one of the chemically reactive sites of the polysilazane. The curable organofluorine-modified polysilazanes can be prepared by combining the components of the composition and allowing or inducing the components to react.
摘要翻译：一种用于制备可固化的有机氟改性聚硅氮烷的组合物包括（a）至少一种包含至少一个化学反应性位点的可固化低聚或聚合聚硅氮烷; 和（b）至少一种含氟化合物，其包含（1）至少一种有机氟或异丙基部分，和（2）至少一种官能团，其能够通过化学反应性的至少一种与可固化的低聚或聚合的聚硅氮烷反应聚硅氮烷的地点。可固化的有机氟改性的聚硅氮烷可以通过组合组合物的组分并允许或诱导组分反应来制备。

2. 发明申请

US20100331498A1 COMPOSITION AND PROCESS FOR PREPARING CURABLE ORGANOFLUORINE-MODIFIED POLYSILAZANES, AND POLYSILAZANES PREPARED THEREBY 有权
标题翻译：用于制备可固化有机膦改性多晶硅的组合物和方法及其制备的多晶硅
公开(公告)号：US20100331498A1
公开(公告)日：2010-12-30
申请号：US12792065
申请日：2010-06-02
申请人： Yu Yang , George G. I. Moore , Thomas P. Klun
发明人： Yu Yang , George G. I. Moore , Thomas P. Klun
IPC分类号： C08G77/62
CPC分类号： C08L83/04 , B05D3/0254 , B05D5/083 , B05D2202/25 , C08G77/24 , C08G77/62 , C08L83/16 , C08L83/00
摘要： A composition for preparing curable organofluorine-modified polysilazanes comprises (a) at least one curable oligomeric or polymeric polysilazane comprising at least one chemically reactive site; and (b) at least one fluorochemical compound comprising (1) at least one organofluorine or heteroorganofluorine moiety, and (2) at least one functional group that is capable of reacting with the curable oligomeric or polymeric polysilazane through at least one of the chemically reactive sites of the polysilazane. The curable organofluorine-modified polysilazanes can be prepared by combining the components of the composition and allowing or inducing the components to react.
摘要翻译：一种用于制备可固化的有机氟改性聚硅氮烷的组合物包括（a）至少一种包含至少一个化学反应性位点的可固化低聚或聚合聚硅氮烷; 和（b）至少一种含氟化合物，其包含（1）至少一种有机氟或异丙基部分，和（2）至少一种官能团，其能够通过化学反应性的至少一种与可固化的低聚或聚合的聚硅氮烷反应聚硅氮烷的地点。可固化的有机氟改性的聚硅氮烷可以通过组合组合物的组分并允许或诱导组分反应来制备。

3. 发明授权

US08329830B2 Surface treatment process and treated article 有权
标题翻译：表面处理工艺和处理制品
公开(公告)号：US08329830B2
公开(公告)日：2012-12-11
申请号：US12792153
申请日：2010-06-02
申请人： Yu Yang , George G. I. Moore , Thomas P. Klun
发明人： Yu Yang , George G. I. Moore , Thomas P. Klun
IPC分类号： C08F283/00 , C08G77/62
CPC分类号： C08L83/04 , B05D3/0254 , B05D5/083 , B05D2202/25 , C08G77/24 , C08G77/62 , C08L83/16 , C08L83/00
摘要： A surface treatment process comprises (a) providing at least one substrate having at least one major surface; (b) combining (1) at least one curable oligomeric or polymeric polysilazane comprising at least one chemically reactive site, and (2) at least one fluorochemical compound comprising (i) at least one organofluorine or heteroorganofluorine moiety that comprises at least about six perfluorinated carbon atoms, and (ii) at least one functional group that is capable of reacting with the polysilazane through at least one of the chemically reactive sites; (c) allowing or inducing the polysilazane and the fluorochemical compound to react to form at least one curable organofluorine-modified polysilazane; (d) applying the curable organofluorine-modified polysilazane or its precursors to at least a portion of at least one major surface of the substrate; and (e) curing the curable organofluorine-modified polysilazane to form a surface treatment.
摘要翻译：表面处理方法包括（a）提供至少一个具有至少一个主表面的基材; （b）组合（1）包含至少一个化学反应位点的至少一种可固化的低聚或聚合的聚硅氮烷，和（2）至少一种含氟化合物，其包含（i）至少一种有机氟或杂有机氟部分，其包含至少约六个全氟化碳原子，和（ii）能够通过至少一个化学反应性位点与聚硅氮烷反应的至少一个官能团; （c）允许或诱导聚硅氮烷和含氟化合物反应以形成至少一种可固化的有机氟改性的聚硅氮烷; （d）将可固化的有机氟改性的聚硅氮烷或其前体施加到基材的至少一个主表面的至少一部分上; 和（e）固化可固化的有机氟改性聚硅氮烷以形成表面处理。

4. 发明授权

US07473462B2 Low refractive index fluoropolymer compositions having improved coating and durability properties 有权
$Low refractive index fluoropolymer compositions having improved coating and durability properties$
标题翻译：具有改进的涂层和耐久性的低折射率含氟聚合物组合物
公开(公告)号：US07473462B2
公开(公告)日：2009-01-06
申请号：US11972034
申请日：2008-01-10
申请人： William D. Coggio , Thomas P. Klun , George G. I. Moore , Naiyong Jing , Chuntao Cao , Sharon Wang , Patricia M. Savu , Lan H. Liu , Joan M. Noyola
发明人： William D. Coggio , Thomas P. Klun , George G. I. Moore , Naiyong Jing , Chuntao Cao , Sharon Wang , Patricia M. Savu , Lan H. Liu , Joan M. Noyola
IPC分类号： B32B27/20 , B32B27/26 , B32B27/28 , B32B27/30 , B32B33/00
CPC分类号： C08F14/18 , C08F259/08 , C08F283/00 , C08L51/003 , C09D151/003 , G02B1/111 , Y10T428/24942 , Y10T428/259 , Y10T428/3154 , Y10T428/31544 , Y10T428/31935 , C08F2/00 , C08L2666/02
摘要： A low refractive index composition that forms a low refractive index layer on an optical display is formed having a co-crosslinked interpenetrating polymer network of a fluoropolymer phase and an acrylate phase. The fluoropolymer phase is preferably formed from fluoropolymers based on THV or FKM and having either a degree of unsaturation and/or containing a reactive cure site monomer in its polymer backbone. The acrylate phase includes a multifunctional acrylate crosslinker, and more preferably includes a perfluoropolyether acrylate crosslinker. The formed low refractive index layer has improved interfacial adhesion to other layers or substrates contained in the optical display. Further, the mechanical strength and scratch resistance of the either of above low refractive index compositions can be further enhanced through the incorporation of surface functionalized inorganic particle into the formed layer.
摘要翻译：形成在光学显示器上形成低折射率层的低折射率组合物，其具有含氟聚合物相和丙烯酸酯相的共交联互穿聚合物网络。含氟聚合物相优选由基于THV或FKM的含氟聚合物形成，并且在其聚合物主链中具有不饱和度和/或含有反应性固化位点单体。丙烯酸酯相包括多官能丙烯酸酯交联剂，更优选包括全氟聚醚丙烯酸酯交联剂。所形成的低折射率层具有改善的与光学显示器中包含的其它层或基底的界面粘合性。此外，通过将表面官能化的无机颗粒并入成形层，可以进一步提高上述低折射率组合物中的任一种的机械强度和耐划伤性。

5. 发明授权

US07332217B2 Article and comprising fluorochemical surface layer 有权
标题翻译：包含含氟表面层的文章
公开(公告)号：US07332217B2
公开(公告)日：2008-02-19
申请号：US11756662
申请日：2007-06-01
申请人： William D. Coggio , Thomas P. Klun , Mark J. Pellerite , George G. I. Moore , Cheryl L. S. Elsbernd , Sharon Wang , Richard S. Buckanin , Christopher B. Walker, Jr. , Naiyong Jing , Zai-Ming Qiu
发明人： William D. Coggio , Thomas P. Klun , Mark J. Pellerite , George G. I. Moore , Cheryl L. S. Elsbernd , Sharon Wang , Richard S. Buckanin , Christopher B. Walker, Jr. , Naiyong Jing , Zai-Ming Qiu
IPC分类号： B32B27/20 , B32B27/26 , B32B27/30
CPC分类号： B32B33/00 , B32B27/18 , B32B27/28 , B32B2307/21 , B32B2307/40 , B32B2457/20 , B32B2457/204 , C08F220/22 , C08F220/24 , Y10T428/10 , Y10T428/1059 , Y10T428/25 , Y10T428/263 , Y10T428/265 , Y10T428/2848 , Y10T428/3154 , Y10T428/31935
摘要： The invention relates to articles such as protective films and displays having a fluorochemical surface layer comprising an antistatic agent and the reaction products of at least one fluoropolyether (meth)acryl compound and at least 50 wt-% of non-fluorinated crosslinking agent(s).
摘要翻译：本发明涉及诸如保护膜和显示器的制品，其具有包含抗静电剂的含氟表面层和至少一种含氟聚醚（甲基）丙烯酸化合物和至少50重量％的非氟化交联剂的反应产物，。

6. 发明授权

US07199197B2 Water- and oil-repellent fluoroacrylates 有权
标题翻译：拒水拒油氟代丙烯酸酯
公开(公告)号：US07199197B2
公开(公告)日：2007-04-03
申请号：US11027604
申请日：2004-12-28
申请人： Gregg A. Caldwell , John C. Clark , David J. Kinning , Alan R. Kirk , Thomas P. Klun , Ramesh C. Kumar , Roger A. Mader , George G. I. Moore , Zai-Ming Qiu , Richard B. Ross
发明人： Gregg A. Caldwell , John C. Clark , David J. Kinning , Alan R. Kirk , Thomas P. Klun , Ramesh C. Kumar , Roger A. Mader , George G. I. Moore , Zai-Ming Qiu , Richard B. Ross
IPC分类号： C08F12/20
CPC分类号： C08F220/38 , C07C271/20 , C07C271/28 , C07C311/09 , Y10T442/2287
摘要： Fluoroacrylates comprise the reaction product of: (a) at least one fluorochemical alcohol represented by the formula: CnF2n+1—X—OH wherein: R=hydrogen or an alkyl group of 1 to 4 carbon atoms, m=2 to 8, Rf=CnF2n+1, y=0 to 6, and q=1 to 8; (b) at least one unbranched symmetric diisocyanate; and (c) at least one hydroxy-terminated alkyl (meth)acrylate or 2-fluoro acrylate monomer having 2 to about 30 carbon atoms in its alkylene portion.
摘要翻译：氟丙烯酸酯包含反应产物

7. 发明授权

US07101618B2 Article comprising fluorochemical surface layer 有权
标题翻译：文章包含含氟表层
公开(公告)号：US07101618B2
公开(公告)日：2006-09-05
申请号：US10841159
申请日：2004-05-07
申请人： William D. Coggio , Thomas P. Klun , Mark J. Pellerite , George G. I. Moore , Cheryl L. S. Elsbernd , Sharon Wang , Richard S. Buckanin , Christopher B. Walker, Jr. , Naiyong Jing , Zai-Ming Qiu
发明人： William D. Coggio , Thomas P. Klun , Mark J. Pellerite , George G. I. Moore , Cheryl L. S. Elsbernd , Sharon Wang , Richard S. Buckanin , Christopher B. Walker, Jr. , Naiyong Jing , Zai-Ming Qiu
IPC分类号： B32B27/28 , B32B33/00
CPC分类号： B32B33/00 , B32B27/18 , B32B27/28 , B32B2307/21 , B32B2307/40 , B32B2457/20 , B32B2457/204 , C08F220/22 , C08F220/24 , Y10T428/10 , Y10T428/1059 , Y10T428/25 , Y10T428/263 , Y10T428/265 , Y10T428/2848 , Y10T428/3154 , Y10T428/31935
摘要： The invention relates to display and protective articles having a fluorochemical surface layer, and methods of making such articles. The invention also relates to fluoropolyether acrylate compositions.
摘要翻译：本发明涉及具有含氟表面层的显示和保护制品，以及制造这种制品的方法。本发明还涉及含氟聚醚丙烯酸酯组合物。

8. 发明授权

US07659351B2 Water- and oil-repellent fluoroacrylates 失效
标题翻译：拒水拒油氟代丙烯酸酯
公开(公告)号：US07659351B2
公开(公告)日：2010-02-09
申请号：US11688074
申请日：2007-03-19
申请人： Gregg A. Caldwell , John C. Clark , David J. Kinning , Alan R. Kirk , Thomas P. Klun , Ramesh C. Kumar , Roger A. Mader , George G I. Moore , Zai-Ming Qiu , Richard B. Ross
发明人： Gregg A. Caldwell , John C. Clark , David J. Kinning , Alan R. Kirk , Thomas P. Klun , Ramesh C. Kumar , Roger A. Mader , George G I. Moore , Zai-Ming Qiu , Richard B. Ross
IPC分类号： C08F12/20
CPC分类号： C08F220/38 , C07C271/20 , C07C271/28 , C07C311/09 , Y10T442/2287
摘要： Fluoroacrylates comprise the reaction product of: (a) at least one fluorochemical alcohol represented by the formula: CnF2n+1—X—OH wherein: n=1 to 4, R=hydrogen or an alkyl group of 1 to 4 carbon atoms, m=2 to 8, Rf=CnF2n+1, y=0 to 6, and q=1 to 8; (b) at least one unbranched symmetric diusocyanate; and (c) at least one hydroxy-terminated alkyl (meth)acrylate or 2-fluoro acrylate monomer having 2 to about 30 carbon atoms in its alkylene portion.
摘要翻译：氟代丙烯酸酯包括以下反应产物：（a）至少一种由式CnF2n + 1-X-OH表示的含氟醇，其中：n = 1-4，R =氢或1-4个碳原子的烷基，m = 2〜8，Rf = CnF2n + 1，y = 0〜6，q = 1〜8; （b）至少一种非支化对称二异氰酸酯; 和（c）至少一个羟基封端的（甲基）丙烯酸烷基酯或其亚烷基部分具有2至约30个碳原子的2-氟丙烯酸酯单体。

9. 发明授权

US07361782B2 Process for preparing fluorochemical monoisocyanates 有权
标题翻译：氟化物单异氰酸酯的制备方法
公开(公告)号：US07361782B2
公开(公告)日：2008-04-22
申请号：US11457037
申请日：2006-07-12
申请人： Thomas P. Klun , Alan R. Kirk , George G. I. Moore , John C. Clark , Zai-Ming Qiu
发明人： Thomas P. Klun , Alan R. Kirk , George G. I. Moore , John C. Clark , Zai-Ming Qiu
IPC分类号： C07C249/00
CPC分类号： C07C303/40 , C07C311/09
摘要： A process for preparing fluorochemical monoisocyanates comprises reacting at least one fluorochemical alcohol represented by the formula CnF2n+1SO2NCH3(CH2)mOH, wherein n=2 to 5, and m=2 to 4, with 4,4′-diphenylmethane diisocyanate (MDI) in a solvent in which the resulting fluorochemical monoisocyanate is not soluble; wherein the molar ratio of fluorochemical alcohol:MDI is from about 1:1 to about 1:2.5.
摘要翻译：一种制备含氟化合物单异氰酸酯的方法包括使至少一种由式C n 2 N 2n + 1 SO 2 NCH 3表示的含氟化合物醇反应，其中n = 2〜5，m = 2〜4，与4,4'-二苯基甲烷二异氰酸酯（MDI）反应，得到（CH 2 CH 2）m OH ）在其中所得氟化异氰酸酯不溶于其中的溶剂中; 其中含氟醇：MDI的摩尔比为约1:1至约1:2.5。

10. 发明授权

US07268197B2 Water- and oil-repellent fluorourethanes and fluoroureas 有权
标题翻译：防水和防油氟聚氨酯和氟脲
公开(公告)号：US07268197B2
公开(公告)日：2007-09-11
申请号：US11275114
申请日：2005-12-12
申请人： George G. I. Moore , Ramesh C. Kumar , Zai-Ming Qiu , John C. Clark , Chetan P. Jariwala , Thomas P. Klun
发明人： George G. I. Moore , Ramesh C. Kumar , Zai-Ming Qiu , John C. Clark , Chetan P. Jariwala , Thomas P. Klun
IPC分类号： C08F12/20
CPC分类号： C08G18/2885 , C08G18/2845 , C08G18/3228 , C08G18/61 , C08G18/6212 , C08G18/6705 , C08G18/71 , C09D175/04 , Y10T428/31551
摘要： A fluorochemical compound comprises the reaction product of: (a) the reaction product of: (i) at least one fluorochemical alcohol represented by the formula: CnF2n+1—X—OH wherein: n=1 to 6, R=hydrogen or an alkyl group of 1 to 4 carbon atoms, m=2 to 8, Rf=CnF2n+1, y=0 to 6, q=1 to 8; and (ii) at least one unbranched symmetric diisocyanate, and (b) at least one co-reactant comprising two or more functional groups that are capable of reacting with an isocyanate group.
摘要翻译：含氟化合物包括以下反应产物：（a）反应产物：（i）至少一种由下式表示的含氟醇：<？in-line-formula description =“In-Line Formulas”end =“lead” 其中：在线式公式描述=“在线公式”end =“tail”→>其中： n = 1至6，R =氢或1至4个碳原子的烷基，m = 2至8，R f = C n N +1，y = 0〜6，q = 1〜8; 和（ii）至少一种非支化的对称二异氰酸酯，和（b）至少一种包含两个或更多个能够与异氰酸酯基团反应的官能团的共反应物。

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