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1. 发明授权

US07199197B2 Water- and oil-repellent fluoroacrylates 有权
标题翻译：拒水拒油氟代丙烯酸酯
公开(公告)号：US07199197B2
公开(公告)日：2007-04-03
申请号：US11027604
申请日：2004-12-28
申请人： Gregg A. Caldwell , John C. Clark , David J. Kinning , Alan R. Kirk , Thomas P. Klun , Ramesh C. Kumar , Roger A. Mader , George G. I. Moore , Zai-Ming Qiu , Richard B. Ross
发明人： Gregg A. Caldwell , John C. Clark , David J. Kinning , Alan R. Kirk , Thomas P. Klun , Ramesh C. Kumar , Roger A. Mader , George G. I. Moore , Zai-Ming Qiu , Richard B. Ross
IPC分类号： C08F12/20
CPC分类号： C08F220/38 , C07C271/20 , C07C271/28 , C07C311/09 , Y10T442/2287
摘要： Fluoroacrylates comprise the reaction product of: (a) at least one fluorochemical alcohol represented by the formula: CnF2n+1—X—OH wherein: R=hydrogen or an alkyl group of 1 to 4 carbon atoms, m=2 to 8, Rf=CnF2n+1, y=0 to 6, and q=1 to 8; (b) at least one unbranched symmetric diisocyanate; and (c) at least one hydroxy-terminated alkyl (meth)acrylate or 2-fluoro acrylate monomer having 2 to about 30 carbon atoms in its alkylene portion.
摘要翻译：氟丙烯酸酯包含反应产物

2. 发明授权

US07659351B2 Water- and oil-repellent fluoroacrylates 失效
标题翻译：拒水拒油氟代丙烯酸酯
公开(公告)号：US07659351B2
公开(公告)日：2010-02-09
申请号：US11688074
申请日：2007-03-19
申请人： Gregg A. Caldwell , John C. Clark , David J. Kinning , Alan R. Kirk , Thomas P. Klun , Ramesh C. Kumar , Roger A. Mader , George G I. Moore , Zai-Ming Qiu , Richard B. Ross
发明人： Gregg A. Caldwell , John C. Clark , David J. Kinning , Alan R. Kirk , Thomas P. Klun , Ramesh C. Kumar , Roger A. Mader , George G I. Moore , Zai-Ming Qiu , Richard B. Ross
IPC分类号： C08F12/20
CPC分类号： C08F220/38 , C07C271/20 , C07C271/28 , C07C311/09 , Y10T442/2287
摘要： Fluoroacrylates comprise the reaction product of: (a) at least one fluorochemical alcohol represented by the formula: CnF2n+1—X—OH wherein: n=1 to 4, R=hydrogen or an alkyl group of 1 to 4 carbon atoms, m=2 to 8, Rf=CnF2n+1, y=0 to 6, and q=1 to 8; (b) at least one unbranched symmetric diusocyanate; and (c) at least one hydroxy-terminated alkyl (meth)acrylate or 2-fluoro acrylate monomer having 2 to about 30 carbon atoms in its alkylene portion.
摘要翻译：氟代丙烯酸酯包括以下反应产物：（a）至少一种由式CnF2n + 1-X-OH表示的含氟醇，其中：n = 1-4，R =氢或1-4个碳原子的烷基，m = 2〜8，Rf = CnF2n + 1，y = 0〜6，q = 1〜8; （b）至少一种非支化对称二异氰酸酯; 和（c）至少一个羟基封端的（甲基）丙烯酸烷基酯或其亚烷基部分具有2至约30个碳原子的2-氟丙烯酸酯单体。

3. 发明授权

US07268197B2 Water- and oil-repellent fluorourethanes and fluoroureas 有权
标题翻译：防水和防油氟聚氨酯和氟脲
公开(公告)号：US07268197B2
公开(公告)日：2007-09-11
申请号：US11275114
申请日：2005-12-12
申请人： George G. I. Moore , Ramesh C. Kumar , Zai-Ming Qiu , John C. Clark , Chetan P. Jariwala , Thomas P. Klun
发明人： George G. I. Moore , Ramesh C. Kumar , Zai-Ming Qiu , John C. Clark , Chetan P. Jariwala , Thomas P. Klun
IPC分类号： C08F12/20
CPC分类号： C08G18/2885 , C08G18/2845 , C08G18/3228 , C08G18/61 , C08G18/6212 , C08G18/6705 , C08G18/71 , C09D175/04 , Y10T428/31551
摘要： A fluorochemical compound comprises the reaction product of: (a) the reaction product of: (i) at least one fluorochemical alcohol represented by the formula: CnF2n+1—X—OH wherein: n=1 to 6, R=hydrogen or an alkyl group of 1 to 4 carbon atoms, m=2 to 8, Rf=CnF2n+1, y=0 to 6, q=1 to 8; and (ii) at least one unbranched symmetric diisocyanate, and (b) at least one co-reactant comprising two or more functional groups that are capable of reacting with an isocyanate group.
摘要翻译：含氟化合物包括以下反应产物：（a）反应产物：（i）至少一种由下式表示的含氟醇：<？in-line-formula description =“In-Line Formulas”end =“lead” 其中：在线式公式描述=“在线公式”end =“tail”→>其中： n = 1至6，R =氢或1至4个碳原子的烷基，m = 2至8，R f = C n N +1，y = 0〜6，q = 1〜8; 和（ii）至少一种非支化的对称二异氰酸酯，和（b）至少一种包含两个或更多个能够与异氰酸酯基团反应的官能团的共反应物。

4. 发明授权

US07361782B2 Process for preparing fluorochemical monoisocyanates 有权
标题翻译：氟化物单异氰酸酯的制备方法
公开(公告)号：US07361782B2
公开(公告)日：2008-04-22
申请号：US11457037
申请日：2006-07-12
申请人： Thomas P. Klun , Alan R. Kirk , George G. I. Moore , John C. Clark , Zai-Ming Qiu
发明人： Thomas P. Klun , Alan R. Kirk , George G. I. Moore , John C. Clark , Zai-Ming Qiu
IPC分类号： C07C249/00
CPC分类号： C07C303/40 , C07C311/09
摘要： A process for preparing fluorochemical monoisocyanates comprises reacting at least one fluorochemical alcohol represented by the formula CnF2n+1SO2NCH3(CH2)mOH, wherein n=2 to 5, and m=2 to 4, with 4,4′-diphenylmethane diisocyanate (MDI) in a solvent in which the resulting fluorochemical monoisocyanate is not soluble; wherein the molar ratio of fluorochemical alcohol:MDI is from about 1:1 to about 1:2.5.
摘要翻译：一种制备含氟化合物单异氰酸酯的方法包括使至少一种由式C n 2 N 2n + 1 SO 2 NCH 3表示的含氟化合物醇反应，其中n = 2〜5，m = 2〜4，与4,4'-二苯基甲烷二异氰酸酯（MDI）反应，得到（CH 2 CH 2）m OH ）在其中所得氟化异氰酸酯不溶于其中的溶剂中; 其中含氟醇：MDI的摩尔比为约1:1至约1:2.5。

5. 发明授权

US07851387B2 Fluoroacrylate-multifunctional acrylate copolymer compositions 有权
标题翻译：氟丙烯酸酯 - 多官能丙烯酸酯共聚物组合物
公开(公告)号：US07851387B2
公开(公告)日：2010-12-14
申请号：US12028589
申请日：2008-02-08
申请人： Zai-Ming Qiu , George G. I. Moore , John C. Clark , Ramesh C. Kumar
发明人： Zai-Ming Qiu , George G. I. Moore , John C. Clark , Ramesh C. Kumar
IPC分类号： B32B27/04
CPC分类号： C08F220/38 , Y10T428/3154 , Y10T442/2311 , Y10T442/232 , Y10T442/2754
摘要： A composition comprises a copolymer comprising repeating units derived from at least one co-reactant comprising two or more acrylate groups and repeating units derived from a fluoroacrylate comprising the reaction product of: (a) at least one fluorochemical alcohol represented by the formula: C4F9—X—OH wherein: R=hydrogen or an alkyl group of 1 to 4 carbon atoms, m=2 to 8, Rf═CnF2n+1, n=1 to 5, y=0 to 6, and q=1 to 8; (b) at least one unbranched symmetric diisocyanate; and (c) at least one hydroxy-terminated alkyl (meth)acrylate or 2-fluoroacrylate monomer having 2 to about 30 carbon atoms in its alkylene portion; wherein the composition is coatable.
摘要翻译：组合物包含共聚物，其包含衍生自至少一种包含两个或更多个丙烯酸酯基团的共反应物的重复单元和衍生自氟代丙烯酸酯的重复单元，所述重复单元包含以下反应产物：（a）至少一种由式C4F9- X-OH其中：R =氢或1至4个碳原子的烷基，m = 2至8，Rf = C n F 2n + 1，n = 1至5，y = 0至6，q = 1至8; （b）至少一种非支化对称二异氰酸酯; 和（c）至少一种羟基封端的（甲基）丙烯酸烷基酯或其亚烷基部分具有2-30个碳原子的2-氟丙烯酸酯单体; 其中所述组合物是可涂覆的。

6. 发明授权

US07345123B2 Fluoroacrylate-multifunctional acrylate copolymer compositions 有权
标题翻译：氟丙烯酸酯 - 多官能丙烯酸酯共聚物组合物
公开(公告)号：US07345123B2
公开(公告)日：2008-03-18
申请号：US11027612
申请日：2004-12-28
申请人： Zai-Ming Qiu , George G. I. Moore , John C. Clark , Ramesh C. Kumar
发明人： Zai-Ming Qiu , George G. I. Moore , John C. Clark , Ramesh C. Kumar
IPC分类号： C08F12/20 , C08G75/04
CPC分类号： C08F220/38 , Y10T428/3154 , Y10T442/2311 , Y10T442/232 , Y10T442/2754
摘要： A composition comprises a copolymer comprising repeating units derived from at least one co-reactant comprising two or more acrylate groups and repeating units derived from a fluoroacrylate comprising the reaction product of: (a) at least one fluorochemical alcohol represented by the formula: C4F9—X—OH wherein: R=hydrogen or an alkyl group of 1 to 4 carbon atoms, m=2 to 8, Rf=CnF2n+1, n=1 to 5, y 32 0 to 6, and q=1 to 8; (b) at least one unbranched symmetric diisocyanate; and (c) at least one hydroxy-terminated alkyl (meth)acrylate or 2-fluoroacrylate monomer having 2 to about 30 carbon atoms in its alkylene portion; wherein the composition is coatable.
摘要翻译：组合物包含共聚物，其包含衍生自至少一种包含两个或更多个丙烯酸酯基团的共反应物的重复单元和衍生自氟代丙烯酸酯的重复单元，所述重复单元包含以下反应产物：（a）至少一种由下式表示的含氟醇： in-line-formula description =“In-line Formulas”end =“lead”？> C 3 -X-OH <？in-line-formula description 其中：R =氢或1至4个碳原子的烷基，m = 2至8，R f = C 1， n = 2n + 1，n = 1〜5，y = 0〜6，q = 1〜8; （b）至少一种非支化对称二异氰酸酯; 和（c）至少一种羟基封端的（甲基）丙烯酸烷基酯或其亚烷基部分具有2-30个碳原子的2-氟丙烯酸酯单体; 其中所述组合物是可涂覆的。

7. 发明授权

US07081545B2 Process for preparing fluorochemical monoisocyanates 失效
标题翻译：氟化物单异氰酸酯的制备方法
公开(公告)号：US07081545B2
公开(公告)日：2006-07-25
申请号：US10751142
申请日：2003-12-31
申请人： Thomas P. Klun , Alan R. Kirk , George G.I. Moore , John C. Clark , Zai-Ming Qiu
发明人： Thomas P. Klun , Alan R. Kirk , George G.I. Moore , John C. Clark , Zai-Ming Qiu
IPC分类号： C07C269/02
CPC分类号： C07C303/40 , C07C311/09
摘要： A process for preparing fluorochemical monoisocyanates comprises reacting at least one fluorochemical alcohol represented by the formula CnF2n+1SO2NCH3(CH2)mOH, wherein n=2 to 5, and m=2 to 4, with 4,4′-diphenylmethane diisocyanate (MDI) in a solvent in which the resulting fluorochemical monoisocyanate is not soluble; wherein the molar ratio of fluorochemical alcohol:MDI is from about 1:1 to about 1:2.5.
摘要翻译：一种制备含氟化合物单异氰酸酯的方法包括使至少一种由式C n 2 N 2n + 1 SO 2 NCH 3表示的含氟化合物醇反应，其中n = 2〜5，m = 2〜4，与4,4'-二苯基甲烷二异氰酸酯（MDI）反应，得到（CH 2 CH 2）m OH ）在其中所得氟化异氰酸酯不溶于其中的溶剂中; 其中含氟醇：MDI的摩尔比为约1:1至约1:2.5。

8. 发明授权

US07750093B2 Polyurethanes derived from oligomeric fluoroacrylates 失效
标题翻译：衍生自低聚氟代丙烯酸酯的聚氨酯
公开(公告)号：US07750093B2
公开(公告)日：2010-07-06
申请号：US11478219
申请日：2006-06-29
申请人： Cheryl L. S. Elsbernd , Frans A. Audenaert , John C. Clark , Chetan P. Jariwala , George G. I. Moore , Zai-Ming Qiu
发明人： Cheryl L. S. Elsbernd , Frans A. Audenaert , John C. Clark , Chetan P. Jariwala , George G. I. Moore , Zai-Ming Qiu
IPC分类号： C08F283/04 , C08G18/28
CPC分类号： C09D175/04 , C08G18/2825 , C08G18/2885 , C08G18/6279 , C08G18/672 , C08G18/792 , C08G18/8077 , C14C11/006
摘要： The present invention relates to fluorochemical polyurethane compounds, a method for their preparation, a method of application, and compositions comprising that fluorochemical polyurethane compound. The compound and the composition comprising that compound are suitable to impart durable oil- and water-repellency to substrates.
摘要翻译：本发明涉及含氟聚氨酯化合物，其制备方法，应用方法和包含该含氟聚氨酯化合物的组合物。该化合物和包含该化合物的组合物适用于赋予基材持久的耐油和拒水性。

9. 发明授权

US07291688B2 Fluoroacrylate-mercaptofunctional copolymers 有权
标题翻译：氟丙烯酸酯 - 巯基官能共聚物
公开(公告)号：US07291688B2
公开(公告)日：2007-11-06
申请号：US11027605
申请日：2004-12-28
申请人： Zai-Ming Qiu , John C. Clark , Ramesh C. Kumar
发明人： Zai-Ming Qiu , John C. Clark , Ramesh C. Kumar
IPC分类号： C08F12/20 , C08G75/04
CPC分类号： C08F220/38
摘要： A copolymer comprises repeating units derived from at least one co-reactant comprising two or more mercapto functional groups, and repeating units derived from a fluoroacrylate comprising the reaction product of: (a) at least one fluorochemical alcohol represented by the formula: C4F9—X—OH wherein: R=hydrogen or an alkyl group of 1 to 4 carbon atoms, m=2 to 8, Rf=CnF2n+1, n=1 to 5, y=0 to 6, and q=1 to 8; (b) at least one unbranched symmetric diisocyanate; and (c) at least one hydroxy-terminated alkyl (meth)acrylate or 2-fluoroacrylate monomer having 2 to about 30 carbon atoms in its alkylene portion.
摘要翻译：共聚物包含衍生自至少一种包含两个或多个巯基官能团的共反应物的重复单元和衍生自氟代丙烯酸酯的重复单元，该重复单元包含以下反应产物：（a）至少一种由下式表示的含氟醇： -line-formula description =“In-line Formulas”end =“lead”？> C 3 -X-OH <？in-line-formula description = “直链式”末端=“尾”→其中：R =氢或1至4个碳原子的烷基，m = 2至8，R f = C n n = 1〜5，y = 0〜6，q = 1〜8; （b）至少一种非支化的对称二异氰酸酯; 和（c）至少一种羟基封端的（甲基）丙烯酸烷基酯或其亚烷基部分具有2至约30个碳原子的2-氟丙烯酸酯单体。

10. 发明授权

US07666964B2 Fluoroacrylate-mercaptofunctional copolymers 有权
标题翻译：氟丙烯酸酯 - 巯基官能共聚物
公开(公告)号：US07666964B2
公开(公告)日：2010-02-23
申请号：US11859295
申请日：2007-09-21
申请人： Zai-Ming Qiu , John C. Clark , Ramesh C. Kumar
发明人： Zai-Ming Qiu , John C. Clark , Ramesh C. Kumar
IPC分类号： C08F12/30 , C08G18/00 , C08L27/12 , C08C261/00
CPC分类号： C08F220/38
摘要： A copolymer comprises repeating units derived from at least one co-reactant comprising two or more mercapto functional groups, and repeating units derived from a fluoroacrylate comprising the reaction product of: (a) at least one fluorochemical alcohol represented by the formula: C4F9—X—OH wherein: R=hydrogen or an alkyl group of 1 to 4 carbon atoms, m=2 to 8, Rf=CnF2n+1, n=1 to 5, y=0 to 6, and q=1 to 8; (b) at least one unbranched symmetric diisocyanate; and (c) at least one hydroxy-terminated alkyl (meth)acrylate or 2-fluoroacrylate monomer having 2 to about 30 carbon atoms in its alkylene portion.
摘要翻译：共聚物包含衍生自至少一种包含两个或多个巯基官能团的共反应物的重复单元和衍生自氟代丙烯酸酯的重复单元，其包含以下反应产物：（a）至少一种由式C4F9-X表示的含氟醇 -OH其中：R =氢或1至4个碳原子的烷基，m = 2至8，R f = C n F 2n + 1，n = 1至5，y = 0至6，q = 1至8; （b）至少一种非支化对称二异氰酸酯; 和（c）至少一种羟基封端的（甲基）丙烯酸烷基酯或其亚烷基部分具有2至约30个碳原子的2-氟丙烯酸酯单体。

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