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1. 发明授权

US06696607B2 Use of phenethyl acrylamides, novel phenethyl acrylamides, method for the production thereof and agents containing the same 失效
标题翻译：使用苯乙基丙烯酰胺，新型苯乙基丙烯酰胺，其制备方法和含有它们的试剂
公开(公告)号：US06696607B2
公开(公告)日：2004-02-24
申请号：US10297287
申请日：2002-12-04
申请人： Wassilios Grammenos , Hubert Sauter , Oliver Cullmann , Markus Gewehr , Bernd Müller , Jordi Tormo i Blasco , Norbert Götz , Thorsten Volk , Gisela Lorenz , Eberhard Ammermann , Reinhard Stierl , Siegfried Strathmann
发明人： Wassilios Grammenos , Hubert Sauter , Oliver Cullmann , Markus Gewehr , Bernd Müller , Jordi Tormo i Blasco , Norbert Götz , Thorsten Volk , Gisela Lorenz , Eberhard Ammermann , Reinhard Stierl , Siegfried Strathmann
IPC分类号： C07C23309
CPC分类号： A01N37/36 , A01N37/18 , A01N37/38 , C07C231/02 , C07C233/22
摘要： Use of phenethylacrylamides of the formula I: in which the substituents have the following meanings: X is halogen, alkyl, haloalkyl, alkoxy, haloalkoxy and —O—C(Ra,Rb)—C≡C—R6; Ra,Rb and Rc have the meanings given in the description; m,n independently of one another are 1 to 4, it being possible for the radicals X or Y to be different if m or n is greater than 1; Y is halogen, nitro, cyano, alkyl, CF3, alkoxy and phenyl; R1,R2 independently of one another are hydrogen, halogen, alkyl, alkoxy, haloalkoxy and CF3; R3,R4,R5,R6 independently of one another are hydrogen, halogen, alkyl, alkoxy, or R3 and R4 together form a cyclopropyl ring, it being possible for the C—R5— and C—R6 bonds can be in the E- or Z-position relative to each other; for controlling phytopathogenic fungal pests, novel phenethylacrylamides, their preparation, and compositions comprising them.
摘要翻译：使用式I的苯乙基丙烯酰胺：其中取代基具有以下含义：X是卤素，烷基，卤代烷基，烷氧基，卤代烷氧基和-OC（R a，R b）-C = CR 6; R a，R b和R c具有说明书中给出的含义; m，n彼此独立地为1至4，如果m或n可以使基团X或Y不同大于1; Y是卤素，硝基，氰基，烷基，CF 3，烷氧基和苯基; R 1，R 2彼此独立地是氢，卤素，烷基，烷氧基，卤代烷氧基和CF 3; R 3 R 4，R 5，R 6彼此独立地是氢，卤素，烷基，烷氧基或R 3和R 4一起形成环丙基环，其中CR <5> - 和CR 6键可以相对于彼此位于E-或Z-位;用于控制植物病原性真菌害虫，新型苯乙基丙烯酰胺，它们的制备和包含它们的组合物。

2. 发明授权

US06469195B1 2-phenoxyphenylacetic acid derivatives, method and intermediate products for the production thereof, their use, and agents containing the same for combating fungicidal pests 失效
标题翻译： 2-苯氧基苯乙酸衍生物，其生产方法和中间产物，其用途和含有它们的用于防治杀真菌害虫的试剂
公开(公告)号：US06469195B1
公开(公告)日：2002-10-22
申请号：US09830365
申请日：2001-04-25
申请人： Wassilios Grammenos , Hubert Sauter , Andreas Gypser , Oliver Cullmann , Markus Gewehr , Bernd Müller , Arne Ptock , Norbert Götz , Roland Götz , Thorsten Volk , Eberhard Ammermann , Thomas Grote , Gisela Lorenz , Siegfried Strathmann
发明人： Wassilios Grammenos , Hubert Sauter , Andreas Gypser , Oliver Cullmann , Markus Gewehr , Bernd Müller , Arne Ptock , Norbert Götz , Roland Götz , Thorsten Volk , Eberhard Ammermann , Thomas Grote , Gisela Lorenz , Siegfried Strathmann
IPC分类号： C07C22900
CPC分类号： C07C251/48 , C07C69/738
摘要： 2-Phenoxyphenylacetic acid derivatives of the formula I where the substituents and the index have the following meanings: A is where R1 is halogen, C1-C4-alkyl, C1-C4-alkoxy, CF3, C1-C4-haloalkoxy, formyl, C(═O)NRaRb or C(Ra)═NORb; Ra is hydrogen or C1-C4-alkyl; Rb is C1-C4-alkyl; n is 1, 2, 3 or 4, where the groups R1 may be different if n is not 1; R2 is halogen, CH3 or CF3; m is 0 or 1; and X is OCH3 or NHCH3; processes and intermediates for preparing the compounds I and the use of the compounds I for controlling harmful fungi are described.
摘要翻译：式I的2-苯氧基苯基乙酸衍生物，其中取代基和指数具有以下含义：A是其中R 1是卤素，C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，CF 3，C 1 -C 4 - 卤代烷氧基，甲酰基，C（= O）NR a R b或C（R a）= NOR b; R a是氢或C 1 -C 4烷基; R b是C 1 -C 4 - 烷基; n是1,2,3或4，其中如果n不是 1; R2是卤素，CH3或CF3; m是0或1; 和X是OCH 3或NHCH 3;描述了制备化合物I的方法和中间体以及用于控制有害真菌的化合物I的用途。

3. 发明授权

US06897322B2 Method of producing 1-alkyl-3-aryl-5-difluoromethoxy-1H-pyrazoles 失效
标题翻译： 1-烷基-3-芳基-5-二氟甲氧基-1H-吡唑的制备方法
公开(公告)号：US06897322B2
公开(公告)日：2005-05-24
申请号：US10250503
申请日：2002-01-15
申请人： Thorsten Volk , Michael Puhl , Cyrill Zagar , Rene Lochtman , Norbert Götz , Gerhard Hamprecht
发明人： Thorsten Volk , Michael Puhl , Cyrill Zagar , Rene Lochtman , Norbert Götz , Gerhard Hamprecht
IPC分类号： C07D231/20 , C07D231/14
CPC分类号： C07D231/20
摘要： The invention relates to a method of preparing 1-alkyl-3-aryl-5-difluoromethoxy-1H-pyrazoles of the formula (I), wherein aryl represents a mono- or polysubstituted phenyl ring, and R1 represents C1-C4 alkyl. The inventive method is characterized by reacting, in a first reaction step, a β-ketoester of the general formula (II) with hydrazine and by successively reacting the reaction product obtained with chlorodifluoromethane and a compound R1-L, wherein R1 has the meanings indicated above and L represents the leaving group of a nucleophilic displacement reaction.
摘要翻译：本发明涉及制备式（I）的1-烷基-3-芳基-5-二氟甲氧基-1H-吡唑的方法，其中芳基表示单取代或多取代的苯环，R 1 >表示C 1 -C 4烷基。本发明的方法的特征在于在第一反应步骤中使通式（II）的β-酮酯与肼反应，并将所得反应产物与氯二氟甲烷和化合物R 1 - L，其中R 1具有上述含义，L表示亲核置换反应的离去基团。

4. 发明授权

US06888003B2 Method for producing 7-(pyrazole-3-yl) benzoxazoles 失效
标题翻译： 7-（吡唑-3-基）苯并恶唑的制备方法
公开(公告)号：US06888003B2
公开(公告)日：2005-05-03
申请号：US10221206
申请日：2001-03-15
申请人： Cyrill Zagar , Robert Reinhard , Michael Puhl , Thorsten Volk , Norbert Götz , Gerhard Hamprecht , Olaf Menke , Ingo Sagasser
发明人： Cyrill Zagar , Robert Reinhard , Michael Puhl , Thorsten Volk , Norbert Götz , Gerhard Hamprecht , Olaf Menke , Ingo Sagasser
IPC分类号： C07D231/12 , A01N43/56 , A01N43/76 , C07B61/00 , C07D231/16 , C07D231/18 , C07D413/04 , C07D413/14 , C07D498/00
CPC分类号： C07D413/04 , A01N43/56
摘要： A process for preparing 7-(pyrazol-3-yl)benzoxazoles of the formula I in which the variables R1-R6 are as defined in claim 1, which process is characterized in that a 2-halo-3-(pyrazol-3-yl)anilide of the formula II, in which X is bromine or iodine is reacted with a base in the presence of a transition metal compound of subgroup VIIa, VIIIa or Ib of the Periodic Table of the Elements, is disclosed.
摘要翻译：制备其中变量R 1〜6的定义的式I的7-（吡唑-3-基）苯并恶唑的方法如权利要求1所定义，该方法其特征在于式Ⅱ的2-卤代-3-（吡唑-3-基）酰苯胺，其中X是溴或碘，在Ⅶa族，Ⅷa族或Ⅷa族过渡金属化合物存在下与碱反应公开了元素周期表的Ib。

5. 发明授权

US06815563B2 Method for producing bicyclic 1,3-diketones 失效
标题翻译：双环1,3-二酮的制备方法
公开(公告)号：US06815563B2
公开(公告)日：2004-11-09
申请号：US10332034
申请日：2003-01-06
申请人： Klaus Langemann , Ulf Misslitz , Ernst Baumann , Wolfgang von Deyn , Steffen Kudis , Thorsten Volk , Guido Mayer
发明人： Klaus Langemann , Ulf Misslitz , Ernst Baumann , Wolfgang von Deyn , Steffen Kudis , Thorsten Volk , Guido Mayer
IPC分类号： A01N4358
CPC分类号： C07C255/47 , C07C17/00 , C07C45/27 , C07C45/29 , C07C45/298 , C07C45/673 , C07C49/433 , C07C2602/44 , C07C23/30 , C07C49/693
摘要： A process for preparing bicyclic 1,3-diketones of the formula I where R1, R2, R3 and R4 are hydrogen, C1-C4-alkyl, C1-C4-alkoxy-carbonyl, halogen, cyano, nitro, C1-C4-alkylthio, C1-C4-alkylsulfenyl or C1-C4-alkylsulfonyl and Z is C1-C4-alkylene, O, S, N—R5 where R5 is C1-C4-alkyl or C1-C4-alkylcarbonyl, which comprises a) reacting a bicyclic olefin of the formula II with haloform in the presence of a base to give the ring-expanded product of the formula III where R1-R4 and Z are as defined above and X is halogen; b) hydrolyzing the allylic halogen of the compound of the formula III to the allyl alcohol of the formula IV c) oxidizing the allyl alcohol of the formula IV to the unsaturated ketone of the formula V d) reacting the ketone of the formula V with a nucleophilic ion Y− which stabilizes a negative charge to give the ketone of the formula VI e) hydrolyzing the ketone of the formula VI to the bicyclic 1,3-diketone of the formula I, novel intermediates and novel processes for preparing these intermediates are described.
摘要翻译：制备式I其中R 1，R 2，R 3和R 4的双环1,3-二酮的方法是氢，C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基 - 羰基，卤素氰基，硝基，C 1 -C 4 - 烷硫基，C 1 -C 4烷基硫基或C 1 -C 4 - 烷基磺酰基，Z是C 1 -C 4 - 亚烷基，O，S，NR 5，其中R 5是C 1 -C 4烷基或C 1 -C4 - 烷基羰基，其包括a）在碱存在下使式II的双环烯烃与卤代甲基反应，得到式III的环扩展产物，其中R 1 -R 4和Z如上所定义，X和X 将式III的化合物的烯丙基卤水解成式IVc的烯丙醇，将式Ⅳ的烯丙醇氧化为式ⅤⅤ的不饱和酮）使式Ⅴ的酮与使负电荷稳定以得到式VIe的酮）将式VI的酮水解成式I的双环1,3-二酮的新型中间体和新方法描述这些中间体。

6. 发明授权

US06541423B1 4-(3′,4′-heterocyclyl benzoyl) pyrazoles as herbicidal agents 失效
标题翻译： 4-（3'，4'-杂环基苯甲酰基）吡唑作为除草剂
公开(公告)号：US06541423B1
公开(公告)日：2003-04-01
申请号：US09959636
申请日：2001-11-01
申请人： Guido Mayer , Ernst Baumann , Wolfgang von Deyn , Steffen Kudis , Klaus Langemann , Ulf Misslitz , Ulf Neidlein , Matthias Witschel , Michael Rack , Thorsten Volk , Martina Otten , Karl-Otto Westphalen , Helmut Walter
发明人： Guido Mayer , Ernst Baumann , Wolfgang von Deyn , Steffen Kudis , Klaus Langemann , Ulf Misslitz , Ulf Neidlein , Matthias Witschel , Michael Rack , Thorsten Volk , Martina Otten , Karl-Otto Westphalen , Helmut Walter
IPC分类号： C07D41706
CPC分类号： C07D403/06 , A01N43/74 , C07D413/06 , C07D417/06
摘要： The invention relates to pyrazolyl derivatives of benzo-condensated, unsaturated 5-membered nitrogen heterocycles of the general formula (I), wherein X represents N or a group C—R3; Y is O, S, SO, SO2 or NR4 or X—Y is S═N, and wherein X means sulfur, and the variables R1, R2 and Pz have the meanings indicated in claim 1. The invention, further relates to a method of producing said compounds, to agents that contain them and to their use as herbicidal agents.
摘要翻译：本发明涉及通式（I）的苯并缩合的不饱和5元氮杂环的吡唑基衍生物，其中X代表N或C-R3基团; Y是O，S，SO，SO 2或NR 4或XY是S = N，并且其中X表示硫，并且变量R1，R2和Pz具有权利要求1中所示的含义。本发明还涉及一种生产所述化合物，含有它们的试剂并用作除草剂。

7. 发明授权

US06908884B2 Benzazolonylcarbonylcyclohexenones and their use as herbicides 失效
标题翻译：苯并唑烷基羰基环己烯酮及其作为除草剂的用途
公开(公告)号：US06908884B2
公开(公告)日：2005-06-21
申请号：US10433013
申请日：2001-12-10
申请人： Guido Mayer , Ulf Misslitz , Ernst Baumann , Wolfgang von Deyn , Steffen Kudis , Michael Hofmann , Thorsten Volk , Matthias Witschel , Cyrill Zagar , Andreas Landes , Klaus Langemann
发明人： Guido Mayer , Ulf Misslitz , Ernst Baumann , Wolfgang von Deyn , Steffen Kudis , Michael Hofmann , Thorsten Volk , Matthias Witschel , Cyrill Zagar , Andreas Landes , Klaus Langemann
IPC分类号： A01N43/74 , A01N43/76 , A01N43/78 , C07D263/58 , C07D277/68 , C07D417/06 , C07D521/00 , C07D261/18 , C07D271/00
CPC分类号： C07D263/58 , A01N43/74 , C07D231/12 , C07D233/56 , C07D249/08 , C07D277/68 , C07D417/06
摘要： Cyclohexenone derivatives of benzazolones of the formula I where the variables R1, R2, R3, A and Hex are as defined in claim 1, and their salts, and their use for controlling harmful plants, are described.
摘要翻译：其中变量R 1，R 2，R 3，A和Hex的式I的苯并唑酮的环己烯酮衍生物如权利要求1中所定义，及其盐，及其用于控制有害植物的用途。

8. 发明授权

US06613717B1 Phosphoric benzoyl derivatives and their use as herbicides 失效
标题翻译：磷酰苯甲酰衍生物及其作为除草剂的用途
公开(公告)号：US06613717B1
公开(公告)日：2003-09-02
申请号：US09959510
申请日：2001-10-29
申请人： Klaus Langemann , Thorsten Volk , Ernst Baumann , Wolfgang von Deyn , Steffen Kudis , Guido Mayer , Ulf Misslitz , Ulf Neidlein , Matthias Witschel , Martina Otten , Karl-Otto Westphalen , Helmut Walter
发明人： Klaus Langemann , Thorsten Volk , Ernst Baumann , Wolfgang von Deyn , Steffen Kudis , Guido Mayer , Ulf Misslitz , Ulf Neidlein , Matthias Witschel , Martina Otten , Karl-Otto Westphalen , Helmut Walter
IPC分类号： A01N5726
CPC分类号： C07F9/65685 , A01N57/22 , A01N57/24 , C07F9/4021 , C07F9/4025 , C07F9/4419 , C07F9/5325 , C07F9/5329 , C07F9/572 , C07F9/65031 , C07F9/653 , C07F9/657181 , C07F9/65785
摘要： Phosphorus-containing benzoyl derivatives of the formula I where: P(═X)R1R2X is an organic phosphorus radical; R3 is hydrogen, nitro, cyano, halogen, unsub. or sub. alkyl, alkylcarbonyl, alkoxycarbonyl, unsub. or sub. alkoxy, unsub. or sub. alkylthio, unsub. or sub. alkylsulfinyl, unsub. or sub. alkylsulfonyl, unsub. or sub. aminosulfonyl, unsub. or sub. amino, P(═X)R1R2, unsub. or sub. phenyl or unsub. or sub. heterocyclyl; R4 is nitro, cyano, halogen, alkyl, alkoxy, alkylthio, alkylsulfinyl or alkylsulfonyl; l is 0, 1 or 2; Q is unsub. or sub. 1-hydroxy-3-oxocyclohex-1-en-2-yl, unsub. or sub. 5-hydroxypyrazol-4-yl, unsub. or sub. isoxazol-4-yl or unsub. or sub. 2-cyano-1-oxoeth-2-yl; and their agriculturally useful salts; processes and intermediates for preparing the phosphorus-containing benzoyl derivatives; compositions comprising them and the use of these derivatives or the compositions comprising them for controlling undesirable plants are described.
摘要翻译：含有式I的苯甲酰基衍生物其中：P（= X）R 1 R 2 X是有机磷基; R 3是氢，硝基，氰基，卤素，未取代的。或子。烷基，烷基羰基，烷氧基羰基，未取代的。或子。烷氧基或子。烷硫基或子。烷基亚磺酰基或子。烷基磺酰基或子氨基磺酰基或子。氨基，P（= X）R 1 R 2，未取代。或子。苯基或未取代的。或子。杂环基; R 4是硝基，氰基，卤素，烷基，烷氧基，烷硫基，烷基亚磺酰基或烷基磺酰基; l是0,1或2; Q是未取代的。或子。 1-羟基-3-氧代环己-1-烯-2-基，或子。 5-羟基吡唑-4-基，或子。异恶唑-4-基或未取代的。或子。 2-氰基-1-氧代乙基-2-基;及其农业上可用的盐;制备含磷苯甲酰基衍生物的方法和中间体; 描述了包含它们的组合物以及这些衍生物或包含它们的组合物用于防治不期望的植物的用途。

9. 发明授权

US06589915B1 Benzohetero cyclylcyclo hexenones and their use as herbicides 失效
标题翻译：苯并环基环己烯酮及其作为除草剂的用途
公开(公告)号：US06589915B1
公开(公告)日：2003-07-08
申请号：US09959801
申请日：2001-11-07
申请人： Guido Mayer , Ernst Baumann , Wolfgang von Deyn , Steffen Kudis , Klaus Langemann , Ulf Misslitz , Ulf Neidlein , Matthias Witschel , Michael Rack , Thorsten Volk , Martina Otten , Karl-Otto Westphalen , Helmut Walter
发明人： Guido Mayer , Ernst Baumann , Wolfgang von Deyn , Steffen Kudis , Klaus Langemann , Ulf Misslitz , Ulf Neidlein , Matthias Witschel , Michael Rack , Thorsten Volk , Martina Otten , Karl-Otto Westphalen , Helmut Walter
IPC分类号： A01N4378
CPC分类号： C07D263/56 , A01N43/74 , C07D249/18 , C07D263/58 , C07D277/62 , C07D277/64 , C07D277/66 , C07D277/68 , C07D277/74 , C07D285/14
摘要： The invention relates to cyclohexenone derivatives of benzo-condensed, unsaturated 5-ring nitrogen heterocycles of general formula (I) wherein X represents N or a group C—R3, Y represents O, S, SO, SO2 or NR4 or X—Y represent S═N and X represents sulfur, and the variables R1, R2 and Hex have the meanings given in claim 1. The invention also relates to a method for producing these compounds, to agents containing these compounds, and to their use as herbicides.
摘要翻译：本发明涉及通式（I）的苯并稠合的不饱和5-环氮杂环的环己烯酮衍生物，其中X表示N或C-R 3，Y表示O，S，SO，SO 2或NR 4或XY表示S = N和X表示硫，并且变量R1，R2和Hex具有权利要求1中给出的含义。本发明还涉及制备这些化合物的方法，含有这些化合物的试剂及其作为除草剂的用途。

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