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1. 发明授权

US4876275A 3,4-dihydro-2H-pyrans useful as pesticides 失效
标题翻译： 3,4-二氢-2H-吡喃可用作农药
公开(公告)号：US4876275A
公开(公告)日：1989-10-24
申请号：US176700
申请日：1988-04-01
申请人： Walter Himmele , Hans Theobald , Franz Merger , Ernst Hofmann , Christoph Kuenast , Peter Hofmeister
发明人： Walter Himmele , Hans Theobald , Franz Merger , Ernst Hofmann , Christoph Kuenast , Peter Hofmeister
IPC分类号： A01N43/16 , A01N43/28 , A01N43/30 , A01N43/32 , C07D309/30 , C07D407/12
CPC分类号： C07D407/12 , A01N43/16 , A01N43/28 , A01N43/30 , A01N43/32 , C07D309/30
摘要： 3,4-dihydro-2H-pyrans of the formula I ##STR1## where R.sup.1 is C.sub.4 -C.sub.20 -alkyl, C.sub.4 -C.sub.20 -alkoxyalkyl, aryl or C.sub.7 -C.sub.20 -arylalkyl, or is aryl or C.sub.7 -C.sub.20 -arylalkyl which bears from one to three substituents selected from the group consisting of halogen, C.sub.1 -C.sub.8 -alkyl, C.sub.1 -C.sub.8 -haloalkyl, C.sub.1 -C.sub.8 -alkoxy or C.sub.1 -C.sub.8 -haloalkoxy, R.sup.2 is hydrogen or C.sub.1 -C.sub.4 -alkyl, R.sup.3 is aryl, or aryl bearing from one to three substituents selected from the group consisting of halogen, C.sub.1 -C.sub.8 -alkyl, C.sub.1 -C.sub.8 -haloalkyl, C.sub.1 -C.sub.8 -alkoxy or C.sub.1 -C.sub.8 -haloalkoxy, or the radical ##STR2## where R.sup.4, R.sup.5 and R.sup.6 are hydrogen or C.sub.1 -C.sub.4 -alkyl, R.sup.7 is phenyl or benzoyl, or phenyl or benzoyl bearing from one to three substituents selected from the group consisting of halogen, C.sub.1 -C.sub.8 -alkyl, C.sub.1 -C.sub.8 -haloalkyl, C.sub.1 -C.sub.8 -alkoxy and C.sub.1 -C.sub.8 -haloalkoxy, or a five- or six-membered heterocycle containing one or two oxygen atoms and which is either unsubstituted or substituted by one to three C.sub.1 -C.sub.8 -alkyl groups or one C.sub.3 -C.sub.6 -spirocycloalkyl, and l, m and n are 0 or 1, and their use for combating pests.
摘要翻译：其中R 1是C 4 -C 20烷基，C 4 -C 20烷氧基烷基，芳基或C 7 -C 20芳基烷基，或者是芳基或C 7 -C 20 - 芳基烷基， 1至3个选自卤素，C 1 -C 8 - 烷基，C 1 -C 8 - 卤代烷基，C 1 -C 8 - 烷氧基或C 1 -C 8 - 卤代烷氧基的取代基的芳基烷基，R 2为氢或C 1 -C 4烷基， R3是芳基或带有1至3个选自卤素，C 1 -C 8 - 烷基，C 1 -C 8 - 卤代烷基，C 1 -C 8 - 烷氧基或C 1 -C 8 - 卤代烷氧基的取代基的芳基或基团< 其中R 4，R 5和R 6是氢或C 1 -C 4 - 烷基，R 7是苯基或苯甲酰基，或苯基或苯甲酰基，其带有一至三个选自卤素，C 1 -C 8 - 烷基，C 1 -C 8 - ，C 1 -C 8 - 烷氧基和C 1 -C 8 - 卤代烷氧基，或含有一个或两个氧原子的五元或六元杂环，其未被取代或被一至三个C 1 -C 8烷基或一个C 3 -C 6 - 螺环烷基，l，m和n为0或1，用于防治害虫。

2. 发明授权

US3975400A Method of continuously producing .gamma.-butyrolactams 失效
标题翻译：连续生产{65-丁内酰胺的方法
公开(公告)号：US3975400A
公开(公告)日：1976-08-17
申请号：US334398
申请日：1973-02-21
申请人： Walter Himmele , Ernst Hofmann , Herwig Hoffmann , Reinhold Plass
发明人： Walter Himmele , Ernst Hofmann , Herwig Hoffmann , Reinhold Plass
IPC分类号： C07D207/26 , C07D207/267
CPC分类号： C07D207/267
摘要： Method of producing .gamma.-butyrolactams by reacting .gamma.-butyrolactones with ammonia in the presence or absence of water at elevated temperatures and pressures. The reaction is carried out continuously at temperatures ranging from 180.degree. to 340.degree.C whilst maintaining pressures which are at least 10 percent higher than the pressure equal to the sum of the partial pressures of the reactants at the temperature used. .gamma.-Butyrolactams are valuable intermediates, for example in the manufacture of polymers, pharmaceuticals and solvents.
摘要翻译：在高温和高压下，在存在或不存在水的情况下，使γ-丁内酯与氨反应制备γ-丁内酰胺的方法。反应在180℃至340℃的温度下连续进行，同时保持比在所用温度下等于反应物分压之和的压力至少高10％的压力。 γ-丁内酰胺是有价值的中间体，例如在聚合物，药物和溶剂的制备中。

3. 发明授权

US4954633A Isoxazolines as intermediates to furans 失效
标题翻译：异恶唑啉作为呋喃的中间体
公开(公告)号：US4954633A
公开(公告)日：1990-09-04
申请号：US384910
申请日：1989-07-25
申请人： Hans Theobald , Rainer Becker , Walter Himmele
发明人： Hans Theobald , Rainer Becker , Walter Himmele
IPC分类号： C07C45/56 , C07D261/04 , C07D307/42 , C07D307/68 , C07F9/653
CPC分类号： C07D307/42 , C07C45/56 , C07D261/04 , C07D307/68 , C07F9/653 , Y02P20/55
摘要： Isoxazolines of the general formula II ##STR1## in which R.sup.1, R.sup.2, R.sup.3 and R.sup.4 are each unsubstituted or halogen-, haloalkyl-, alkoxy-, haloalkoxy-, nitro-, cyano-, dialkylphosphonyl- or alkoxycarbonyl-substituted alkyl, aryl, aralkyl, alkoxycarbonyl or dialkoxyphosphonyl, R.sup.2 and R.sup.4 are each also hydrogen and R.sup.3 is also hydroxyalkyl which is unblocked or blocked by a detachable protective group or is haloalkyl, X is hydrogen or a detachable protective group, are used to prepare furans.
摘要翻译：其中R 1，R 2，R 3和R 4各自是未取代的或卤素，卤代烷基 - ，烷氧基 - ，卤代烷氧基 - ，硝基 - ，氰基 - ，二烷基膦基 - 或烷氧基羰基取代的烷基的异恶唑啉芳基，芳烷基，烷氧基羰基或二烷氧基膦酰基，R2和R4各自也是氢，R3也是被可分离的保护基团阻断或封闭的羟基烷基，或者是卤代烷基，X是氢或可分离的保护基，用于制备呋喃。

4. 发明授权

US4870100A Pyrethroids and their use for controlling pests 失效
标题翻译：拟除虫菊酯及其用于防治害虫的用途
公开(公告)号：US4870100A
公开(公告)日：1989-09-26
申请号：US940649
申请日：1986-12-11
申请人： Bernd Wolf , Hans Theobald , Rainer Becker , Norbert Goetz , Walter Himmele , Rudolf Kropp
发明人： Bernd Wolf , Hans Theobald , Rainer Becker , Norbert Goetz , Walter Himmele , Rudolf Kropp
IPC分类号： A01N43/08 , A01N43/10 , A01N53/00 , A01N53/04 , A01N53/08 , C07C249/00 , C07D261/04 , C07D307/40 , C07D307/42 , C07D307/45 , C07D307/46 , C07D307/54 , C07D409/12
CPC分类号： C07D307/42 , A01N43/08 , A01N53/00 , C07D261/04 , C07D307/46
摘要： 2-benzylfuryl compounds of the general formula I ##STR1## where R.sup.1, R.sup.2 and R.sup.3 are identical or different substituents and are each hydrogen, halogen, alkyl, haloalkyl, alkoxy, haloalkoxy, haloalkylthio, alkenyl or haloalkenyl, each of not more than 6 carbon atoms, n being 1, 2 or 3 where R.sup.3 is not hydrogen, and R.sup.4 and R.sup.5 are each hydrogen or alkyl of not more than 6 carbon atoms, R is --CHO or CHR.sup.6 OA, R.sup.6 is hydrogen, cyano, alkyl, alkenyl, haloalkenyl or alkynyl, each of not more than 6 carbon atoms, or carboxamide, and A is either hydrogen or a radical of an acid typical for pyrethroids, with the proviso that R.sup.2 is not hydrogen, chlorine, bromine, methyl or methoxy when R.sup.1 is hydrogen or methyl and R.sup.3 and A are each hydrogen, and furthermore with the proviso that R.sup.1 and R.sup.2 are not methyl when A is a radical of tetramethylcyclopropanecarboxylic acid, and finally with the proviso that R.sup.2 is not methyl, chlorine, bromine or methoxy and R.sup.1 and R.sup.3 are not hydrogen when A is a radical of chrysanthemumic acid, their preparation and their use as intermediates for crop protection agents or as crop protection agents.
摘要翻译：通式I（I）的2-苄基呋喃基化合物，其中R 1，R 2和R 3是相同或不同的取代基，并且各自为氢，卤素，烷基，卤代烷基，烷氧基，卤代烷氧基，卤代烷硫基，烯基或卤代烯基，大于6个碳原子，n为1,2或3，其中R3不是氢，R4和R5各自为氢或不超过6个碳原子的烷基，R为-CHO或CHR6OA，R6为氢，氰基，烷基，烯基，卤代烯基或炔基，各自不超过6个碳原子，或甲酰胺，A是氢或拟除虫菊酯典型的酸的基团，条件是R2不是氢，氯，溴，甲基或甲氧基当R 1为氢或甲基且R 3和A各自为氢时，此外，当A为四甲基环丙烷羧酸基时，R 1和R 2不为甲基，最后条件是R 2不为甲基，氯，溴或甲氧基，当A是基团时，R 1和R 3不是氢菊花酸，它们的制备及其作为作物保护剂的中间体或作为作物保护剂的用途。

5. 发明授权

US5199969A Azolylethane derivatives and fungicides and growth regulators containing them 失效
标题翻译：芳基聚乙烯衍生物和杀真菌剂以及含有它们的生长调节剂
公开(公告)号：US5199969A
公开(公告)日：1993-04-06
申请号：US660724
申请日：1991-02-25
申请人： Rainer Seele , Walter Himmele , Reiner Kober , Eberhard Ammermann , Gisela Lorenz , Wilhelm Rademacher , Johann Jung
发明人： Rainer Seele , Walter Himmele , Reiner Kober , Eberhard Ammermann , Gisela Lorenz , Wilhelm Rademacher , Johann Jung
IPC分类号： A01N43/50 , A01N43/653 , C07D249/08 , C07D521/00
CPC分类号： C07D231/12 , A01N43/50 , A01N43/653 , C07D233/56 , C07D249/08
摘要： Azolylethane derivatives of the general formula I ##STR1## where A and Z are each alkyl, phenyl, biphenyl, naphthyl, benzyl, cycloalkyl or cycloalkenyl, these radicals being substituted or unsubstituted, D is alkoxy, amino, mercapto, thiophenyl, aminophenyl, hetaryloxy or phenoxy, these radicals being substituted or unsubstituted, n is an integer from 1 to 5 or 0, and X is CH or N, and their plant-tolerated acid addition salts and metal complexes, and fungicides and growth regulators containing these compounds.
摘要翻译：其中A和Z各自为烷基，苯基，联苯基，萘基，苄基，环烷基或环烯基，这些基团为取代或未取代的，D为烷氧基，氨基，巯基，噻吩基，氨基苯基，苯氧基或苯氧基，这些基团是取代或未取代的，n是1至5或0的整数，X是CH或N，以及它们的植物耐受酸加成盐和金属络合物，以及含有这些化合物的杀真菌剂和生长调节剂。

6. 发明授权

US5068245A Fungicidal N-substituted 3-arylpyrrolidine derivatives 失效
标题翻译：杀真菌剂N-取代的3-氨基吡啶衍生物
公开(公告)号：US5068245A
公开(公告)日：1991-11-26
申请号：US251243
申请日：1988-09-30
申请人： Matthias Zipplies , Hubert Sauter , Franz Roehl , Walter Himmele , Eberhard Ammermann , Ernst-Heinrich Pommer
发明人： Matthias Zipplies , Hubert Sauter , Franz Roehl , Walter Himmele , Eberhard Ammermann , Ernst-Heinrich Pommer
IPC分类号： C07D207/06 , C07D207/08 , C07D405/04 , C07D405/08
CPC分类号： C07D405/08 , C07D207/06 , C07D207/08
摘要： N-Substituted 3-arylpyrrolidine derivatives of the formula ##STR1## where R.sup.1 is 2,2-dimethylpropyl, 3,3-dimethylbutyl, 4,4-dimethylpentyl, 2,4,4-trimethylpentyl, 6-methylhept-2-yl, 3,5,5-trimethylhexyl, 6,10-dimethylundec-2-yl, 3-methylcyclohexyl, 3,3-dimethylcyclohexyl, 3,3,5-trimethylcyclohexyl, 3,3,5,5-tetramethylcyclohexyl, 4-methylcyclohexyl, 4-ethylcyclohexyl, 4-propylcyclohexyl, 4-isopropylcyclohexyl, 4-tert.-butylcyclohexyl, trans-4-tert.-butylcyclohexyl, 4(2-methylbut-2-yl)cyclohexyl, 4(2,4,4-trimethylpent-2-yl)-cyclohexyl, cyclododecanyl, C.sub.3 -C.sub.9 -trialkylsilyl-substituted C.sub.4 -C.sub.12 -cycloalkyl, 4-hydroxycyclohexyl, 4-hydroxy-3-methylcyclohexyl, 4-hydroxy-3,5-dimethylcyclohexyl, 4-hydroxy-3,3-dimethylcyclohexyl, 4-hydroxy-3,3,5-trimethylcyclohexyl, unsubstituted or hydroxy-, C.sub.1 -C.sub.9 -alkyl-, C.sub.1 -C.sub.5 -alkoxy- or C.sub.3 -C.sub.9 -trialkylsilyl-substituted C.sub.5 -C.sub.12 -cycloalkenyl,R.sup.1 is further bicycloalkyl,R.sup.1 is further 4-tert.-butyl-benzyl, 4-chlorobenzyl, 4-tert.-butoxybenzyl, 1,4-dioxaspiro[4,5]decan-8-yl,5 to 7-membered heterocycloalkyl,5 to 7-membered heterocycloalkylmethyl,R.sup.2 is alkyl, alkoxy or trialkylsilyl,R.sup.3 is alkyl, alkenyl, alkynyl or arylalkyl,X- is a plant-tolerated anion,n is 0 or 1,and plant-tolerated salts thereof, and fungicides containing these compounds.
摘要翻译：其中R 1是2,2-二甲基丙基，3,3-二甲基丁基，4,4-二甲基戊基，2,4,4-三甲基戊基，6-甲基庚-2-基， 3,5,5-三甲基己基，6,10-二甲基十一烷基-2-基，3-甲基环己基，3,3-二甲基环己基，3,3,5-三甲基环己基，3,3,5,5-四甲基环己基，4-甲基环己基， 4-乙基环己基，4-丙基环己基，4-异丙基环己基，4-叔丁基环己基，反式-4-叔丁基环己基，4（2-甲基丁-2-基）环己基，4（2,4,4-三甲基 - 2-环己基，环十二烷基，C 3 -C 9 - 三烷基甲硅烷基取代的C 4 -C 12环烷基，4-羟基环己基，4-羟基-3-甲基环己基，4-羟基-3,5-二甲基环己基，4-羟基-3， 4-羟基-3,3,5-三甲基环己基，未取代或羟基 - ，C 1 -C 9 - 烷基 - ，C 1 -C 5 - 烷氧基 - 或C 3 -C 9 - 三烷基甲硅烷基取代的C 5 -C 12 - 环烯基，R 1是进一步的双环烷基，R 1还是4-叔丁基 - 苄基，4-氯苄基，4-叔丁氧基苄基，1,4-二氧杂螺[4,5]癸烷-8- 芳基，5至7元杂环烷基，5至7元杂环烷基甲基，R2为烷基，烷氧基或三烷基甲硅烷基，R3为烷基，烯基，炔基或芳烷基，X为植物耐受阴离子，n为0或1，及其耐受植物的盐，以及含有这些化合物的杀真菌剂。

7. 发明授权

US4656282A Preparation of substituted piperidines 失效
标题翻译：取代哌啶的制备
公开(公告)号：US4656282A
公开(公告)日：1987-04-07
申请号：US794744
申请日：1985-11-04
申请人： Walter Himmele , Walter-Wielant Wiersdorff , Marco Thyes
发明人： Walter Himmele , Walter-Wielant Wiersdorff , Marco Thyes
IPC分类号： C07D211/12 , C07D211/14 , C07D211/16 , C07D295/023 , C07D217/02 , C07D217/04
CPC分类号： C07D295/023 , C07D211/12 , C07D211/14
摘要： Piperidines substituted in the 3- and/or 4-position are prepared by reacting a glutardialdehyde substituted in the 2- and/or 3-position with ammonia or a primary amine and hydrogen at elevated temperature and under superatmospheric pressure in the presence of a hydrogenation catalyst.
摘要翻译：通过在2-和/或3-位取代的戊二醛与氨或伯胺和氢在升高的温度和超大气压下在氢化存在下反应制备在3-和/或4-位上取代的哌啶子催化剂。

8. 发明授权

US3996246A Resolution of racemic pantolactone 失效
标题翻译：外消旋泛酸内酯的分辨率
公开(公告)号：US3996246A
公开(公告)日：1976-12-07
申请号：US543695
申请日：1975-01-24
申请人： Werner Hoffmann , Walter Himmele , Joachim Paust , Karl Von Fraunberg , Hardo Siegel , Sigberg Pfohl
发明人： Werner Hoffmann , Walter Himmele , Joachim Paust , Karl Von Fraunberg , Hardo Siegel , Sigberg Pfohl
IPC分类号： B01D9/02 , C07B31/00 , C07B57/00 , C07C51/00 , C07C59/105 , C07C67/00 , C07C209/00 , C07C209/26 , C07C211/19 , C07D307/33 , C07D307/32
CPC分类号： C07D307/33
摘要： A process for resolving racemic .alpha.-hydroxy-.beta.,.beta.-dimethyl-.gamma.-butyrolactone, referred to as D,L-pantolactone, into its optical antipodes, based on the separation of diastereomeric salts of D,L-pantoic acid (.alpha.,.gamma.-dihydroxy-.beta.,.beta.-dimethylbutyric acid), produced from D,L-pantolactone, by means of (-)-3-aminomethylpinane, (+)-3-aminomethylpinane or one of their acid addition salts, as a new resolving agent.
摘要翻译：基于D，L-泛解酸（α，β-二甲基-γ-丁内酯）的非对映异构体盐的分离，将外消旋α-羟基-ββ-二甲基-γ-丁内酯（称为D，L-泛酸内酯）分解成其光学对映体的方法，通过（ - ） - 3-氨基甲基蒎烷，（+） - 3-氨基甲基蒎烷或其酸加成盐之一，由D，L-泛酸内酯产生的γ-二羟基-β，β-二甲基丁酸）作为新的分解代理商

9. 发明授权

US3966827A Production of 3-methylpentane-1,5-diol 失效
标题翻译：制备3-甲基戊烷-1,5-二醇
公开(公告)号：US3966827A
公开(公告)日：1976-06-29
申请号：US541638
申请日：1975-01-16
申请人： Werner Aquila , Walter Himmele , Werner Fliege , Hardo Siegel
发明人： Werner Aquila , Walter Himmele , Werner Fliege , Hardo Siegel
IPC分类号： B01J31/00 , C07B61/00 , C07C27/00 , C07C29/10 , C07C29/132 , C07C31/20 , C07C67/00 , C07D309/10 , C07C29/00
CPC分类号： C07C29/103 , C07D309/10
摘要： The production of 3-methylpentane-1,5-diol by hydroformylation of 2-methylbut-1-en-4-ol with carbon monoxide and hydrogen at elevated temperature and superatmospheric pressure in the presence of a rhodium carbonyl complex which has been modified by a tertiary organic phosphine followed by hydrogenation of the 2-hydroxy-4-methyltetrahydropyran at elevated temperature and superatmospheric pressure in the presence of a hydrogenation catalyst.
摘要翻译：通过2-甲基丁-1-烯-4-醇与一氧化碳和氢气在升高的温度和超大气压下在羰基铑络合物的存在下加氢甲酰化生产3-甲基戊烷-1,5-二醇，已经被然后在氢化催化剂存在下，在升高的温度和超大气压下，对2-羟基-4-甲基四氢吡喃进行氢化。

10. 发明授权

US5102899A Azolylmethyloxiranes and fungicides containing them 失效
标题翻译：青蒿琥酯和含有它们的杀真菌剂
公开(公告)号：US5102899A
公开(公告)日：1992-04-07
申请号：US493319
申请日：1990-03-14
申请人： Rainer Seele , Walter Himmele , Stefan Karbach , Hubert Sauter , Eberhard Ammermann , Gisela Lorenz
发明人： Rainer Seele , Walter Himmele , Stefan Karbach , Hubert Sauter , Eberhard Ammermann , Gisela Lorenz
IPC分类号： C07D405/00 , A01N43/653 , C07D249/08 , C07D521/00
CPC分类号： C07D249/08 , A01N43/653 , C07D231/12 , C07D233/56
摘要： Azolylmethyloxiranes of the general formula I ##STR1## where R.sup.1, R.sup.2 and R.sup.3 are substituted or unsubstituted alkyl, benzyl, naphthyl, biphenyl, dioxanyl, phenyl, tetrahydropyranyl, tetrahydrofuranyl, norbornyl, C.sub.3 -C.sub.12 -cycloalkyl or C.sub.3 -C.sub.12 -cycloalkenyl, and X is CH or N, and plant-tolerated acid addition salts and metal complexes thereof, and fungicides containing these compounds.
摘要翻译：苄基，萘基，联苯基，二烷基，苯基，四氢吡喃基，四氢呋喃基，降冰片基，C 3 -C 12 - 环烷基或C 3 -C 12 - 环烯基的通式I的唑基甲基环氧乙烷， X是CH或N，以及植物耐受的酸加成盐和金属络合物，以及含有这些化合物的杀真菌剂。

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