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1. 发明授权

US4618668A Preparation of polyphenylene ethers 失效
标题翻译：聚苯醚的制备
公开(公告)号：US4618668A
公开(公告)日：1986-10-21
申请号：US722154
申请日：1985-04-11
申请人： Volker Muench , Juergen Hambrecht , Walter Himmele , Adolf Echte , Johann Swoboda
发明人： Volker Muench , Juergen Hambrecht , Walter Himmele , Adolf Echte , Johann Swoboda
IPC分类号： C08G65/44 , C08G65/46
CPC分类号： C08G65/44
摘要： High molecular weight polyphenylene ethers are prepared from monohydric phenols by an oxidative coupling reaction with oxygen in the presence of a solvent and of a catalyst complex consisting of a copper salt and an organic amine of the general formula ##STR1## where R.sup.1 is C.sub.2 -C.sub.20 -alkylidene, preferably C.sub.2 -C.sub.12 -alkylidene, or alkenylidene, R.sup.2 is H or C.sub.1 -C.sub.12 -alkyl, preferably C.sub.1 -C.sub.4 -alkyl, or C.sub.5 -C.sub.8 -cycloalkyl, each of which is unsubstituted or substituted by functional groups, and n is an integer from 1 to 4, preferably 1 or 2. Preferred functional groups are --OR.sup.3, --NHR.sup.3 or --SR.sup.3, in which R.sup.3 is H C.sub.1 -C.sub.12 -alkyl or C.sub.5 -C.sub.8 -cycloalkyl, and the most suitable amines are 3-tert.-butoxypropylamine, 4-tert.-butoxybutylamine, 3-tert.-butoxy-2-methylpropylamine, 3-tert.-butoxy-2,3-dimethylpropylamine, 3-tert.-butoxy-2-methyloctylamine and N-methyl-N-(4-tert.-butoxybutyl)-amine. The polyphenylene ethers can be processed to moldings by a thermoplastic method.
摘要翻译：高分子量聚苯醚通过在溶剂存在下与氧气的氧化偶联反应和由通式为“IMAGE”的铜盐和有机胺组成的催化剂络合物由一元酚制备，其中R1为C2-C20 亚烷基，优选C 2 -C 12亚烷基或亚烯基，R 2是H或C 1 -C 12烷基，优选C 1 -C 4 - 烷基或C 5 -C 8 - 环烷基，其各自是未取代的或被官能团取代，n 是1至4的整数，优选1或2.优选的官能团是-OR 3，-NHR 3或-SR 3，其中R 3是H-C 1 -C 12 - 烷基或C 5 -C 8 - 环烷基，最合适的胺是3 叔丁氧基丙基胺，4-叔丁氧基丁胺，3-叔丁氧基-2-甲基丙胺，3-叔丁氧基-2,3-二甲基丙胺，3-叔丁氧基-2-甲基辛胺和N- 甲基-N-（4-叔丁氧基丁基） - 胺。可以通过热塑性方法将聚苯醚加工成模制品。

2. 发明授权

US5199969A Azolylethane derivatives and fungicides and growth regulators containing them 失效
标题翻译：芳基聚乙烯衍生物和杀真菌剂以及含有它们的生长调节剂
公开(公告)号：US5199969A
公开(公告)日：1993-04-06
申请号：US660724
申请日：1991-02-25
申请人： Rainer Seele , Walter Himmele , Reiner Kober , Eberhard Ammermann , Gisela Lorenz , Wilhelm Rademacher , Johann Jung
发明人： Rainer Seele , Walter Himmele , Reiner Kober , Eberhard Ammermann , Gisela Lorenz , Wilhelm Rademacher , Johann Jung
IPC分类号： A01N43/50 , A01N43/653 , C07D249/08 , C07D521/00
CPC分类号： C07D231/12 , A01N43/50 , A01N43/653 , C07D233/56 , C07D249/08
摘要： Azolylethane derivatives of the general formula I ##STR1## where A and Z are each alkyl, phenyl, biphenyl, naphthyl, benzyl, cycloalkyl or cycloalkenyl, these radicals being substituted or unsubstituted, D is alkoxy, amino, mercapto, thiophenyl, aminophenyl, hetaryloxy or phenoxy, these radicals being substituted or unsubstituted, n is an integer from 1 to 5 or 0, and X is CH or N, and their plant-tolerated acid addition salts and metal complexes, and fungicides and growth regulators containing these compounds.
摘要翻译：其中A和Z各自为烷基，苯基，联苯基，萘基，苄基，环烷基或环烯基，这些基团为取代或未取代的，D为烷氧基，氨基，巯基，噻吩基，氨基苯基，苯氧基或苯氧基，这些基团是取代或未取代的，n是1至5或0的整数，X是CH或N，以及它们的植物耐受酸加成盐和金属络合物，以及含有这些化合物的杀真菌剂和生长调节剂。

3. 发明授权

US5068245A Fungicidal N-substituted 3-arylpyrrolidine derivatives 失效
标题翻译：杀真菌剂N-取代的3-氨基吡啶衍生物
公开(公告)号：US5068245A
公开(公告)日：1991-11-26
申请号：US251243
申请日：1988-09-30
申请人： Matthias Zipplies , Hubert Sauter , Franz Roehl , Walter Himmele , Eberhard Ammermann , Ernst-Heinrich Pommer
发明人： Matthias Zipplies , Hubert Sauter , Franz Roehl , Walter Himmele , Eberhard Ammermann , Ernst-Heinrich Pommer
IPC分类号： C07D207/06 , C07D207/08 , C07D405/04 , C07D405/08
CPC分类号： C07D405/08 , C07D207/06 , C07D207/08
摘要： N-Substituted 3-arylpyrrolidine derivatives of the formula ##STR1## where R.sup.1 is 2,2-dimethylpropyl, 3,3-dimethylbutyl, 4,4-dimethylpentyl, 2,4,4-trimethylpentyl, 6-methylhept-2-yl, 3,5,5-trimethylhexyl, 6,10-dimethylundec-2-yl, 3-methylcyclohexyl, 3,3-dimethylcyclohexyl, 3,3,5-trimethylcyclohexyl, 3,3,5,5-tetramethylcyclohexyl, 4-methylcyclohexyl, 4-ethylcyclohexyl, 4-propylcyclohexyl, 4-isopropylcyclohexyl, 4-tert.-butylcyclohexyl, trans-4-tert.-butylcyclohexyl, 4(2-methylbut-2-yl)cyclohexyl, 4(2,4,4-trimethylpent-2-yl)-cyclohexyl, cyclododecanyl, C.sub.3 -C.sub.9 -trialkylsilyl-substituted C.sub.4 -C.sub.12 -cycloalkyl, 4-hydroxycyclohexyl, 4-hydroxy-3-methylcyclohexyl, 4-hydroxy-3,5-dimethylcyclohexyl, 4-hydroxy-3,3-dimethylcyclohexyl, 4-hydroxy-3,3,5-trimethylcyclohexyl, unsubstituted or hydroxy-, C.sub.1 -C.sub.9 -alkyl-, C.sub.1 -C.sub.5 -alkoxy- or C.sub.3 -C.sub.9 -trialkylsilyl-substituted C.sub.5 -C.sub.12 -cycloalkenyl,R.sup.1 is further bicycloalkyl,R.sup.1 is further 4-tert.-butyl-benzyl, 4-chlorobenzyl, 4-tert.-butoxybenzyl, 1,4-dioxaspiro[4,5]decan-8-yl,5 to 7-membered heterocycloalkyl,5 to 7-membered heterocycloalkylmethyl,R.sup.2 is alkyl, alkoxy or trialkylsilyl,R.sup.3 is alkyl, alkenyl, alkynyl or arylalkyl,X- is a plant-tolerated anion,n is 0 or 1,and plant-tolerated salts thereof, and fungicides containing these compounds.
摘要翻译：其中R 1是2,2-二甲基丙基，3,3-二甲基丁基，4,4-二甲基戊基，2,4,4-三甲基戊基，6-甲基庚-2-基， 3,5,5-三甲基己基，6,10-二甲基十一烷基-2-基，3-甲基环己基，3,3-二甲基环己基，3,3,5-三甲基环己基，3,3,5,5-四甲基环己基，4-甲基环己基， 4-乙基环己基，4-丙基环己基，4-异丙基环己基，4-叔丁基环己基，反式-4-叔丁基环己基，4（2-甲基丁-2-基）环己基，4（2,4,4-三甲基 - 2-环己基，环十二烷基，C 3 -C 9 - 三烷基甲硅烷基取代的C 4 -C 12环烷基，4-羟基环己基，4-羟基-3-甲基环己基，4-羟基-3,5-二甲基环己基，4-羟基-3， 4-羟基-3,3,5-三甲基环己基，未取代或羟基 - ，C 1 -C 9 - 烷基 - ，C 1 -C 5 - 烷氧基 - 或C 3 -C 9 - 三烷基甲硅烷基取代的C 5 -C 12 - 环烯基，R 1是进一步的双环烷基，R 1还是4-叔丁基 - 苄基，4-氯苄基，4-叔丁氧基苄基，1,4-二氧杂螺[4,5]癸烷-8- 芳基，5至7元杂环烷基，5至7元杂环烷基甲基，R2为烷基，烷氧基或三烷基甲硅烷基，R3为烷基，烯基，炔基或芳烷基，X为植物耐受阴离子，n为0或1，及其耐受植物的盐，以及含有这些化合物的杀真菌剂。

4. 发明授权

US4656282A Preparation of substituted piperidines 失效
标题翻译：取代哌啶的制备
公开(公告)号：US4656282A
公开(公告)日：1987-04-07
申请号：US794744
申请日：1985-11-04
申请人： Walter Himmele , Walter-Wielant Wiersdorff , Marco Thyes
发明人： Walter Himmele , Walter-Wielant Wiersdorff , Marco Thyes
IPC分类号： C07D211/12 , C07D211/14 , C07D211/16 , C07D295/023 , C07D217/02 , C07D217/04
CPC分类号： C07D295/023 , C07D211/12 , C07D211/14
摘要： Piperidines substituted in the 3- and/or 4-position are prepared by reacting a glutardialdehyde substituted in the 2- and/or 3-position with ammonia or a primary amine and hydrogen at elevated temperature and under superatmospheric pressure in the presence of a hydrogenation catalyst.
摘要翻译：通过在2-和/或3-位取代的戊二醛与氨或伯胺和氢在升高的温度和超大气压下在氢化存在下反应制备在3-和/或4-位上取代的哌啶子催化剂。

5. 发明授权

US3996246A Resolution of racemic pantolactone 失效
标题翻译：外消旋泛酸内酯的分辨率
公开(公告)号：US3996246A
公开(公告)日：1976-12-07
申请号：US543695
申请日：1975-01-24
申请人： Werner Hoffmann , Walter Himmele , Joachim Paust , Karl Von Fraunberg , Hardo Siegel , Sigberg Pfohl
发明人： Werner Hoffmann , Walter Himmele , Joachim Paust , Karl Von Fraunberg , Hardo Siegel , Sigberg Pfohl
IPC分类号： B01D9/02 , C07B31/00 , C07B57/00 , C07C51/00 , C07C59/105 , C07C67/00 , C07C209/00 , C07C209/26 , C07C211/19 , C07D307/33 , C07D307/32
CPC分类号： C07D307/33
摘要： A process for resolving racemic .alpha.-hydroxy-.beta.,.beta.-dimethyl-.gamma.-butyrolactone, referred to as D,L-pantolactone, into its optical antipodes, based on the separation of diastereomeric salts of D,L-pantoic acid (.alpha.,.gamma.-dihydroxy-.beta.,.beta.-dimethylbutyric acid), produced from D,L-pantolactone, by means of (-)-3-aminomethylpinane, (+)-3-aminomethylpinane or one of their acid addition salts, as a new resolving agent.
摘要翻译：基于D，L-泛解酸（α，β-二甲基-γ-丁内酯）的非对映异构体盐的分离，将外消旋α-羟基-ββ-二甲基-γ-丁内酯（称为D，L-泛酸内酯）分解成其光学对映体的方法，通过（ - ） - 3-氨基甲基蒎烷，（+） - 3-氨基甲基蒎烷或其酸加成盐之一，由D，L-泛酸内酯产生的γ-二羟基-β，β-二甲基丁酸）作为新的分解代理商

6. 发明授权

US3975400A Method of continuously producing .gamma.-butyrolactams 失效
标题翻译：连续生产{65-丁内酰胺的方法
公开(公告)号：US3975400A
公开(公告)日：1976-08-17
申请号：US334398
申请日：1973-02-21
申请人： Walter Himmele , Ernst Hofmann , Herwig Hoffmann , Reinhold Plass
发明人： Walter Himmele , Ernst Hofmann , Herwig Hoffmann , Reinhold Plass
IPC分类号： C07D207/26 , C07D207/267
CPC分类号： C07D207/267
摘要： Method of producing .gamma.-butyrolactams by reacting .gamma.-butyrolactones with ammonia in the presence or absence of water at elevated temperatures and pressures. The reaction is carried out continuously at temperatures ranging from 180.degree. to 340.degree.C whilst maintaining pressures which are at least 10 percent higher than the pressure equal to the sum of the partial pressures of the reactants at the temperature used. .gamma.-Butyrolactams are valuable intermediates, for example in the manufacture of polymers, pharmaceuticals and solvents.
摘要翻译：在高温和高压下，在存在或不存在水的情况下，使γ-丁内酯与氨反应制备γ-丁内酰胺的方法。反应在180℃至340℃的温度下连续进行，同时保持比在所用温度下等于反应物分压之和的压力至少高10％的压力。 γ-丁内酰胺是有价值的中间体，例如在聚合物，药物和溶剂的制备中。

7. 发明授权

US3966827A Production of 3-methylpentane-1,5-diol 失效
标题翻译：制备3-甲基戊烷-1,5-二醇
公开(公告)号：US3966827A
公开(公告)日：1976-06-29
申请号：US541638
申请日：1975-01-16
申请人： Werner Aquila , Walter Himmele , Werner Fliege , Hardo Siegel
发明人： Werner Aquila , Walter Himmele , Werner Fliege , Hardo Siegel
IPC分类号： B01J31/00 , C07B61/00 , C07C27/00 , C07C29/10 , C07C29/132 , C07C31/20 , C07C67/00 , C07D309/10 , C07C29/00
CPC分类号： C07C29/103 , C07D309/10
摘要： The production of 3-methylpentane-1,5-diol by hydroformylation of 2-methylbut-1-en-4-ol with carbon monoxide and hydrogen at elevated temperature and superatmospheric pressure in the presence of a rhodium carbonyl complex which has been modified by a tertiary organic phosphine followed by hydrogenation of the 2-hydroxy-4-methyltetrahydropyran at elevated temperature and superatmospheric pressure in the presence of a hydrogenation catalyst.
摘要翻译：通过2-甲基丁-1-烯-4-醇与一氧化碳和氢气在升高的温度和超大气压下在羰基铑络合物的存在下加氢甲酰化生产3-甲基戊烷-1,5-二醇，已经被然后在氢化催化剂存在下，在升高的温度和超大气压下，对2-羟基-4-甲基四氢吡喃进行氢化。

8. 发明授权

US5102899A Azolylmethyloxiranes and fungicides containing them 失效
标题翻译：青蒿琥酯和含有它们的杀真菌剂
公开(公告)号：US5102899A
公开(公告)日：1992-04-07
申请号：US493319
申请日：1990-03-14
申请人： Rainer Seele , Walter Himmele , Stefan Karbach , Hubert Sauter , Eberhard Ammermann , Gisela Lorenz
发明人： Rainer Seele , Walter Himmele , Stefan Karbach , Hubert Sauter , Eberhard Ammermann , Gisela Lorenz
IPC分类号： C07D405/00 , A01N43/653 , C07D249/08 , C07D521/00
CPC分类号： C07D249/08 , A01N43/653 , C07D231/12 , C07D233/56
摘要： Azolylmethyloxiranes of the general formula I ##STR1## where R.sup.1, R.sup.2 and R.sup.3 are substituted or unsubstituted alkyl, benzyl, naphthyl, biphenyl, dioxanyl, phenyl, tetrahydropyranyl, tetrahydrofuranyl, norbornyl, C.sub.3 -C.sub.12 -cycloalkyl or C.sub.3 -C.sub.12 -cycloalkenyl, and X is CH or N, and plant-tolerated acid addition salts and metal complexes thereof, and fungicides containing these compounds.
摘要翻译：苄基，萘基，联苯基，二烷基，苯基，四氢吡喃基，四氢呋喃基，降冰片基，C 3 -C 12 - 环烷基或C 3 -C 12 - 环烯基的通式I的唑基甲基环氧乙烷， X是CH或N，以及植物耐受的酸加成盐和金属络合物，以及含有这些化合物的杀真菌剂。

9. 发明授权

US4914133A Amino compounds and fungicides containing them 失效
标题翻译：含有氨基化合物和杀真菌剂
公开(公告)号：US4914133A
公开(公告)日：1990-04-03
申请号：US181503
申请日：1988-04-14
申请人： Walter Himmele , Hubert Sauter , Hardo Siegel , Eberhard Ammermann , Ernst-Heinrich Pommer
发明人： Walter Himmele , Hubert Sauter , Hardo Siegel , Eberhard Ammermann , Ernst-Heinrich Pommer
IPC分类号： A01N33/04
CPC分类号： A01N33/04
摘要： Amino compounds of the formula ##STR1## where R.sup.1 is alkyl, A is alkylene or alkenylene, and Ar is aryl, and their acid addition salts, and fungicides containing these compounds.
摘要翻译：其中R1是烷基，A是亚烷基或亚烯基，Ar是芳基的氨基化合物及其酸加成盐和含有这些化合物的杀真菌剂。

10. 发明授权

US4877807A 5-phenyl-1,2,3a,4,5,9b-hexahydro-3H-benz(e)indotes preparation and use thereof as drugs 失效
标题翻译： 5-苯基-1,2,3a，4,5,9b-六氢-3H-苯并（e）将其制备和用途作为药物
公开(公告)号：US4877807A
公开(公告)日：1989-10-31
申请号：US197274
申请日：1988-05-23
申请人： Gerd Steiner , Walter Himmele , Ernst Buschmann , Hans-Juergen Teschendorf , Harald Weifenbach
发明人： Gerd Steiner , Walter Himmele , Ernst Buschmann , Hans-Juergen Teschendorf , Harald Weifenbach
IPC分类号： A61K31/40 , A61K31/403 , A61P25/08 , A61P25/18 , A61P25/20 , A61P25/24 , A61P25/26 , C07D209/60
CPC分类号： C07D209/60
摘要： A 5-phenyl-1,3,3a,4,5,9b-hexahydro-3H-benz(e)indole compound of the formula I: ##STR1## wherein R.sup.1 is hydrogen or C.sub.1-6 alkyl, R.sup.2 is hydrogen or C.sub.1-3 alkyl in the 3a- or 4-position, R.sup.3 and R.sup.4 are each hydrogen, hydroxyl, halogen, C.sub.1-3 alkyl, C.sub.1-3 alkoxy, C.sub.1-3 alkylthio or trifluoromethyl, acetylamino or amino and R.sup.5 is hydrogen or C.sub.1-3 alkyl, or a salt thereof with a physiologically tolerated acid. The compounds and compositions are useful for treating depression or trating convulsions and which exhibit a sedative and tranquilizing effect when administered to a patient.
摘要翻译：式I的5-苯基-1,3,3a，4,5,9b-六氢-3H-苯并（e）吲哚化合物：其中R 1是氢或C 1-6烷基，R 2是氢或 R 3和R 4各自为氢，羟基，卤素，C 1-3烷基，C 1-3烷氧基，C 1-3烷硫基或三氟甲基，乙酰氨基或氨基，R 5为氢或C 1 -C 3烷基 -3烷基或其盐与生理上耐受的酸反应。所述化合物和组合物可用于治疗抑郁症或治疗惊厥，并且当施用于患者时其具有镇静和镇静作用。

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