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1. 发明授权

US5073650A Preparation of 1,4-butanediol 失效
标题翻译： 1,4-丁二醇的制备
公开(公告)号：US5073650A
公开(公告)日：1991-12-17
申请号：US672671
申请日：1991-03-20
申请人： Uwe Stabel , Hans-Juergen Gosch , Rolf Fischer , Wolfgang Harder , Claus Hechler
发明人： Uwe Stabel , Hans-Juergen Gosch , Rolf Fischer , Wolfgang Harder , Claus Hechler
IPC分类号： B01J23/889 , B01J23/75 , C07B61/00 , C07C29/149 , C07C29/17 , C07C31/20
CPC分类号： C07C29/177
摘要： A process for the preparation of 1,4-butanediol by catalytically hydrogenating maleic anhydride in the presence of an alcohol, at elevated temperature and elevated pressure and with the aid of a cobalt-containing catalyst comprises partially hydrogenating the reaction mixture in a first hydrogenation step at from 100.degree. to 200.degree. C. and at from 30 to 200 bar and subsequently post-hydrogenating the product of this first hydrogenation step, without further work-up at higher temperature and pressure than in the first hydrogenation step, in a second hydrogenation step at from 200.degree. to 300.degree. C. and at from 200 to 350 bar.
摘要翻译：通过在醇的存在下，在升高的温度和升高的压力下并借助含钴催化剂催化氢化马来酸酐来制备1,4-丁二醇的方法包括在第一氢化步骤中部分氢化反应混合物在100至200℃和30至200巴条件下，随后在第二加氢步骤中将第一氢化步骤的产物后氢化，而不需要在比第一加氢步骤更高的温度和压力下进一步处理。步骤为200〜300℃，200〜350巴。

2. 发明授权

US5128490A Isolation of tetrahydrofuran from mixtures which contain tetrahydrofuran, 1,4-butanediol, gamma-butyro-lactone and succinic acid esters 失效
标题翻译：从含有四氢呋喃，1,4-丁二醇，甘氨酸和乳酸的混合物中分离出四氢呋喃
公开(公告)号：US5128490A
公开(公告)日：1992-07-07
申请号：US658087
申请日：1991-02-20
申请人： Stabel Uwe , Hans-Juergen Gosch , Rolf Fischer , Wolfgang Harder , Claus Hechler
发明人： Stabel Uwe , Hans-Juergen Gosch , Rolf Fischer , Wolfgang Harder , Claus Hechler
IPC分类号： B01J21/16 , C07B61/00 , C07B63/04 , C07D307/08
CPC分类号： C07D307/08
摘要： A process is described for isolating tetrahydrofuran from mixtures containing tetrahydrofuran, 1,4-butanediol, -butyrolactone and succinic acid esters, in which the mixtures are heated to from 150.degree. to 250.degree. C. in the presence of phyllosilicates, the resultant tetrahydrofuran and water of reaction are removed from the reaction mixture by distillation, and the tetrahydrofuran is separated from the distillate.
摘要翻译：描述了从含有四氢呋喃，1,4-丁二醇，丁内酯和琥珀酸酯的混合物中分离四氢呋喃的方法，其中将混合物在页硅酸盐存在下加热至150-250℃，得到的四氢呋喃和通过蒸馏从反应混合物中除去反应水，并将四氢呋喃与馏出物分离。

3. 发明授权

US5342488A Separation of 1,4-butanediol from hydrogenation mixtures 失效
标题翻译：从氢化混合物中分离出1,4-丁二醇
公开(公告)号：US5342488A
公开(公告)日：1994-08-30
申请号：US18496
申请日：1993-02-17
申请人： Hans-Juergen Gosch , Harald Rust , Rolf Fischer , Claus Hechler , Rolf Pinkos
发明人： Hans-Juergen Gosch , Harald Rust , Rolf Fischer , Claus Hechler , Rolf Pinkos
IPC分类号： C07C29/80 , C07C29/82 , C07C31/20 , B01D3/00 , C07C27/00
CPC分类号： C07C29/80 , Y10S203/20
摘要： A process for the separation of 1,4-butanediol from mixtures obtained by the catalytic hydrogenation of maleates, fumarates, and/or succinates, which also contain tetrahydrofuran, water, C.sub.1 -C.sub.4 alcohols, succinic diesters, hydroxybutyrates, alkylhydroxyalkyl succinates, gamma-butyrolactone and butyrates, in addition to 1,4-butanediol, comprising the following steps:a) separating, in a first column having an actual number of plates of from 20 to 70 and operated at a top pressure of from 50 to 1100 mbar and preferably from 50 to 500 mbar and a top temperature of from 40.degree. to 120.degree. C., alcohol, water and tetrahydrofuran, as overhead product,b) feeding the bottom product of the first column into a second column having an actual number of plates of from 30 to 90 and withdrawing the overhead product consisting of alcohol and butyrate and obtained at a top pressure of from 45 to 250 mbar and a top temperature of from 45.degree. to 120.degree. C., and withdrawing gamma-butyrolactone and butyrates through a side outlet, and feeding the bottom product to a phase separator,c) feeding the 1,4-butanediol-enriched bottom phase of the liquid two-phase mixture coming from the phase separator to a third column having an actual number of plates of from 30 to 90, alcohol being distilled off as overhead product at a top pressure of from 45 to 250 mbar and a top temperature of from 45.degree. to 120.degree. C., and the azeotrope comprising 1,4 -butanediol and succinic diester is withdrawn as a sidestream and recycled to the phase separator, whilst 1,4-butanediol is removed together with alkyl-hydroxyalkyl succinate, butyl hydroxybutyrate, and high-boiling fractions as bottoms, andd) separating the succinate-enriched top phase in the phase separator.
摘要翻译：还含有四氢呋喃，水，C 1 -C 4醇，琥珀酸二酯，羟基丁酸酯，琥珀酸烷基羟基烷基酯，γ-丁内酯和/或琥珀酸酯的马来酸盐，富马酸盐和/或琥珀酸盐的催化氢化得到的混合物的分离方法，丁内酯和丁酸酯除了1,4-丁二醇外还包括以下步骤：a）在具有20至70的实际板数的第一塔中分离并在50至1100毫巴的最高压力下操作，以及优选为50至500毫巴，顶部温度为40至120℃，醇，水和四氢呋喃作为塔顶产物，b）将第一塔的底部产物进料到具有实际数量的板的第二塔 30至90份，并取出由醇和丁酸盐组成的塔顶产物，并在顶部压力为45至250毫巴，顶部温度为45至120℃下获得，并将γ-丁内酯和丁酸酯通过侧出口将底部产物供给到相分离器中，c）将来自相分离器的液体两相混合物的富含1,4-丁二醇的底相进料到具有实际数量的板的第三塔为30至90，在顶部压力为45至250毫巴，顶部温度为45至120℃的条件下，蒸馏出作为塔顶产物的醇，由1,4-丁二醇和琥珀酸二酯组成的共沸物为作为侧流回收并循环到相分离器中，而1,4-丁二醇与琥珀酸烷基 - 羟基烷基酯，羟基丁酸丁酯和作为塔底产物的高沸点馏分一起除去，以及d）在相中分离富含琥珀酸酯的顶相分隔器。

4. 发明授权

US07253308B1 Method for catalytic phase oxidation to (meth) acrolein and/or (meth) acrylic acid 有权
标题翻译：催化相氧化成（甲基）丙烯醛和/或（甲基）丙烯酸的方法
公开(公告)号：US07253308B1
公开(公告)日：2007-08-07
申请号：US10110229
申请日：2000-11-03
申请人： Claus Hechler , Otto Machhammer , Gerhard Olbert , Uwe Stabel , Peter Zehner
发明人： Claus Hechler , Otto Machhammer , Gerhard Olbert , Uwe Stabel , Peter Zehner
IPC分类号： C07C51/16 , C07B41/00
CPC分类号： B01J19/249 , B01J8/0285 , B01J2208/0015 , B01J2208/022 , B01J2219/0002 , B01J2219/2453 , B01J2219/2456 , B01J2219/2462 , B01J2219/2474 , B01J2219/2479 , B01J2219/2481 , C07C45/33 , C07C45/35 , C07C45/37 , F28D9/0006 , F28D9/0031 , F28F2250/104
摘要： A process for the continuous gas-phase oxidation of C3- and C4-precursors to (meth)acrolein and/or (meth)acrylic acid in the presence of a catalyst in a reactor which has a feed for the reaction mixture at one reactor end and removal of the reaction mixture at the opposite reactor end and which is equipped with means, arranged in the interior of the reactor, for removing the heat of reaction, through which means a heat exchange composition flows and which means are in the form of heat exchanger plates, is proposed.
摘要翻译：一种将C 3 - 和C 4 - - 前体连续气相氧化成（甲基）丙烯醛和/或（甲基）丙烯酸的方法，在反应器中的催化剂，其在一个反应器端具有用于反应混合物的进料并在相对的反应器端除去反应混合物，并且装备有设置在反应器内部的装置，用于除去反应热，通过这意味着热交换组合物流动，并且哪种装置是热交换器板的形式。

5. 发明授权

US06624315B2 Method of gas phase catalytic oxidation to give maleic acid anhydride 失效
标题翻译：气相催化氧化法得到马来酸酐
公开(公告)号：US06624315B2
公开(公告)日：2003-09-23
申请号：US09936347
申请日：2001-09-11
申请人： Peter Zehner , Otto Machhammer , Claus Hechler , Alexander Weck , Gerhard Olbert , Uwe Stabel
发明人： Peter Zehner , Otto Machhammer , Claus Hechler , Alexander Weck , Gerhard Olbert , Uwe Stabel
IPC分类号： C07D30760
CPC分类号： B01J35/04 , B01J8/0285 , B01J19/249 , B01J2208/0015 , B01J2208/022 , B01J2219/0002 , B01J2219/2453 , B01J2219/2454 , B01J2219/2455 , B01J2219/2462 , B01J2219/2464 , B01J2219/2479 , B01J2219/2495 , B01J2219/2497 , B01J2219/2498 , B01J2219/32475 , C07C51/215 , C07C57/145
摘要： A process for the preparation of maleic anhydride by heterogeneously catalyzed gas-phase oxidation in a reactor with feed for the reaction mixture at one end of the reactor and discharge of the product mixture at the opposite end of the reactor, and with devices for dissipating the heat of reaction which are arranged in the reactor interior and through which a heat-exchange medium flows and which are designed as heat-exchanger plates.
摘要翻译：在反应器中通过异构催化气相氧化制备马来酸酐的方法，其中反应器的一端具有反应混合物的进料并在反应器的另一端排出产物混合物，以及用于消散反应器的装置布置在反应器内部并通过热交换介质流动并被设计为热交换器板的反应热。

6. 发明授权

US08721996B2 Reactor for continuous heterogeneously catalyzed partial dehydrogenation of at least one hydrocarbon to be dehydrogenated 有权
标题翻译：用于连续非均相催化的至少一种待脱氢烃的部分脱氢反应器
公开(公告)号：US08721996B2
公开(公告)日：2014-05-13
申请号：US12841211
申请日：2010-07-22
申请人： Claus Hechler , Wilhelm Ruppel , Goetz-Peter Schindler , Catharina Klanner , Hans-Juergen Bassler , Martin Dieterle , Karl-Heinrich Klappert , Klaus Joachim Mueller-Engel
发明人： Claus Hechler , Wilhelm Ruppel , Goetz-Peter Schindler , Catharina Klanner , Hans-Juergen Bassler , Martin Dieterle , Karl-Heinrich Klappert , Klaus Joachim Mueller-Engel
IPC分类号： B01J8/00
CPC分类号： C07C5/3335 , B01J8/008 , B01J8/02 , B01J8/18 , B01J19/02 , B01J2219/00033 , B01J2219/0236 , B01J2219/0286 , C07C5/321 , C07C5/333 , C07C5/48 , C07C45/33 , C07C45/35 , C07C51/215 , C07C51/252 , C07C51/43 , C07C67/08 , C22C38/001 , C22C38/005 , C22C38/02 , C22C38/04 , C22C38/34 , C22C38/40 , C23C10/08 , C23C10/50 , Y02P20/52 , Y02T50/67 , C07C11/06 , C07C57/04 , C07C69/54 , C07C11/04 , C07C47/22
摘要： A shell which encloses an interior and has at least one first orifice for feeding at least one gas stream into the interior and at least one second orifice for withdrawing a gas stream fed to the interior beforehand via the at least one first orifice from the interior, the surface of the shell, on its side in contact with the interior, being manufactured at least partly, in a layer thickness of at least 1 mm, from a steel which has a specific elemental composition, and in the interior, a process for continuous heterogeneously catalyzed partial dehydrogenation of at least one hydrocarbon to be dehydrogenated is carried out in a reactor which is manufactured from the steel on its side in contact with the reaction gas.
摘要翻译：壳体，其包围内部并且具有至少一个用于将至少一个气流输送到内部的第一孔口和至少一个第二孔口，用于从内部经由至少一个第一孔口预先提取送入内部的气流，壳体的与内部接触的一侧的表面至少部分地由具有特定元素组成的钢制成至少1mm的层厚度，并且在内部制造连续的工艺至少一种待脱氢烃的非均相催化的部分脱氢在反应器中进行，该反应器是由与反应气体接触的一侧的钢制成的。

7. 发明申请

US20060004229A1 Preparation of acrylic acid by heterogeneously catalyzed partial gas phase oxidation of propylene 有权
公开(公告)号：US20060004229A1
公开(公告)日：2006-01-05
申请号：US11131256
申请日：2005-05-18
申请人： Martin Dieterle , Klaus Muller-Engel , Claus Hechler , Ulrich Hammon , Armin Diefenbacher
发明人： Martin Dieterle , Klaus Muller-Engel , Claus Hechler , Ulrich Hammon , Armin Diefenbacher
IPC分类号： C07C51/25
CPC分类号： C07C51/252 , C07C45/35 , C07C57/04 , C07C47/22
摘要： The present invention relates to a process for preparing acrylic acid by two-stage heterogeneously catalyzed partial gas phase oxidation of propylene, in which the propylene source used is a preceding propane dehydrogenation and in which the first oxidation stage is operated with restricted propylene conversion, and unconverted propane and propylene present in the product gas mixture of the second partial oxidation stage are recycled substantially into the preceding propane dehydrogenation.

8. 发明授权

US07910766B2 Preparation of at least one partial oxidation and/or ammoxidation product of a hydrocarbon 有权
标题翻译：制备烃的至少一种部分氧化和/或氨氧化产物
公开(公告)号：US07910766B2
公开(公告)日：2011-03-22
申请号：US10813010
申请日：2004-03-31
申请人： Goetz-Peter Schindler , Otto Machhammer , Klaus Joachim Mueller-Engel , Claus Hechler , Jochen Petzoldt , Christoph Adami , Klaus Harth
发明人： Goetz-Peter Schindler , Otto Machhammer , Klaus Joachim Mueller-Engel , Claus Hechler , Jochen Petzoldt , Christoph Adami , Klaus Harth
IPC分类号： C07C253/08 , C07C255/06 , C07C51/16
CPC分类号： B01J23/63 , B01J23/626 , C07C45/33 , C07C45/34 , C07C45/35 , C07C51/252 , C07C253/26 , Y02P20/52 , C07C47/22 , C07C57/04 , C07C255/08
摘要： A process for preparing at least one partial oxidation and/or ammoxidation product of a hydrocarbon by partially dehydrogenating at least one saturated hydrocarbon H under heterogeneous catalysis and using the resulting product gas mixture A, which comprises the partially dehydrogenated hydrocarbon H, as such or in modified form for heterogeneously catalyzed partial oxidation and/or ammoxidation of the partially dehydrogenated hydrocarbon present in the product gas mixture A, said process including at least one mechanical separating operation inserted between the product gas mixture A and the heterogeneously catalyzed partial oxidation and/or ammoxidation.
摘要翻译：通过在非均相催化下部分脱氢至少一种饱和烃H并且使用所得到的产物气体混合物A（其包含部分脱氢的烃H）本身或其中的方法制备烃的至少一种部分氧化和/或氨氧化产物的方法产物气体混合物A中存在的部分脱氢的烃的非均相催化部分氧化和/或氨氧化的改性形式，所述方法包括插入产物气体混合物A和非均相催化的部分氧化和/或氨氧化之间的至少一个机械分离操作。

9. 发明申请

US20110038763A1 PROCESS FOR CONTINUOUS HETEROGENEOUSLY CATALYZED PARTIAL DEHYDROGENATION OF AT LEAST ONE HYDROCARBON TO BE DEHYDROGENATED 有权
标题翻译：连续异源催化部分去除脱氢脱氢酶的方法
公开(公告)号：US20110038763A1
公开(公告)日：2011-02-17
申请号：US12912127
申请日：2010-10-26
申请人： Claus Hechler , Wilhelm Ruppel , Götz-Peter Schindler , Catharina Klanner , Hans-Jürgen Bassler , Martin Dieterle , Karl-Heinrich Klappert , Klaus Joachim Müller-Engel
发明人： Claus Hechler , Wilhelm Ruppel , Götz-Peter Schindler , Catharina Klanner , Hans-Jürgen Bassler , Martin Dieterle , Karl-Heinrich Klappert , Klaus Joachim Müller-Engel
IPC分类号： B01J8/00
CPC分类号： C07C5/333 , B01J8/067 , B01J19/02 , B01J2219/0236 , C07C51/215 , C22C30/00 , C22C38/40 , Y02P20/52 , C07C11/06 , C07C11/02 , C07C57/04
摘要： A process for continuous heterogeneously catalyzed partial dehydrogenation of at least one hydrocarbon to be dehydrogenated in a reactor which is manufactured from a composite material which consists, on its side in contact with the reaction chamber, of a steel B with specific elemental composition which, on its side facing away from the reaction chamber, either directly or via an intermediate layer of copper, or of nickel, or of copper and nickel, is plated onto a steel A with specific elemental composition, and also partial oxidations of the dehydrogenated hydrocarbon and the reactor itself.
摘要翻译：在反应器中连续不均匀催化的待脱氢烃的部分脱氢的方法，该反应器由复合材料制成，该复合材料在其与反应室接触的一侧由具有特定元素组成的钢B组成，其直接或经由铜或镍或铜和镍的中间层离开反应室的一侧被镀在具有特定元素组成的钢A上，并且还将脱氢烃和反应堆本身。

10. 发明授权

US07723549B2 Process for preparing at least one target product by partial oxidation and/or ammoxidation of propylene 有权
标题翻译：通过丙烯的部分氧化和/或氨氧化制备至少一种目标产物的方法
公开(公告)号：US07723549B2
公开(公告)日：2010-05-25
申请号：US11411882
申请日：2006-04-27
申请人： Armin Diefenbacher , Claus Hechler , Christoph Adami , Martin Dieterle
发明人： Armin Diefenbacher , Claus Hechler , Christoph Adami , Martin Dieterle
IPC分类号： C07C45/28 , C07C51/25 , C07C253/24
CPC分类号： C07C51/43 , B01J23/002 , B01J23/8876 , B01J23/8885 , B01J35/0006 , B01J2523/00 , C07C45/33 , C07C45/35 , C07C51/25 , C07C51/252 , C07C253/26 , Y02P20/52 , C07C47/22 , C07C57/04 , B01J2523/17 , B01J2523/55 , B01J2523/68 , B01J2523/69 , C07C255/08 , B01J2523/36
摘要： A process for preparing at least one target product by partial oxidation and/or ammoxidation of propylene, in which the propylene source used is a propane dehydrogenation, the propane used therein being obtained by a rectificative prepurification of crude propane.
摘要翻译：通过丙烯的部分氧化和/或氨氧化制备至少一种目标产物的方法，其中使用的丙烯源是丙烷脱氢，其中使用的丙烷是通过粗丙烷的精馏预纯化获得的。

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