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1. 发明授权

US07253308B1 Method for catalytic phase oxidation to (meth) acrolein and/or (meth) acrylic acid 有权
标题翻译：催化相氧化成（甲基）丙烯醛和/或（甲基）丙烯酸的方法
公开(公告)号：US07253308B1
公开(公告)日：2007-08-07
申请号：US10110229
申请日：2000-11-03
申请人： Claus Hechler , Otto Machhammer , Gerhard Olbert , Uwe Stabel , Peter Zehner
发明人： Claus Hechler , Otto Machhammer , Gerhard Olbert , Uwe Stabel , Peter Zehner
IPC分类号： C07C51/16 , C07B41/00
CPC分类号： B01J19/249 , B01J8/0285 , B01J2208/0015 , B01J2208/022 , B01J2219/0002 , B01J2219/2453 , B01J2219/2456 , B01J2219/2462 , B01J2219/2474 , B01J2219/2479 , B01J2219/2481 , C07C45/33 , C07C45/35 , C07C45/37 , F28D9/0006 , F28D9/0031 , F28F2250/104
摘要： A process for the continuous gas-phase oxidation of C3- and C4-precursors to (meth)acrolein and/or (meth)acrylic acid in the presence of a catalyst in a reactor which has a feed for the reaction mixture at one reactor end and removal of the reaction mixture at the opposite reactor end and which is equipped with means, arranged in the interior of the reactor, for removing the heat of reaction, through which means a heat exchange composition flows and which means are in the form of heat exchanger plates, is proposed.
摘要翻译：一种将C 3 - 和C 4 - - 前体连续气相氧化成（甲基）丙烯醛和/或（甲基）丙烯酸的方法，在反应器中的催化剂，其在一个反应器端具有用于反应混合物的进料并在相对的反应器端除去反应混合物，并且装备有设置在反应器内部的装置，用于除去反应热，通过这意味着热交换组合物流动，并且哪种装置是热交换器板的形式。

2. 发明授权

US06624315B2 Method of gas phase catalytic oxidation to give maleic acid anhydride 失效
标题翻译：气相催化氧化法得到马来酸酐
公开(公告)号：US06624315B2
公开(公告)日：2003-09-23
申请号：US09936347
申请日：2001-09-11
申请人： Peter Zehner , Otto Machhammer , Claus Hechler , Alexander Weck , Gerhard Olbert , Uwe Stabel
发明人： Peter Zehner , Otto Machhammer , Claus Hechler , Alexander Weck , Gerhard Olbert , Uwe Stabel
IPC分类号： C07D30760
CPC分类号： B01J35/04 , B01J8/0285 , B01J19/249 , B01J2208/0015 , B01J2208/022 , B01J2219/0002 , B01J2219/2453 , B01J2219/2454 , B01J2219/2455 , B01J2219/2462 , B01J2219/2464 , B01J2219/2479 , B01J2219/2495 , B01J2219/2497 , B01J2219/2498 , B01J2219/32475 , C07C51/215 , C07C57/145
摘要： A process for the preparation of maleic anhydride by heterogeneously catalyzed gas-phase oxidation in a reactor with feed for the reaction mixture at one end of the reactor and discharge of the product mixture at the opposite end of the reactor, and with devices for dissipating the heat of reaction which are arranged in the reactor interior and through which a heat-exchange medium flows and which are designed as heat-exchanger plates.
摘要翻译：在反应器中通过异构催化气相氧化制备马来酸酐的方法，其中反应器的一端具有反应混合物的进料并在反应器的另一端排出产物混合物，以及用于消散反应器的装置布置在反应器内部并通过热交换介质流动并被设计为热交换器板的反应热。

3. 发明申请

US20100022785A1 METHOD FOR PRODUCING PHTHALIC ANHYDRIDE 有权
标题翻译：生产苯基非对映体的方法
公开(公告)号：US20100022785A1
公开(公告)日：2010-01-28
申请号：US11722449
申请日：2005-12-21
申请人： Claus Hechler , Gerhard Olbert
发明人： Claus Hechler , Gerhard Olbert
IPC分类号： C07D307/89
CPC分类号： C07C51/265 , B01J8/0488 , B01J8/0496 , B01J19/249 , B01J2208/0015 , B01J2219/00155 , B01J2219/2453 , B01J2219/2459 , B01J2219/2462 , B01J2219/2481 , B01J2219/2485 , C07C51/313 , C07C63/16
摘要： Processes comprising: (a) providing a reactant comprising a component selected from the group consisting of o-xylene, naphthalene and mixtures thereof, and a gas comprising oxygen; (b) reacting the reactant and the gas in a reaction system, in the presence of a catalyst, to form phthalic anhydride; wherein the reaction system comprises: (i) at least two reaction zones, each reaction zone cooled with a coolant; and (ii) an intermediate cooling zone disposed between a first of the at least two reaction zones and a second of the at least two reaction zones; and wherein the coolant entering the first of the at least two reaction zones has a temperature which is more than 20° C. higher than a temperature of the coolant entering the second of the at leas two reaction zones.
摘要翻译：方法包括：（a）提供包含选自邻二甲苯，萘及其混合物的组分的反应物和包含氧的气体; （b）使反应物和气体在反应体系中，在催化剂存在下反应，形成邻苯二甲酸酐; 其中所述反应体系包括：（i）至少两个反应区，每个反应区用冷却剂冷却; 和（ii）设置在所述至少两个反应区中的第一个和所述至少两个反应区中的第二个之间的中间冷却区; 并且其中进入所述至少两个反应区中的第一个的冷却剂的温度比进入所述两个反应区中的第二个的冷却剂的温度高大于20℃。

4. 发明申请

US20050020851A1 Preparation of (meth)acrolein and/or (meth)acrylic acid by heterogeneously catalyzed partial oxidation of C3 and/or C4 precursor compounds in a reactor having thermoplate modules 有权
标题翻译：在具有热电板模块的反应器中通过C3和/或C4前体化合物的非均相催化部分氧化制备（甲基）丙烯醛和/或（甲基）丙烯酸
公开(公告)号：US20050020851A1
公开(公告)日：2005-01-27
申请号：US10889081
申请日：2004-07-13
申请人： Gerhard Olbert , Claus Hechler
发明人： Gerhard Olbert , Claus Hechler
IPC分类号： B01J19/24 , C07C45/35 , C07C51/215 , C07C51/25 , C07C51/16
CPC分类号： C07C51/215 , B01J19/249 , B01J2208/0015 , B01J2219/2453 , B01J2219/2458 , B01J2219/2459 , B01J2219/2462 , B01J2219/2474 , B01J2219/2481 , B01J2219/2486 , B01J2219/2493 , B01J2219/2495 , B01J2219/2496 , B01J2219/2497 , B01J2219/2498 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A process is proposed for partial oxidation oxidation in the gas phase of C3 and/or C4 precursor compounds to (meth)acrolein and/or (meth)acrylic acid in the presence of a heterogeneous particulate catalyst in a reactor having one or more cuboidal thermoplate modules (1) which are each formed from two or more rectangular thermoplates (2) arranged parallel to each other while in each case leaving a gap (3) which can be filled with the heterogeneous particulate catalyst and is flowed through by the fluid reaction mixture; the heat of reaction being absorbed by a heat carrier which flows through the thermoplates (2) and thus at least partly evaporating, and also having a predominantly cylindrical shell (4, 15, 16) which releases the pressure at the thermoplate modules, completely surrounds them and comprises a cylinder jacket (4) and hoods (15, 16) which seal it at both ends and whose longitudinal axis is aligned parallel to the plane of the thermoplates (2), and also having one or more sealing elements (7, 23) which are arranged in such a way that the fluid reaction mixture, apart from flowing through the reactor interior spaces bounded by the hoods (15, 16), only flows through the gap (3).
摘要翻译：在具有一个或多个立方形热电板的反应器中，在非均相颗粒催化剂存在下，提出在C3和/或C4前体化合物的气相中部分氧化氧化成（甲基）丙烯醛和/或（甲基）丙烯酸的方法模块（1）各自由彼此平行布置的两个或更多个矩形热板（2）形成，而在每个情况下留下间隙（3），所述间隙可以填充有异相颗粒催化剂并且被流体反应混合物流过 ; 反应热被被流经热板（2）并因此至少部分蒸发的热载体吸收，并且还具有释放热电板模块上的压力的主要为圆柱形的壳体（4,15,16），完全包围并且包括气缸套（4）和在两端密封其并且其纵向轴线平行于热板（2）的平面对准的罩（15,16），并且还具有一个或多个密封元件（7， 23），其被布置成使得流体反应混合物除了流过由罩（15,16）限定的反应器内部空间外，仅流过间隙（3）。

5. 发明授权

US07268254B2 Preparation of (meth)acrolein and/or (meth)acrylic acid by heterogeneously catalyzed partial oxidation of C3 and/or C4 precursor compounds in a reactor having thermoplate modules 有权
标题翻译：在具有热电板模块的反应器中通过C3和/或C4前体化合物的非均相催化部分氧化制备（甲基）丙烯醛和/或（甲基）丙烯酸
公开(公告)号：US07268254B2
公开(公告)日：2007-09-11
申请号：US10889081
申请日：2004-07-13
申请人： Gerhard Olbert , Claus Hechler
发明人： Gerhard Olbert , Claus Hechler
IPC分类号： C07C57/02 , C07C45/00
CPC分类号： C07C51/215 , B01J19/249 , B01J2208/0015 , B01J2219/2453 , B01J2219/2458 , B01J2219/2459 , B01J2219/2462 , B01J2219/2474 , B01J2219/2481 , B01J2219/2486 , B01J2219/2493 , B01J2219/2495 , B01J2219/2496 , B01J2219/2497 , B01J2219/2498 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A process is proposed for partial oxidation oxidation in the gas phase of C3 and/or C4 precursor compounds to (meth)acrolein and/or (meth)acrylic acid in the presence of a heterogeneous particulate catalyst in a reactor having one or more cuboidal thermoplate modules (1) which are each formed from two or more rectangular thermoplates (2) arranged parallel to each other while in each case leaving a gap (3) which can be filled with the heterogeneous particulate catalyst and is flowed through by the fluid reaction mixture; the heat of reaction being absorbed by a heat carrier which flows through the thermoplates (2) and thus at least partly evaporating, and also having a predominantly cylindrical shell (4, 15, 16) which releases the pressure at the thermoplate modules, completely surrounds them and comprises a cylinder jacket (4) and hoods (15, 16) which seal it at both ends and whose longitudinal axis is aligned parallel to the plane of the thermoplates (2), and also having one or more sealing elements (7, 23) which are arranged in such a way that the fluid reaction mixture, apart from flowing through the reactor interior spaces bounded by the hoods (15, 16), only flows through the gap (3).
摘要翻译：在具有一个或多个立方形热电板的反应器中，在非均相颗粒催化剂存在下，提出在C3和/或C4前体化合物的气相中部分氧化氧化成（甲基）丙烯醛和/或（甲基）丙烯酸的方法模块（1）各自由彼此平行布置的两个或更多个矩形热板（2）形成，而在每个情况下留下间隙（3），所述间隙可以填充有异相颗粒催化剂并且被流体反应混合物流过 ; 反应热被被流经热板（2）并因此至少部分蒸发的热载体吸收，并且还具有释放热电板模块上的压力的主要为圆柱形的壳体（4,15,16），完全包围并且包括气缸套（4）和在两端密封其并且其纵向轴线平行于热板（2）的平面对准的罩（15,16），并且还具有一个或多个密封元件（7， 23），其被布置成使得流体反应混合物除了流过由罩（15,16）限定的反应器内部空间外，仅流过间隙（3）。

6. 发明授权

US07410622B2 Reactor for partial oxidations having thermoplate modules 有权
标题翻译：具有热电板模块的部分氧化反应器
公开(公告)号：US07410622B2
公开(公告)日：2008-08-12
申请号：US10888977
申请日：2004-07-13
申请人： Gerhard Olbert , Claus Hechler
发明人： Gerhard Olbert , Claus Hechler
IPC分类号： B01J19/00 , C07C229/00
CPC分类号： B01J19/32 , B01J19/249 , B01J2219/2453 , B01J2219/2459 , B01J2219/2462 , B01J2219/2469 , B01J2219/2481 , B01J2219/2497 , B01J2219/2498 , B01J2219/3221 , B01J2219/32213 , B01J2219/32227 , B01J2219/32268 , B01J2219/32275 , B01J2219/32466 , B01J2219/32475 , B01J2219/3306 , C07C45/35 , C07C51/215 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A reactor is proposed for partial oxidations of a fluid reaction mixture in the presence of a heterogeneous particulate catalyst, comprising one or more cuboidal thermoplate modules (1) which are each formed from two or more rectangular thermoplates (2) arranged parallel to each other while in each case leaving a gap (3) which can be filled with the heterogeneous particulate catalyst and is flowed through by the fluid reaction mixture; the heat of reaction being absorbed by a heat carrier which flows through the thermoplates (2) and thus at least partly evaporates, and also having a predominantly cylindrical shell (4, 15, 16) which releases the pressure at the thermoplate modules, completely surrounds them and comprises a cylinder jacket (4) and hoods (15, 16) which seal it at both ends and whose longitudinal axis is aligned parallel to the plane of the thermoplates (2), and also having one or more sealing elements (7, 23) which are arranged in such a way that the fluid reaction mixture, apart from flowing through the reactor interior spaces bounded by the hoods (15, 16), only flows through the gap (3).
摘要翻译：提出了一种反应器，用于在非均相颗粒催化剂存在下的流体反应混合物的部分氧化，包括一个或多个立方形热电板模块（1），每个热电板模块（1）由两个或更多个彼此平行布置的矩形热电偶（2）形成，同时在每种情况下留下可以用异质颗粒催化剂填充并被流体反应混合物流过的间隙（3）; 反应热被被热板（2）流过并因此至少部分蒸发的热载体吸收，并且还具有释放热电板模块上的压力的主要为圆柱形的壳（4,15,16），完全包围并且包括气缸套（4）和在两端密封其并且其纵向轴线平行于热板（2）的平面对准的罩（15,16），并且还具有一个或多个密封元件（7， 23），其被布置成使得流体反应混合物除了流过由罩（15,16）限定的反应器内部空间外，仅流过间隙（3）。

7. 发明授权

US07214821B2 Preparation of (meth)acrolein and/or (meth)acrylic acid by heterogeneously catalyzed partial oxidation of C3 and/or C4 precursor compounds 有权
标题翻译：通过C3和/或C4前体化合物的非均相催化部分氧化制备（甲基）丙烯醛和/或（甲基）丙烯酸
公开(公告)号：US07214821B2
公开(公告)日：2007-05-08
申请号：US11019160
申请日：2004-12-23
申请人： Claus Hechler , Gerhard Olbert , Dietmar Loewen
发明人： Claus Hechler , Gerhard Olbert , Dietmar Loewen
IPC分类号： C07C229/00
CPC分类号： C07C45/35 , B01J8/0242 , B01J8/0285 , B01J19/249 , B01J2208/0015 , B01J2219/00063 , B01J2219/00155 , B01J2219/2453 , B01J2219/2459 , B01J2219/2462 , B01J2219/2481 , B01J2219/2485 , C07C51/21 , C07C47/22 , C07C57/04
摘要： A process is proposed for preparing (meth)acrolein and/or (meth)acrylic acid by partially oxidizing C3 and/or C4 precursor compounds in the gas phase in the presence of a heterogeneous particulate catalyst, in a reactor having two or more thermoplates (1) arranged vertically and parallel to each other while in each case leaving a gap (2), the heterogeneous particulate catalyst being installed in the gaps (2) and the gaseous reaction mixture being passed through the gaps (2), which comprises monitoring, controlling and/or regulating the process by selecting as a monitoring, control and/or regulation parameter one or more temperatures which are measured in one or more gaps (2), at one or more measurement points which are distributed over the height of each gap (2).
摘要翻译：提出了一种制备（甲基）丙烯醛和/或（甲基）丙烯酸的方法，其通过在气相中部分氧化C 3 3和/或C 4 H 3前体化合物在具有两个或更多个彼此垂直且平行布置的热板（1）的反应器中存在非均相颗粒催化剂，而在每种情况下留下间隙（2）时，异质颗粒催化剂安装在间隙（2）和气态反应混合物通过间隙（2），其包括通过选择作为监测，控制和/或调节参数的监测，控制和/或调节过程在一个或多个间隙（2）中测量的一个或多个温度，在一个或多个分布在每个间隙（2）的高度上的测量点。

8. 发明申请

US20050158217A1 Monitoring, control and/or regulation of reactions of a fluid reaction mixture in a reactor having thermoplates 审中-公开
标题翻译：在具有热板的反应器中监测，控制和/或调节流体反应混合物的反应
公开(公告)号：US20050158217A1
公开(公告)日：2005-07-21
申请号：US11019193
申请日：2004-12-23
申请人： Gerhard Olbert , Claus Hechler , Dietmar Loewen
发明人： Gerhard Olbert , Claus Hechler , Dietmar Loewen
IPC分类号： B01J8/00 , B01J8/02 , B01J19/00 , B01J19/24 , G05D23/00
CPC分类号： B01J19/249 , B01J8/001 , B01J8/0285 , B01J19/0013 , B01J2208/00061 , B01J2208/0015 , B01J2208/00628 , B01J2208/00964 , B01J2208/00973 , B01J2219/00063 , B01J2219/002 , B01J2219/2453 , B01J2219/2459 , B01J2219/2462 , B01J2219/2464 , B01J2219/2481 , B01J2219/2486 , B01J2219/2497
摘要： A process is proposed for monitoring, controlling and/or regulating reactions of a fluid reaction mixture in the presence of a heterogeneous particulate catalyst, in a reactor having two or more thermoplates (1) arranged vertically and parallel to each other while in each case leaving a gap (2), the heterogeneous particulate catalyst being installed in the gaps (2) and the fluid reaction mixture being passed through the gaps (2), which comprises selecting as a regulation signal the temperature which is determined in one or more gaps (2), at two or more measurement points which are distributed over the height of each gap (2).
摘要翻译：在具有两个或更多个垂直且彼此平行布置的热电极板（1）的反应器中，提出了用于监测，控制和/或调节流体反应混合物在异质颗粒催化剂存在下的反应的方法，同时在每种情况下离开间隙（2），所述异质颗粒催化剂安装在所述间隙（2）中并且所述流体反应混合物通过所述间隙（2），所述间隙包括选择在一个或多个间隙中确定的温度作为调节信号 2），在两个或更多个分布在每个间隙（2）的高度上的测量点。

9. 发明授权

US07772410B2 Method for producing phthalic anhydride 有权
标题翻译：邻苯二甲酸酐的制造方法
公开(公告)号：US07772410B2
公开(公告)日：2010-08-10
申请号：US11722449
申请日：2005-12-21
申请人： Claus Hechler , Gerhard Olbert
发明人： Claus Hechler , Gerhard Olbert
IPC分类号： C07D307/89
CPC分类号： C07C51/265 , B01J8/0488 , B01J8/0496 , B01J19/249 , B01J2208/0015 , B01J2219/00155 , B01J2219/2453 , B01J2219/2459 , B01J2219/2462 , B01J2219/2481 , B01J2219/2485 , C07C51/313 , C07C63/16
摘要： Processes comprising: (a) providing a reactant comprising a component selected from the group consisting of o-xylene, naphthalene and mixtures thereof, and a gas comprising oxygen; (b) reacting the reactant and the gas in a reaction system, in the presence of a catalyst, to form phthalic anhydride; wherein the reaction system comprises: (i) at least two reaction zones, each reaction zone cooled with a coolant; and (ii) an intermediate cooling zone disposed between a first of the at least two reaction zones and a second of the at least two reaction zones; and wherein the coolant entering the first of the at least two reaction zones has a temperature which is more than 20° C. higher than a temperature of the coolant entering the second of the at leas two reaction zones.
摘要翻译：方法包括：（a）提供包含选自邻二甲苯，萘及其混合物的组分的反应物和包含氧的气体; （b）使反应物和气体在反应体系中，在催化剂存在下反应，形成邻苯二甲酸酐; 其中所述反应体系包括：（i）至少两个反应区，每个反应区用冷却剂冷却; 和（ii）设置在所述至少两个反应区中的第一个和所述至少两个反应区中的第二个之间的中间冷却区; 并且其中进入所述至少两个反应区中的第一个的冷却剂的温度比进入所述两个反应区中的第二个的冷却剂的温度高大于20℃。

10. 发明申请

US20050159618A1 Preparation of (meth)acrolein and/or (meth)acrylic acid by heterogeneously catalyzed partial oxidation of C3 and/or C4 precursor compounds 有权
标题翻译：通过C3和/或C4前体化合物的非均相催化部分氧化制备（甲基）丙烯醛和/或（甲基）丙烯酸
公开(公告)号：US20050159618A1
公开(公告)日：2005-07-21
申请号：US11019160
申请日：2004-12-23
申请人： Claus Hechler , Gerhard Olbert , Dietmar Lowen
发明人： Claus Hechler , Gerhard Olbert , Dietmar Lowen
IPC分类号： C07C45/35 , C07C51/16 , C07C51/21 , C07C51/235
CPC分类号： C07C45/35 , B01J8/0242 , B01J8/0285 , B01J19/249 , B01J2208/0015 , B01J2219/00063 , B01J2219/00155 , B01J2219/2453 , B01J2219/2459 , B01J2219/2462 , B01J2219/2481 , B01J2219/2485 , C07C51/21 , C07C47/22 , C07C57/04
摘要： A process is proposed for preparing (meth)acrolein and/or (meth)acrylic acid by partially oxidizing C3 and/or C4 precursor compounds in the gas phase in the presence of a heterogeneous particulate catalyst, in a reactor having two or more thermoplates (1) arranged vertically and parallel to each other while in each case leaving a gap (2), the heterogeneous particulate catalyst being installed in the gaps (2) and the gaseous reaction mixture being passed through the gaps (2), which comprises monitoring, controlling and/or regulating the process by selecting as a monitoring, control and/or regulation parameter one or more temperatures which are measured in one or more gaps (2), at one or more measurement points which are distributed over the height of each gap (2).
摘要翻译：提出了一种制备（甲基）丙烯醛和/或（甲基）丙烯酸的方法，其通过在气相中部分氧化C 3和/或C 4 H 3前体化合物在具有两个或更多个彼此垂直且平行布置的热板（1）的反应器中存在非均相颗粒催化剂，而在每种情况下留下间隙（2）时，异质颗粒催化剂安装在间隙（2）和气态反应混合物通过间隙（2），其包括通过选择作为监测，控制和/或调节参数的监测，控制和/或调节过程在一个或多个间隙（2）中测量的一个或多个温度，在一个或多个分布在每个间隙（2）的高度上的测量点。

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