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    • 5. 发明授权
    • Thermosetting resin composition comprising dicyanamide and polyvalent
imide
    • 包含二氰胺和多价酰亚胺的热固性树脂组合物
    • US4482703A
    • 1984-11-13
    • US435766
    • 1982-10-20
    • Akio TakahashiTakeshi ShimazakiMotoyo WajimaHirosada Morishita
    • Akio TakahashiTakeshi ShimazakiMotoyo WajimaHirosada Morishita
    • C08G73/00C08G73/06C08G73/12C09D179/08C08G73/10
    • C08G73/12
    • A thermosetting resin composition comprises (A) at least one dicyanamide compound and (B) at least one polyvalent imide having one or more unsaturated bonds and, if necessary (C) at least one polymerizable compound of epoxy compounds, phenolic compounds and triallyl isocyanurate compounds. A thermosetting prepolymer can be obtained by subjecting the composition to a preliminary reaction with heating to the B stage and this prepolymer can give a cured product having excellent heat resistance of class C and flexibility. An exemplary composition containing 60 parts by wt. of 4,4'-dicyanomidodiphenylmethane and 40 parts by wt. of N,N'-4,4'-diphenylmethane bismaleimide dissolved in methyl Cellosolve is reacted at 70.degree. to 110.degree. C. for about 40 minutes to obtain a prepolymer soluble in methyl ethyl ketone. This prepolymer when admixed with 2-ethyl-4-methyl-imidazole and after removal of the methyl cellusolve will form an insoluble and infusible cured product upon heating at temperatures on the order of 170.degree. to 200.degree. C. for about 80 minutes. The resin composition when admixed with a solvent, is useful for impregnation and when used as a powder, it is useful as a molding resin.
    • 热固性树脂组合物包含(A)至少一种二氰酰胺化合物和(B)至少一种具有一个或多个不饱和键的多价酰亚胺,并且如果需要(C)至少一种环氧化合物的可聚合化合物,酚类化合物和三烯丙基异氰脲酸酯化合物 。 通过将加热至B阶段的组合物进行预反应,可以获得热固性预聚物,该预聚物可以得到具有优异的C级耐热性和柔软性的固化产物。 含有60重量份的示例性组合物 的4,4'-二氰基二苯基甲烷和40重量份。 溶解在甲基溶纤剂中的N,N'- 4,4'-二苯基甲烷双马来酰亚胺在70〜110℃下反应约40分钟,得到可溶于甲基乙基酮的预聚物。 当与2-乙基-4-甲基 - 咪唑混合并且除去甲基溶液后,该预聚物将在约170℃至200℃的温度下加热约80分钟时形成不溶性和不可渗透的固化产物。 当与溶剂混合时,树脂组合物可用于浸渍,并且当用作粉末时,其可用作模制树脂。
    • 6. 发明授权
    • Bismide-ether compounds, compositions thereof, and method of producing
same
    • 二苯醚类化合物及其组合物及其制备方法
    • US4296219A
    • 1981-10-20
    • US5233
    • 1979-01-22
    • Akio TakahashiYutaka ItohMotoyo WajimaHirosada MorishitaAkio Nishikawa
    • Akio TakahashiYutaka ItohMotoyo WajimaHirosada MorishitaAkio Nishikawa
    • C07D207/44C07D207/448C08G73/12
    • C07D207/448C08G73/121
    • A bisimide-ether compound having the general formula is obtained by reacting an ethylenically unsaturated dicarboxylic acid anhydride, a diamine compound and a phenolic compound having in the molecule at least two hydroxyl groups, or by reacting a prepolymer of the anhydride and diamine compound with the phenolic compound: ##STR1## wherein R.sub.1 is a group containing at least two carbon atoms, R.sub.2 is a group containing at least two carbon atoms, R'.sub.2 is a group containing at least two carbon atoms and a carbon-carbon double bond, R.sub.3 is an aromatic group, the nitrogen atoms of the imide rings being directly connected to different carbon atoms of the group R.sub.1, the carbonyl groups of the imide rings being directly connected to different carbon atoms of the group R.sub.2 or R'.sub.2, the oxygen atoms between the groups R.sub.2 and R.sub.3 being directly connected to an aromatic nucleus of the group R.sub.3, and n is an integer of zero, one or more than 1.
    • 通过使烯键式不饱和二羧酸酐,二胺化合物和分子中至少两个羟基的酚类化合物反应,或者使酸酐与二胺化合物的预聚物与 酚类化合物:其中R1是含有至少两个碳原子的基团,R2是含有至少两个碳原子的基团,R'2是含有至少两个碳原子的基团和碳 - 碳双键,R3 是芳族基团,酰亚胺环的氮原子直接连接到基团R1的不同碳原子上,酰亚胺环的羰基直接连接到基团R 2或R'2的不同碳原子上,氧原子 在基团R 2和R 3直接连接到基团R 3的芳香环上,且n是0,1或1以上的整数。