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1. 发明授权

US06183558B2 Method and apparatus for producing molecular film 有权
标题翻译：生产分子膜的方法和装置
公开(公告)号：US06183558B2
公开(公告)日：2001-02-06
申请号：US09294297
申请日：1999-04-19
申请人： Tadashi Otake , Norihisa Mino , Tohru Nakagawa , Mamoru Soga , Kazufumi Ogawa , Takaiki Nomura , Yasuo Takebe
发明人： Tadashi Otake , Norihisa Mino , Tohru Nakagawa , Mamoru Soga , Kazufumi Ogawa , Takaiki Nomura , Yasuo Takebe
IPC分类号： B05C108
CPC分类号： B82Y30/00 , B05D1/283 , B05D3/0486 , B82Y40/00
摘要： A method for forming a molecular film includes the steps of: coating a surface of a substrate having active hydrogen atoms on its surface with a coating solution containing a silane-based compound having at least one reactive group selected from the group consisting of a chloro group, an alkoxy group and an isocyanate group; and effecting an elimination reaction between the active hydrogen atoms on the surface of the substrate and reactive groups of the silane-based compound, thereby covalently bonding the silane-based compounds to the surface of the substrate. The substrate is supplied to a chamber in which an atmosphere is maintained at a low water vapor density. The surface of the substrate is coated with a coating solution containing the silane-based compound and a solvent by using a transfer element. A dehydrochlorination reaction is effected between the active hydrogen atoms and the chloro groups of the silane-based compounds. Thereafter, any coating solution containing unreacted silane-based compounds after coating is removed inside or outside the chamber.
摘要翻译：形成分子膜的方法包括以下步骤：用包含具有至少一个选自氯基团的反应性基团的硅烷基化合物的涂布溶液在其表面上涂覆具有活性氢原子的基材的表面，烷氧基和异氰酸酯基; 并且进行基板表面上的活性氢原子与硅烷类化合物的反应性基团之间的消除反应，从而将硅烷类化合物共价键合到基板的表面。将基板供给到气氛保持在低水蒸汽密度的室中。通过使用转印元件，将含有硅烷系化合物和溶剂的涂布液涂布在基材的表面上。在活性氢原子和硅烷基化合物的氯基之间进行脱氯化氢反应。此后，在室内或室外除去涂布后含有未反应的硅烷类化合物的任何涂布溶液。

2. 发明授权

US5948476A Method and apparatus for producing molecular film 失效
标题翻译：生产分子膜的方法和装置
公开(公告)号：US5948476A
公开(公告)日：1999-09-07
申请号：US964471
申请日：1997-11-04
申请人： Tadashi Otake , Norihisa Mino , Tohru Nakagawa , Mamoru Soga , Kazufumi Ogawa , Takaiki Nomura , Yasuo Takebe
发明人： Tadashi Otake , Norihisa Mino , Tohru Nakagawa , Mamoru Soga , Kazufumi Ogawa , Takaiki Nomura , Yasuo Takebe
IPC分类号： B05D1/28 , B05D3/04
CPC分类号： B82Y30/00 , B05D1/283 , B05D3/0486 , B82Y40/00
摘要： A method for forming a molecular film includes the steps of: coating a surface of a substrate having active hydrogen atoms on its surface with a coating solution containing a silane-based compound having at least one reactive group selected from the group consisting of a chloro group, an alkoxy group and an isocyanate group; and effecting an elimination reaction between the active hydrogen atoms on the surface of the substrate and reactive groups of the silane-based compound, thereby covalently bonding the silane-based compounds to the surface of the substrate. The substrate is supplied to a chamber in which an atmosphere is maintained at a low water vapor density. The surface of the substrate is coated with a coating solution containing the silane-based compound and a solvent by using a transfer element. A dehydrochlorination reaction is effected between the active hydrogen atoms and the chloro groups of the silane-based compounds. Thereafter, any coating solution containing unreacted silane-based compounds after coating is removed inside or outside the chamber.
摘要翻译：形成分子膜的方法包括以下步骤：用包含具有至少一个选自氯基团的反应性基团的硅烷基化合物的涂布溶液在其表面上涂覆具有活性氢原子的基材的表面，烷氧基和异氰酸酯基; 并且进行基板表面上的活性氢原子与硅烷类化合物的反应性基团之间的消除反应，从而将硅烷类化合物共价键合到基板的表面。将基板供给到气氛保持在低水蒸汽密度的室中。通过使用转印元件，将含有硅烷系化合物和溶剂的涂布液涂布在基材的表面上。在活性氢原子和硅烷基化合物的氯基之间进行脱氯化氢反应。此后，在室内或室外除去涂布后含有未反应的硅烷类化合物的任何涂布溶液。

3. 发明授权

US5868827A Chemically bonding material and method for manufacturing the same 失效
标题翻译：化学结合材料及其制造方法
公开(公告)号：US5868827A
公开(公告)日：1999-02-09
申请号：US988645
申请日：1997-12-11
申请人： Norihisa Mino , Kazufumi Ogawa , Yasuo Takebe , Tadashi Otake
发明人： Norihisa Mino , Kazufumi Ogawa , Yasuo Takebe , Tadashi Otake
IPC分类号： C07F7/10 , C07F7/12 , C07F7/18 , C09D183/04 , C09D183/06 , C09D183/07
CPC分类号： C07F7/12 , C07F7/10 , C07F7/1836 , C07F7/184
摘要： A method for manufacturing a chemically bonding material comprising the steps of: mixing a compound expressed by a general formula ABX.sub.n (Formula 1), wherein A shows a group including carbon, B indicates Si, Ge, Sn, Ti or Zr, X is a hydrolyzable group and n indicates 1, 2 or 3, and at least one kind of compound not including active hydrogen groups in a dry atmosphere having a water vapor density of 0.0076 kg/m.sup.3 or less; and storing the same in a dry atmosphere having a water vapor density of 0.0076 kg/m.sup.3 or less. A coating solution including compounds that are easily hydrolyzed is stored in a dry state so that the material is not deactivated before reacting with a substrate.
摘要翻译：一种化学键合材料的制造方法，包括以下步骤：将由通式ABXn（式1）表示的化合物混合，其中A表示包含碳的基团，B表示Si，Ge，Sn，Ti或Zr，X为水解性基团，n表示1,2或3，并且在水蒸汽密度为0.0076kg / m 3以下的干燥气氛中含有至少一种不包括活性氢基团的化合物; 并将其储存在水蒸汽密度为0.0076kg / m 3以下的干燥气氛中。包含容易水解的化合物的涂布溶液以干燥状态储存，使得材料在与基材反应之前不失活。

4. 发明授权

US06333074B1 Water repellent coating film, method and apparatus for manufacturing the same, and water repellent coating material composition 失效
标题翻译：防水涂膜，其制造方法和装置以及防水涂料组合物
公开(公告)号：US06333074B1
公开(公告)日：2001-12-25
申请号：US09480252
申请日：2000-01-11
申请人： Kazufumi Ogawa , Yasuo Takebe , Norihisa Mino
发明人： Kazufumi Ogawa , Yasuo Takebe , Norihisa Mino
IPC分类号： B05D300
CPC分类号： B82Y30/00 , B05D1/185 , B82Y40/00 , F28F17/005 , F28F2245/02 , Y10T428/2936 , Y10T428/2995 , Y10T428/31663 , Y10T428/31678
摘要： By forming a film that comprises a microcrystalline polymer having at least a fluorocarbon group and has a rough surface on a surface of a base material, super-water-repellency is provided, the dew condensation water of an air conditioner, for example, can be easily removed, and the freezing of the fin of the heat exchanger can be prevented. A fin that is made of aluminium is coated with a solution for forming a coating film, in which CF3(CF2)7—(CH2)2—SiCl3 is diluted with nonaqueous cyclohexamethyl trisiloxane at a concentration of 10 vol. % for preparation, to a thickness of 1 to 10 &mgr;m by a brush, and then the cyclohexamethyl trisiloxane is vaporized in an atmosphere having a relative humidity of about 75% at room temperature. CF3(CF2)7—(CH2)2—SiCl3 that remained on the fin is rapidly hydrolyzed with the moisture in the atmosphere, and the moisture in air and a —SiCl3 group dehydrochlorinated to form a microcrystalline polymer on the fin. As a result, a coating film having a surface roughness in the range of 1 to 40 &mgr;m and a contact angle of about 171° to water can be formed.
摘要翻译：通过形成包含至少具有碳氟化合物基团并且在基材表面上具有粗糙表面的微晶聚合物的膜，提供超疏水性，例如空调的结露水可以是容易地除去，并且可以防止热交换器的翅片的冻结。用铝制成的翅片涂覆有形成涂膜的溶液，其中CF 3（CF 2）7 - （CH 2）2 -SiCl 3用10体积浓度的非水性环己甲基三硅氧烷稀释。制备时，用刷子将其厚度设定为1〜10μm，然后在室温下在相对湿度为约75％的气氛中将环己甲基三硅氧烷蒸发。残留在翅片上的CF 3（CF 2）7 - （CH 2）2 -SiCl 3随着大气中的水分，空气中的水分和-SiCl 3基团脱氯化氢而迅速水解，从而在翅片上形成微晶聚合物。结果，可以形成表面粗糙度为1〜40μm，与水接触角为约171°的涂膜。

5. 发明授权

US06495247B1 Functional member having molecular layer on its surface and method of producing the same 有权
标题翻译：其表面具有分子层的功能元件及其制造方法
公开(公告)号：US06495247B1
公开(公告)日：2002-12-17
申请号：US09125622
申请日：1998-08-21
申请人： Hiroaki Takezawa , Tadashi Otake , Yasuo Takebe , Hiroshi Onishi , Norihisa Mino , Toru Shiino
发明人： Hiroaki Takezawa , Tadashi Otake , Yasuo Takebe , Hiroshi Onishi , Norihisa Mino , Toru Shiino
IPC分类号： B32B516
CPC分类号： B82Y30/00 , B05D1/185 , B82Y40/00 , Y10T428/268 , Y10T428/269 , Y10T428/31678 , Y10T428/31681
摘要： A functional member having a molecular layer on its surface, wherein the molecular layer is formed through a coordinate bond, and the coordinate bond is a multidentate bond in which at least one molecule is bonded to one metallic atom of the member and two or more ligands of the molecule are coordinated.
摘要翻译：在其表面具有分子层的功能性构件，其中所述分子层通过配位键形成，所述配位键是多元键，其中至少一个分子与所述成员的一个金属原子键合，以及两个或更多个配体的分子是协调的。

6. 发明授权

US6042948A Water repellent coating film, method and apparatus for manufacturing the same, and water repellent coating material composition 失效
标题翻译：防水涂膜，其制造方法和装置以及防水涂料组合物
公开(公告)号：US6042948A
公开(公告)日：2000-03-28
申请号：US792133
申请日：1997-01-31
申请人： Kazufumi Ogawa , Yasuo Takebe , Norihisa Mino
发明人： Kazufumi Ogawa , Yasuo Takebe , Norihisa Mino
IPC分类号： B05D1/18 , F28F17/00 , B32B9/04
CPC分类号： B82Y30/00 , B05D1/185 , B82Y40/00 , F28F17/005 , F28F2245/02 , Y10T428/2936 , Y10T428/2995
摘要： By forming a film that comprises a microcrystalline polymer having at least a fluorocarbon group and has a rough surface on a surface of a base material, super-water-repellency is provided, the dew condensation water of an air conditioner, for example, can be easily removed, and the freezing of the fin of the heat exchanger can be prevented. A fin that is made of aluminium is coated with a solution for forming a coating film, in which CF.sub.3 (CF.sub.2).sub.7 --(CH.sub.2).sub.2 --SiCl.sub.3 is diluted with nonaqueous cyclohexamethyl trisiloxane at a concentration of 10 vol. % for preparation, to a thickness of 1 to 10 .mu.m by a brush, and then the cyclohexamethyl trisiloxane is vaporized in an atmosphere having a relative humidity of about 75% at room temperature. CF.sub.3 (CF.sub.2).sub.7 --(CH.sub.2).sub.2 --SiCl.sub.3 that remained on the fin is rapidly hydrolyzed with the moisture in the atmosphere, and the moisture in air and a --SiCl.sub.3 group dehydrochlorinated to form a microcrystalline polymer on the fin. As a result, a coating film having a surface roughness in the range of 1 to 40 .mu.m and a contact angle of about 171.degree. to water can be formed.
摘要翻译：通过形成包含至少具有碳氟化合物基团并且在基材表面上具有粗糙表面的微晶聚合物的膜，提供超疏水性，例如空调的结露水可以是容易地除去，并且可以防止热交换器的翅片的冻结。用铝制成的翅片涂覆有形成涂膜的溶液，其中CF 3（CF 2）7 - （CH 2）2 -SiCl 3用10体积浓度的非水性环己甲基三硅氧烷稀释。用于制备，通过刷子至1至10μm的厚度，然后环己基三硅氧烷在室温下在相对湿度为约75％的气氛中蒸发。残留在翅片上的CF 3（CF 2）7 - （CH 2）2 -SiCl 3随着大气中的水分，空气中的水分和-SiCl 3基团脱氯化氢而迅速水解，从而在翅片上形成微晶聚合物。结果，可以形成表面粗糙度为1〜40μm，接触角为171度左右的涂膜。

7. 发明授权

US07468206B1 Organic ultra-thin film 失效
标题翻译：有机超薄膜
公开(公告)号：US07468206B1
公开(公告)日：2008-12-23
申请号：US08992049
申请日：1997-12-17
申请人： Tadashi Ootake , Yasuo Takebe , Norihisa Mino , Hiroaki Takezawa
发明人： Tadashi Ootake , Yasuo Takebe , Norihisa Mino , Hiroaki Takezawa
IPC分类号： G11B5/64 , B05D1/18
CPC分类号： B82Y30/00 , B05D1/185 , B82Y40/00 , Y10T428/26 , Y10T428/261 , Y10T428/265 , Y10T428/31504
摘要： The present invention provides an organic ultra-thin film firmly fixed to a substrate with the film thickness ranging from tens of nm to hundreds of nm. The organic ultra-thin film comprises polymers fixed on a substrate by M2—O—A— bond in which A represents an Si, Ge, Ti, Sn or Zr atom in the polymer, and M2 represents an atom in the substrate) or by a coordinate bond, the polymers are combined with each other by —A1—O—A1′— bond in which A1 and A1′ are Si, Ge, Ti, Sn, Zr or S or by a coordinate bond.
摘要翻译：本发明提供一种牢固地固定在基板上的有机超薄膜，其膜厚度为数十nm至数百nm。有机超薄膜包括通过M2-OA-键固定在基材上的聚合物，其中A表示聚合物中的Si，Ge，Ti，Sn或Zr原子，M2表示基材中的原子）或通过坐标通过-A1-O-A1'-键将聚合物彼此组合，其中A1和A1'是Si，Ge，Ti，Sn，Zr或S或通过配位键。

8. 发明授权

US6096380A Method for water repellent coating and coating apparatus for the same 失效
标题翻译：防水涂布方法及其涂布装置
公开(公告)号：US6096380A
公开(公告)日：2000-08-01
申请号：US185100
申请日：1998-11-03
申请人： Yasuo Takebe , Norihisa Mino
发明人： Yasuo Takebe , Norihisa Mino
IPC分类号： B05C1/14 , B05D1/28 , B05D5/08 , C03C17/00 , C03C17/30
CPC分类号： C03C17/001 , B05C1/14 , B05D1/286 , C03C17/002 , C03C17/30 , B05D5/08 , C03C2218/118
摘要： It is provided a water repellent coating method and apparatus which permits efficient coating either plain or curved surfaces of articles. There is disclosed in the present specification a water repellent coating method comprises the steps of: (a) loading to a carrier in the form of endless belt a coating solution containing at least a water repellent, (b) bringing said carrier into contact with an article to transfer said coating solution on the material, and (c) forming a water repellent film on said article.
摘要翻译：提供了一种防水涂布方法和装置，其允许有效地涂覆制品的平面或曲面。在本说明书中公开了一种防水涂布方法，包括以下步骤：（a）以环形带的形式将至少包含防水剂的涂布溶液装载到载体上，（b）使所述载体与将所述涂布溶液转移到所述材料上的制品，和（c）在所述制品上形成防水膜。

9. 发明授权

US5906871A Latent image, preparation and development thereof and articles with the image 失效
标题翻译：潜在的形象，准备和发展以及形象的文章
公开(公告)号：US5906871A
公开(公告)日：1999-05-25
申请号：US645773
申请日：1996-05-14
申请人： Yasuo Takebe , Koichi Kugimiya , Norihisa Mino , Tohru Nakagawa
发明人： Yasuo Takebe , Koichi Kugimiya , Norihisa Mino , Tohru Nakagawa
IPC分类号： B41M3/00 , B44F1/02
CPC分类号： B41M3/005 , Y10T428/24802 , Y10T428/24835 , Y10T428/24942
摘要： A latent image comprising a first substance formed on a substrate of a second substance having a surface tension different from a surface tension of the first substance, the first substance and the substrate having a difference of 0.1 to 100 nm in height from each other. The latent image is formed by a method comprising the-step of subjecting a substrate of a first substance to a chemical treatment or a physical treatment to form a surface of a second substance which has a surface tension different from a surface tension of the first substance and has a difference of 0.1 to 100 nm in height from the substrate on part of the substrate. The latent image is developed by a method comprising the steps of contacting a latent image comprising a first substance formed on a substrate of a second substance having a surface tension different from a surface tension of the first substance with a third substance different from the first substance and the second substance, and applying a developing ray to the latent image.
摘要翻译：一种潜像，其包括形成在第二物质的基底上的第一物质，所述第二物质的表面张力不同于所述第一物质的表面张力，所述第一物质和所述基底的高度彼此的差异为0.1〜100nm。该潜像通过包括以下步骤的方法形成：将第一物质的基材进行化学处理或物理处理以形成具有与第一物质的表面张力不同的表面张力的第二物质的表面的方法并且在基板的一部分上与基板的高度差为0.1〜100nm。通过包括以下步骤的方法显影潜像：将形成在第一物质的表面张力不同于第一物质的第二物质的基板上形成的第一物质的潜像与不同于第一物质的第三物质和第二物质，并将显影射线施加到潜像上。

10. 发明授权

US06210793B1 Electrically chargeable substrate 失效
标题翻译：可充电的基板
公开(公告)号：US06210793B1
公开(公告)日：2001-04-03
申请号：US08976302
申请日：1997-11-21
申请人： Tohru Nakagawa , Yasuo Takebe , Norihisa Mino
发明人： Tohru Nakagawa , Yasuo Takebe , Norihisa Mino
IPC分类号： B32B1700
CPC分类号： C03C17/30 , Y10S29/90 , Y10T29/49998 , Y10T428/261 , Y10T428/265 , Y10T428/31612 , Y10T428/31663 , Y10T428/31667
摘要： A thin film composed of a silane-based compound comprising an alkyl group or a fluoroalkyl group is bonded to the surface of an electrically insulating substrate through a covalent bond, thus obtaining an electrically chargeable substrate maintaining a charged state for a long time regardless of relative humidity of an atmosphere. A glass plate for placing a sheet in an overhead projector is dipped into a solution comprising CF3(CF)7(CH2)2SiCl3. As a result, a molecular composed of CF3(CF2)7(CH2)2Si(O)3—is chemically bonded to the glass surface. A high charged state, a water-repelling property having a static contact angle of pure water on the thin film formed on the glass surface of 110 degrees and a volume electric resistivity in the range of 1×1011−1×1019&OHgr;·cm are provided.
摘要翻译：由包含烷基或氟烷基的硅烷类化合物构成的薄膜通过共价键与电绝缘性基板的表面接合，从而获得长时间保持充电状态的可充电基板，而不管相关气氛湿度将用于将片材放置在高架投影仪中的玻璃板浸入包含CF 3（CF）7（CH 2）2 SiCl 3的溶液中。结果，由CF 3（CF 2）7（CH 2）2 Si（O）3组成的分子化学键合到玻璃表面。提供高充电状态，在110度的玻璃表面上形成的薄膜上具有纯水的静态接触角以及1×10 11〜1×10 19Ω·cm范围内的体积电阻率的防水性。

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