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1. 发明申请

US20140114038A1 METHOD AND APPARATUS FOR DISCHARGING A POLYMER FROM A GAS-PHASE REACTOR 有权
标题翻译：从气相反应器中排出聚合物的方法和装置
公开(公告)号：US20140114038A1
公开(公告)日：2014-04-24
申请号：US14125777
申请日：2012-06-19
申请人： Manfred Hecker , Paulus-Petrus Maria De Lange , Klaus Berhalter , Thomas Andreas Hora , Axel Hamann
发明人： Manfred Hecker , Paulus-Petrus Maria De Lange , Klaus Berhalter , Thomas Andreas Hora , Axel Hamann
IPC分类号： C08F2/34
CPC分类号： C08F2/34 , B01J8/003 , B01J8/008 , B01J8/24 , B01J2208/00274 , B01J2208/00761 , B01J2208/00991 , C08F10/00 , Y10S526/92 , C08F2/01
摘要： Process for discharging polyolefin particles from a gas-phase polymerization reactor of a pressure from 1.0 MPa to 10 MPa to a discharge vessel of a pressure from 0.1 MPa to 1.0 MPa wherein the discharging is carried out discontinuously through at least two discharge lines in which the polyolefin particles are transported horizontally or upwards, process for polymerizing olefins at temperatures of from 30° C. to 160° C. and pressures of from 1.0 MPa to 10 MPa in the presence of a polymerization catalyst in a gas-phase polymerization reactor comprising discharging the obtained polyolefin particles from the gas-phase polymerization reactor by the process for discharging polyolefin particles and apparatus for polymerizing olefins in the gas-phase comprising a polymerization reactor, a discharge vessel and at least two pipes connecting the polymerization reactor and the discharge vessel for discharging polyolefin particles, wherein the discharge lines are constructed in a way that the polyolefin particles conveyed from the polymerization reactor to the discharge vessel are transported horizontally or upwards.
摘要翻译：从压力为1.0MPa至10MPa的气相聚合反应器中将聚烯烃颗粒排放至压力为0.1MPa至1.0MPa的放电容器的方法，其中通过至少两个排放管线不连续地进行排放，其中，聚烯烃颗粒水平或向上输送，在气相聚合反应器中在聚合催化剂存在下，在30℃至160℃的温度和1.0MPa至10MPa的压力下聚合烯烃的方法，包括排出通过排出聚烯烃颗粒的方法从气相聚合反应器获得的聚烯烃颗粒和在气相中聚合烯烃的装置包括聚合反应器，放电容器和连接聚合反应器和放电容器的至少两个管，排出聚烯烃颗粒，其中排出管线以这样的方式构造从聚合反应器输送到放电容器的裂解烯烃颗粒被水平或向上输送。

2. 发明授权

US08853334B2 Method and apparatus for discharging a polymer from a gas-phase reactor 有权
标题翻译：从气相反应器中排出聚合物的方法和装置
公开(公告)号：US08853334B2
公开(公告)日：2014-10-07
申请号：US14125777
申请日：2012-06-19
申请人： Manfred Hecker , Paulus-Petrus Maria De Lange , Klaus Berhalter , Thomas Andreas Hora , Axel Hamann
发明人： Manfred Hecker , Paulus-Petrus Maria De Lange , Klaus Berhalter , Thomas Andreas Hora , Axel Hamann
IPC分类号： C08F2/34 , B01J8/24 , B01J19/24 , B01J8/00 , C08F10/00
CPC分类号： C08F2/34 , B01J8/003 , B01J8/008 , B01J8/24 , B01J2208/00274 , B01J2208/00761 , B01J2208/00991 , C08F10/00 , Y10S526/92 , C08F2/01
摘要： Process and apparatus for discharging polyolefin particles from a gas-phase polymerization reactor of a pressure from 1.0 MPa to 10 MPa to a discharge vessel of a pressure from 0.1 MPa to 1.0 MPa wherein the discharging is carried out discontinuously through at least two discharge lines in which the polyolefin particles are transported horizontally or upwards.
摘要翻译：从压力为1.0MPa至10MPa的气相聚合反应器中将聚烯烃颗粒排放至压力为0.1MPa至1.0MPa的放电容器的方法和装置，其中通过至少两条排出管线不连续地进行排放，聚烯烃颗粒水平或向上输送。

3. 发明申请

US20070264171A1 Apparatus for the Gas-Phase Polymerization of Olefins,in Particular Ethylene 有权
标题翻译：用于烯烃气相聚合的装置，特别是乙烯
公开(公告)号：US20070264171A1
公开(公告)日：2007-11-15
申请号：US11667349
申请日：2005-11-09
申请人： Eberhard Herrmann , Axel Sperber , Manfred Hecker , Rainer Karer , Klaus Berhalter , Paulus de Lange , Jorg Halpap , Cyrus Ahmadzade-Youssefi
发明人： Eberhard Herrmann , Axel Sperber , Manfred Hecker , Rainer Karer , Klaus Berhalter , Paulus de Lange , Jorg Halpap , Cyrus Ahmadzade-Youssefi
IPC分类号： C08F2/34
CPC分类号： B01J8/1872 , B01J8/0055 , B01J8/24 , B01J2208/00256 , B01J2208/00274 , B04C5/081 , C08F6/02 , C08F10/00 , C08F10/02 , C08F110/02 , C08L23/04 , C08F2/34
摘要： An apparatus for the polymerization of olefins, in particular ethylene, comprising a gas-phase fluidized-bed reactor (1), a recycle gas line (2) connected to the reactor for discharging and recirculating the recycle gas stream comprising the unpolymerized olefin and a cyclone (3) located in the recycle gas line for the reduction and precipitation of the solid particles entrained in the recycle gas from the reactor, with the cyclone comprising an upper section (3a) which has an essentially vertical central axis, whose wall extends along a rotationally symmetric body and which is provided with a cyclone inlet (4) arranged eccentrically relative to the central axis, a middle section (3b) which adjoins the upper section (3a) and whose wall extends along a rotationally symmetric body which tapers in a downward direction, a lower section (3c) for discharging the solid particles precipitated from the recycle gas which adjoins the middle section (3b) and whose wall extends along a rotationally symmetric body and a tube (5) extending essentially axially symmetrically down into the upper section and, if appropriate, the middle section for discharging the recycle gas which has been freed of the particles. According to the invention the ratio Hi of the distance hi from the lower end of the tube (5) extending downward into the cyclone to the intersection (6) of an imaginary extension of the wall of the downward-extending tube (5) with the wall of the middle section (3b) to the diameter di of the downward-extending tube (5) is from 3 to 8, in particular from 4 to 7.
摘要翻译：用于烯烃聚合的装置，特别是乙烯，包括气相流化床反应器（1），连接到反应器的再循环气体管线（2），用于排出和再循环包含未聚合烯烃的循环气流和旋流器（3），其位于循环气体管线中，用于还原和沉淀夹带在来自反应器的再循环气体中的固体颗粒，旋风分离器包括具有基本上垂直的中心轴线的上部分（3a），其上壁延伸沿着旋转对称体并且设置有相对于中心轴线偏心布置的旋风入口（4），邻近上部（3a）并且其壁沿旋转对称体延伸的中间部分（3b）用于排出邻近中间部分（3b）并且其壁延伸的再循环气体沉淀的固体颗粒的下部分（3c）旋转对称体和基本上轴向对称地延伸到上部的管（5）以及适当的中间部分用于排出已经没有颗粒的循环气体。根据本发明，与从下游进入旋风分离器的管（5）的下端距离h i i的距离h i i的比例H i 向下延伸的管（5）的壁与中间部分（3b）的壁与向下延伸的管（5）的直径d iI i的假想延伸为3至 8，特别是4到7。

4. 发明申请

US20080014128A1 Apparatus and Process for the Gas-Phase Polymerization of Olefins 有权
标题翻译：用于烯烃气相聚合的装置和方法
公开(公告)号：US20080014128A1
公开(公告)日：2008-01-17
申请号：US11667417
申请日：2005-11-08
申请人： Eberhard Herrmann , Manfred Hecker , Rainer Karer , Klaus Berhalter , Paulus de Lange , Jorg Halpap , Cyrus Ahmadzade-Youssefi
发明人： Eberhard Herrmann , Manfred Hecker , Rainer Karer , Klaus Berhalter , Paulus de Lange , Jorg Halpap , Cyrus Ahmadzade-Youssefi
IPC分类号： C08F10/00 , B01J19/18
CPC分类号： B01J8/003 , B01J8/006 , B01J8/1872 , B01J2208/00256 , B01J2208/00274 , B01J2208/00761 , C08F10/00 , C08F110/02 , C08F2/34
摘要： Apparatus for the polymerization of olefins, in particular ethylene, comprising a gas-phase fluidized-bed reactor (1), a product offtake line (15) for taking polymer particles either continuously or discontinuously from the reactor (1), which line (15) is connected to a depressurization vessel (2) for separating polymer particles and gas, a recycle gas filter (3) for freeing the gas of entrained fine particles connected to the depressurization vessel (2), a compressor which compresses the gas which has been freed of fine particles and recirculates it into the reactor (1), with the recycle gas filter (3) having an inlet chamber (4) provided with a gas inlet (6), an outlet chamber (5) provided with a gas outlet (7), an essentially vertical sheet-like filter medium (9) for retaining the fine particles which separates the inlet chamber (4) from the outlet chamber (5) and a particle outlet (8). The inlet chamber (4) has a dividing wall (10) which is arranged essentially parallel to the filter medium (9) and separates the inlet chamber (4) into an inflow region (4a), which is connected to the gas inlet (6), and a filter region (4b) in which the filter medium is located and has an upper opening and a lower opening which are dimensioned so that from 60 to 90% of the volume flow flows through the upper opening so that flow along the filter medium (9) from the top downward results.
摘要翻译：用于烯烃聚合的设备，特别是乙烯，包括气相流化床反应器（1），用于从反应器（1）连续或不连续地获取聚合物颗粒的出口管线（15），该管线（15））连接到用于分离聚合物颗粒和气体的减压容器（2），用于释放连接到减压容器（2）的夹带的细颗粒的气体的循环气体过滤器（3），压缩已经被释放细颗粒并将其再循环到反应器（1）中，循环气体过滤器（3）具有设置有气体入口（6）的入口室（4），设置有气体出口的出口室（5） 7），用于保持将入口室（4）与出口室（5）分离的细颗粒和颗粒出口（8）的基本垂直的片状过滤介质（9）。入口室（4）具有基本上与过滤介质（9）平行布置的分隔壁（10），并将入口室（4）分离成入口区域（4a），该入口区域连接到气体入口 6）和过滤器区域（4b），其中过滤介质位于并具有上开口和下开口，其尺寸使得体积流量的60％至90％流过上开口，使得沿着过滤介质（9）从顶部向下的结果。

5. 发明授权

US07781544B2 Apparatus for the gas-phase polymerization of olefins, in particular ethylene 有权
标题翻译：用于烯烃气相聚合的装置，特别是乙烯
公开(公告)号：US07781544B2
公开(公告)日：2010-08-24
申请号：US11667349
申请日：2005-11-09
申请人： Eberhard Herrmann , Axel Sperber , Manfred Hecker , Rainer Karer , Klaus Berhalter , Paulus De Lange , Jörg Halpap , Cyrus Ahmadzade-Youssefi
发明人： Eberhard Herrmann , Axel Sperber , Manfred Hecker , Rainer Karer , Klaus Berhalter , Paulus De Lange , Jörg Halpap , Cyrus Ahmadzade-Youssefi
IPC分类号： C08F2/00 , F27B15/08
CPC分类号： B01J8/1872 , B01J8/0055 , B01J8/24 , B01J2208/00256 , B01J2208/00274 , B04C5/081 , C08F6/02 , C08F10/00 , C08F10/02 , C08F110/02 , C08L23/04 , C08F2/34
摘要： An apparatus for the polymerization of olefins, in particular ethylene, comprising a gas-phase fluidized-bed reactor (1), a recycle gas line (2) connected to the reactor for discharging and recirculating the recycle gas stream comprising the unpolymerized olefin and a cyclone (3) located in the recycle gas line for the reduction and precipitation of the solid particles entrained in the recycle gas from the reactor, with the cyclone comprising an upper section (3a) which has an essentially vertical central axis, whose wall extends along a rotationally symmetric body and which is provided with a cyclone inlet (4) arranged eccentrically relative to the central axis, a middle section (3b) which adjoins the upper section (3a) and whose wall extends along a rotationally symmetric body which tapers in a downward direction, a lower section (3c) for discharging the solid particles precipitated from the recycle gas which adjoins the middle section (3b) and whose wall extends along a rotationally symmetric body and a tube (5) extending essentially axially symmetrically down into the upper section and, if appropriate, the middle section for discharging the recycle gas which has been freed of the particles. According to the invention the ratio Hi of the distance hi from the lower end of the tube (5) extending downward into the cyclone to the intersection (6) of an imaginary extension of the wall of the downward-extending tube (5) with the wall of the middle section (3b) to the diameter di of the downward-extending tube (5) is from 3 to 8, in particular from 4 to 7.
摘要翻译：用于烯烃聚合的装置，特别是乙烯，包括气相流化床反应器（1），连接到反应器的再循环气体管线（2），用于排出和再循环包含未聚合烯烃的循环气流和旋风分离器（3）位于循环气体管线中，用于还原和沉淀夹带在来自反应器的再循环气体中的固体颗粒，其中旋风分离器包括具有基本垂直的中心轴线的上部分（3a），其上壁沿着旋转对称体，并且设置有相对于中心轴偏心布置的旋风入口（4），邻接上部（3a）的中间部分（3b），并且其壁沿着旋转对称的体用于排出邻近中间部分（3b）的循环气体沉淀的固体颗粒的下部（3c），并且其壁沿旋转方向延伸对称体和管（5），其基本上轴向对称地延伸到上部，并且如果适当的话，中间部分用于排出已经没有颗粒的循环气体。根据本发明，从管（5）的下端向下延伸到旋风分离器中的距离hi的距离hi与向下延伸的管（5）的壁的假想延伸部的交点（6）中间部分（3b）的壁向下延伸管（5）的直径di为3至8，特别是4至7。

6. 发明授权

US07776278B2 Apparatus and process for the gas-phase polymerization of olefins 有权
标题翻译：用于烯烃气相聚合的装置和方法
公开(公告)号：US07776278B2
公开(公告)日：2010-08-17
申请号：US11667417
申请日：2005-11-08
申请人： Eberhard Herrmann , Manfred Hecker , Rainer Karer , Klaus Berhalter , Paulus De Lange , Jörg Halpap , Cyrus Ahmadzade-Youssefi
发明人： Eberhard Herrmann , Manfred Hecker , Rainer Karer , Klaus Berhalter , Paulus De Lange , Jörg Halpap , Cyrus Ahmadzade-Youssefi
IPC分类号： B01J19/00
CPC分类号： B01J8/003 , B01J8/006 , B01J8/1872 , B01J2208/00256 , B01J2208/00274 , B01J2208/00761 , C08F10/00 , C08F110/02 , C08F2/34
摘要： Apparatus for the polymerization of olefins, in particular ethylene, comprising a gas-phase fluidized-bed reactor (1), a product offtake line (15) for taking polymer particles either continuously or discontinuously from the reactor (1), which line (15) is connected to a depressurization vessel (2) for separating polymer particles and gas, a recycle gas filter (3) for freeing the gas of entrained fine particles connected to the depressurization vessel (2), a compressor which compresses the gas which has been freed of fine particles and recirculates it into the reactor (1), with the recycle gas filter (3) having an inlet chamber (4) provided with a gas inlet (6), an outlet chamber (5) provided with a gas outlet (7), an essentially vertical sheet-like filter medium (9) for retaining the fine particles which separates the inlet chamber (4) from the outlet chamber (5) and a particle outlet (8). The inlet chamber (4) has a dividing wall (10) which is arranged essentially parallel to the filter medium (9) and separates the inlet chamber (4) into an inflow region (4a), which is connected to the gas inlet (6), and a filter region (4b) in which the filter medium is located and has an upper opening and a lower opening which are dimensioned so that from 60 to 90% of the volume flow flows through the upper opening so that flow along the filter medium (9) from the top downward results.
摘要翻译：用于烯烃聚合的设备，特别是乙烯，包括气相流化床反应器（1），用于从反应器（1）连续或不连续地获取聚合物颗粒的出口管线（15），该管线（15））连接到用于分离聚合物颗粒和气体的减压容器（2），用于释放连接到减压容器（2）的夹带的细颗粒的气体的循环气体过滤器（3），压缩已经被释放细颗粒并将其再循环到反应器（1）中，循环气体过滤器（3）具有设置有气体入口（6）的入口室（4），设置有气体出口的出口室（5） 7），用于保持将入口室（4）与出口室（5）分离的细颗粒和颗粒出口（8）的基本垂直的片状过滤介质（9）。入口室（4）具有基本上与过滤介质（9）平行布置的分隔壁（10），并将入口室（4）分离成入口区域（4a），该入口区域连接到气体入口）和过滤器区域（4b），其中所述过滤介质定位并具有上开口和下开口，所述上开口和下开口的尺寸使得所述体积流的60至90％流过所述上开口，使得沿着所述过滤器的流动中等（9）从上方下降。

7. 发明授权

US08710160B2 Process for the preparation of ethylene homopolymers or copolymers in a high-pressure reactor controlled by a model based predictive controller 有权
标题翻译：在由基于模型的预测控制器控制的高压反应器中制备乙烯均聚物或共聚物的方法
公开(公告)号：US08710160B2
公开(公告)日：2014-04-29
申请号：US13516703
申请日：2010-12-20
申请人： Christian-Ulrich Schmidt , Klaus Berhalter , Steve Makin , Kevin Taylor
发明人： Christian-Ulrich Schmidt , Klaus Berhalter , Steve Makin , Kevin Taylor
IPC分类号： C08F2/00 , C08F4/28 , C08F10/00 , C08F110/02
CPC分类号： C08F110/02 , C08F2400/02 , C08F2/00 , C08F2500/12
摘要： Process for the preparation of ethylene homopolymers or copolymers in the presence of free-radical polymerization initiator at from 100° C. to 350° C. and pressures in the range of from 160 MPa to 350 MPa in a high-pressure polymerization unit comprising a high-pressure reactor with one or more reaction zones, to each of which free-radical polymerization initiator is fed, which is controlled by a model based predictive controller carrying out the steps.
摘要翻译：在自由基聚合引发剂存在下，在100℃至350℃下制备乙烯均聚物或共聚物的方法以及在160MPa至350MPa范围内的压力在包含具有一个或多个反应区的高压反应器，其中每一个自由基聚合引发剂进料，其由基于模型的预测控制器进行控制。

8. 发明申请

US20100256320A1 CONTINUOUS FEED OF AUXILIARIES FOR THE POLYMERIZATION OF OLEFINS 有权
标题翻译：连续生产烯烃聚合的辅助剂
公开(公告)号：US20100256320A1
公开(公告)日：2010-10-07
申请号：US12733454
申请日：2008-09-02
申请人： Jürgen Schwind , Horst Klassen , Gerald Lutz , Robert Gelinas , Klaus Berhalter , Ursula Krügers
发明人： Jürgen Schwind , Horst Klassen , Gerald Lutz , Robert Gelinas , Klaus Berhalter , Ursula Krügers
IPC分类号： C08F10/00 , C08F10/02 , C08F10/06
CPC分类号： C08F10/00 , C08F2/005 , C08F2/00 , C08F2/34
摘要： Continuous feed of auxiliaries for the polymerization reaction of ethylene, propene, and other higher homologous olefins in the preparation of homo- and copolymers, avoiding production of inhomogeneities, such as lumps or chunks which are present because the condition of the auxiliaries is not suitable for precise metering, becomes possible when auxiliaries in paste or solid form, in particular antistatic auxiliaries, are subjected, prior to feed, to a heat treatment in the presence of a solvent at a temperature of from 20 to 80° C., and then recooled, and then fed to the polymerization reaction.
摘要翻译：在制备均聚物和共聚物时，连续进料乙烯，丙烯和其他较高同系烯烃的聚合反应助剂，避免产生不均匀性，如由于助剂的状态而不适合存在的团块或块当将糊剂或固体形式的助剂，特别是抗静电助剂在进料前，在溶剂存在下，在20〜80℃的温度下进行热处理，然后重新冷却，然后进料至聚合反应。

9. 发明授权

US08017703B2 Continuous feed of auxiliaries for the polymerization of olefins 有权
标题翻译：连续进料烯烃聚合助剂
公开(公告)号：US08017703B2
公开(公告)日：2011-09-13
申请号：US12733454
申请日：2008-09-02
申请人： Jürgen Schwind , Horst Klassen , Gerald Lutz , Robert Gelinas , Klaus Berhalter , Ursula Krügers
发明人： Jürgen Schwind , Horst Klassen , Gerald Lutz , Robert Gelinas , Klaus Berhalter , Ursula Krügers
IPC分类号： C08F2/34 , C08F2/12 , C08F10/02
CPC分类号： C08F10/00 , C08F2/005 , C08F2/00 , C08F2/34
摘要： Continuous feed of auxiliaries for the polymerization reaction of ethylene, propene, and other higher homologous olefins in the preparation of homo- and copolymers, avoiding production of inhomogeneities, such as lumps or chunks which are present because the condition of the auxiliaries is not suitable for precise metering, becomes possible when auxiliaries in paste or solid form, in particular antistatic auxiliaries, are subjected, prior to feed, to a heat treatment in the presence of a solvent at a temperature of from 20 to 80° C., and then recooled, and then fed to the polymerization reaction.
摘要翻译：在制备均聚物和共聚物时，连续进料乙烯，丙烯和其他较高同系烯烃的聚合反应助剂，避免产生不均匀性，如由于助剂的状态而不适合存在的团块或块当将糊剂或固体形式的助剂，特别是抗静电助剂在进料前，在溶剂存在下，在20〜80℃的温度下进行热处理，然后重新冷却，然后进料至聚合反应。

10. 发明申请

US20130333832A1 PROCESS FOR PREPARING ETHYLENE HOMOPOLYMERS OR COPOLYMERS IN A TUBULAR REACTOR WITH AT LEAST TWO REACTION ZONES HAVING DIFFERENT CONCENTRATIONS OF CHAIN TRANSFER AGENT 审中-公开
标题翻译：在具有链转移剂不同浓度的至少两个反应区的管状反应器中制备乙烯共聚物或共聚物的方法
公开(公告)号：US20130333832A1
公开(公告)日：2013-12-19
申请号：US14002242
申请日：2012-03-01
申请人： Iakovos Vittorias , Barbara Gall , Sebastian Weiand , Andrei Gonioukh , Stephan Schmitz , Klaus Berhalter , Gerd Mannebach , Markus Busch , Thomas Herrmann
发明人： Iakovos Vittorias , Barbara Gall , Sebastian Weiand , Andrei Gonioukh , Stephan Schmitz , Klaus Berhalter , Gerd Mannebach , Markus Busch , Thomas Herrmann
IPC分类号： C08F2/38
CPC分类号： C08F2/38 , B29C48/022 , B29C48/09 , B29C48/154 , C08F10/02 , C08F110/02 , C08F210/02 , C08F2/00 , C08F2500/09 , C08F2500/10 , C08F218/08 , C08F4/38
摘要： Process for preparing ethylene homopolymers or copolymers in the presence of free-radical polymerization initiator and at least one chain transfer agent at pressures in the range of from 110 MPa to 350 MPa and temperatures in the range of from 100° C. to 350° C. in a tubular reactor with at least two reaction zones having different concentrations of the chain transfer agent, wherein the concentration of the chain transfer agent in the first reaction zone is less than 70% of the concentration of the chain transfer agent in the reaction zone with the highest concentration of the chain transfer agent, ethylene homopolymers or copolymers obtainable by such a process, the use of the ethylene homopolymers or copolymers for extrusion coating and a process for extrusion coating a substrate selected from the group consisting of paper, paperboard, polymeric film, and metal, with such ethylene homopolymers or copolymers.
摘要翻译：在自由基聚合引发剂和至少一种链转移剂的存在下，在110MPa至350MPa的压力和100℃至350℃的温度范围内制备乙烯均聚物或共聚物的方法在具有不同浓度的链转移剂的至少两个反应区的管式反应器中，其中第一反应区中链转移剂的浓度小于反应区中链转移剂浓度的70％具有最高浓度的链转移剂，乙烯均聚物或可通过这种方法得到的共聚物，使用乙烯均聚物或共聚物进行挤出涂布，以及用于挤出涂布选自纸，纸板，聚合物膜和金属，与这种乙烯均聚物或共聚物。

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