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1. 发明申请

US20180112017A1 Ethylene-Based Polymers with Low Hexane Extractables 审中-公开
公开(公告)号：US20180112017A1
公开(公告)日：2018-04-26
申请号：US15737448
申请日：2016-06-23
申请人： Dow Global Technologies LLC
发明人： Otto J. Berbee , Cornelis F.J. Den Doelder , Stefan Hinrichs , Teresa P. Karjala , John O. Osby
IPC分类号： C08F110/02 , C08F2/00 , C08F2/01 , C08F2/38 , C08F4/38 , B01J19/24
CPC分类号： C08F110/02 , B01J19/2415 , C08F2/001 , C08F2/01 , C08F2/38 , C08F4/38 , C08F2400/02 , C08F2500/08 , C08F2500/12 , Y02P20/582 , C08F2500/17
摘要： Ethylene-based polymers comprising the following properties: (A) a density from 0.9190 g/cc to 0.9240 g/cc; (B) a hexane extractable level that is less than or equal to the lower of: (1) (A+(B*density (g/cc))+(C*log(MI) dg/min)) based on total weight of the ethylene-based polymer; where A=250.5 wt %, B=−270 wt %/(g/cc), C=0.25 wt %/[log(dg/min)], or (2) 2.0 wt %; (C) a G′ (at G″=500 Pa, 170° C.) that meets the following equation: G′≥D+E[log (12)], where D=150 Pa and E=−60 Pa/[log(dg/min)]; and (D) a melt index (12) from 1.0 to 20 dg/min; are made in process comprising the step of contacting in a reaction configuration, comprising a first tubular reaction zone 1 and a last tubular reaction zone i, in which i is greater than or equal to (≥) 3, under high pressure polymerization conditions, and in which the first reaction zone 1 has a peak polymerization temperature greater than the peak temperature of the ith reaction zone, and wherein the difference in these two peak temperatures is ≥30° C.

2. 发明申请

US20170283526A1 LOW DENSITY ETHYLENE-BASED POLYMERS WITH BROAD MOLECULAR WEIGHT DISTRIBUTIONS AND LOW EXTRACTABLES 审中-公开
公开(公告)号：US20170283526A1
公开(公告)日：2017-10-05
申请号：US15626952
申请日：2017-06-19
申请人： Dow Global Technologies LLC
发明人： Otto J. Berbee , Cornelis F. J. Den Doelder , Stefan Hinrichs , Teresa P. Karjala
IPC分类号： C08F10/02 , C08F210/02 , C09D123/08 , C08F220/18 , C08L23/04 , C09D123/06 , C08F110/02 , C08F218/08
CPC分类号： C08F10/02 , C08F110/02 , C08F210/02 , C08F218/08 , C08F220/18 , C08L23/04 , C09D123/06 , C09D123/0815 , C08F2/00 , C08F2/38 , C08F2500/04 , C08F2500/08 , C08F2500/12 , C08F2500/17 , C08F2500/19 , C08F220/06 , C08F220/14 , C08L23/06 , C08F4/38
摘要： The invention provides an ethylene-based polymer comprising the following properties: a) a melt index (I2)≧2.0 dg/min; b) a Mw(abs) versus I2 relationship: Mw(abs)

3. 发明授权

US09453087B2 Method for synthesizing homopolymer N-vinyl butyrolactam with super-low molecular weight and super-low residual monomer 有权
标题翻译：用超低分子量和超低残留单体合成均聚物N-乙烯基丁内酰胺的方法
公开(公告)号：US09453087B2
公开(公告)日：2016-09-27
申请号：US14401743
申请日：2012-07-23
申请人： Yu Wang , Wei Liu , Zhan Chen
发明人： Yu Wang , Wei Liu , Zhan Chen
IPC分类号： C08F24/00 , C08F126/06 , C08F4/38 , C08F6/00
CPC分类号： C08F24/00 , C08F4/38 , C08F6/003 , C08F126/06 , C08L39/04
摘要： A synthesis method of ultra low molecular weight homopolymerized N-vinyl butyrolactam with ultra low residual monomer content is provided N-vinyl butyrolactam monomers and water are provided with the mass ratio of 3:17˜8:12 0.5%˜5.0% by weight of initiators, 0.1%˜5.0% by weight of a catalyst, and 0.1%˜10% by weight of a molecular weight regulator are provided in the presence of an inert gas, adding the above mentioned raw materials in batches, adjusting the pH of the reaction system to 7.0-8.0 with an activator, reacting at the polymerization temperature of 60-85° C. A peroxide is added and maintaining the temperature for 2 hours, to obtain an aqueous solution of ultra low molecular weight homopolymerized N-vinyl butyrolactam. The aqueous solution is dried to obtain a powdery ultra low molecular weight homopolymerized N-vinyl butyrolactam with ultra low residual monomer content.
摘要翻译：提供了具有超低残留单体含量的超低分子量均聚的N-乙烯基丁内酰胺的合成方法，提供了N-乙烯基丁内酰胺单体和水，其质量比为3：17〜8：12 0.5％〜5.0％引发剂，0.1重量％〜5.0重量％的催化剂和0.1重量％〜10重量％的分子量调节剂，在惰性气体存在下，分批加入上述原料，调节pH值反应体系为7.0-8.0，用活化剂，在聚合温度为60-85℃下反应。加入过氧化物并保持温度2小时，得到超低分子量均聚N-乙烯基丁内酰胺水溶液。将水溶液干燥，得到具有超低残留单体含量的粉末状超低分子量均聚N-乙烯基丁内酰胺。

4. 发明授权

US09394389B2 Low density ethylene-based polymers with high melt strength 有权
标题翻译：具有高熔体强度的低密度乙烯基聚合物
公开(公告)号：US09394389B2
公开(公告)日：2016-07-19
申请号：US14434204
申请日：2013-03-12
申请人： Dow Global Technologies LLC
发明人： Otto J. Berbee , Cornelis F. J. den Doelder , Teresa P. Karjala , Karl Zuercher , Jian Wang , Stefan Hinrichs
IPC分类号： C08F110/02 , C08L23/06 , C08L23/08 , C09D123/06 , C09D123/08
CPC分类号： C08F110/02 , C08L23/06 , C08L23/0815 , C08L23/0869 , C08L2205/02 , C08L2205/025 , C08L2207/066 , C09D123/06 , C09D123/0815 , C09D123/0869 , C08F2500/12 , C08F2500/11 , C08F4/38
摘要： The invention provides a composition comprising a first ethylene-based polymer, formed by a high pressure, free-radical polymerization process, and comprising the following properties: a) a Mw(abs) versus I2 relationship: Mw(abs)
摘要翻译：本发明提供一种组合物，其包含通过高压自由基聚合方法形成的第一种基于乙烯的聚合物，并且包含以下性质：a）Mw（abs）与I 2的关系：Mw（abs）

5. 发明授权

US09303107B2 Ethylene-based polymers and processes to make the same 有权
标题翻译：乙烯基聚合物和工艺相同
公开(公告)号：US09303107B2
公开(公告)日：2016-04-05
申请号：US14578654
申请日：2014-12-22
申请人： Dow Global Technologies LLC
发明人： Teresa P. Karjala , Lori L. Kardos , Wallace W. Yau , Jose Ortega , Alfred E. Vigil, Jr.
IPC分类号： C08F210/02 , C08F110/02 , C08J5/18
CPC分类号： C08F110/02 , C08J5/18 , C08J2323/06 , C08F10/00 , C08F4/38 , C08F2500/04 , C08F2500/05 , C08F2500/10 , C08F2500/11 , C08F2500/12 , C08F2500/17 , C08F2500/26 , C08F2/001
摘要： An ethylene-based polymer, which is a low density polyethylene (LDPE), obtained by free radical polymerization of ethylene, and wherein the LDPE has a GPC parameter “LSP” less than 1.60.An ethylene-based polymer that comprises the following features: a) at least 0.1 amyl groups per 1000 total carbon atoms; b) a melt index of 0.01 to 0.3; c) a z-average molecular weight of Mz (conv.) of greater than 350,000 g/mol and less than 425,000 g/mol; d) a gpcBR value from 1.50 to 2.05, and e) a MWD(conv) [Mw(conv)/Mn(conv)] from 6 to 9. An ethylene-based polymer that comprises the following features: a) at least 0.1 amyl groups per 1000 total carbon atoms; b) a melt viscosity ratio (V0.1/V100), at 190° C., greater than, or equal to, 58; c) a melt viscosity at 0.1 rad/s, 190° C., greater than, or equal to, 40,000 Pa·s, and d) a gpcBR value from 1.50 to 2.25.
摘要翻译：通过乙烯的自由基聚合获得的低密度聚乙烯（LDPE）的乙烯类聚合物，其中LDPE具有小于1.60的GPC参数“LSP”。一种乙烯基聚合物，其包含以下特征：a）每1000个总碳原子至少0.1个戊基; b）熔体指数为0.01至0.3; c）大于350,000g / mol且小于425,000g / mol的Mz（转化）的z-平均分子量; d）gpcBR值为1.50至2.05，e）MWD（conv）[Mw（conv）/ Mn（conv）]为6至9.一种乙烯基聚合物，其包含以下特征：a）至少0.1 每1000个总碳原子的戊基; b）熔体粘度比（V0.1 / V100），在190℃，大于或等于58; c）0.1rad / s，190℃，大于或等于40,000Pa·s的熔体粘度，和d）gpcBR值为1.50-2.25。

6. 发明申请

US20150210819A1 PROCESS FOR THE PREPARATION OF EXPANDABLE POLYSTYRENE BY CONTINUOUS INJECTION OF A LIQUID ORGANIC PEROXIDE 审中-公开
标题翻译：通过连续注射有机有机过氧化物制备可膨胀的聚苯乙烯的方法
公开(公告)号：US20150210819A1
公开(公告)日：2015-07-30
申请号：US14683238
申请日：2015-04-10
申请人： ARKEMA FRANCE
发明人： Pascal NICOL , Jacques COCHET
IPC分类号： C08J9/20 , C08J9/00 , C08J9/14
CPC分类号： C08J9/20 , C08F2/18 , C08F4/34 , C08F4/38 , C08J9/0023 , C08J9/141 , C08J2203/14 , C08J2325/04 , C08J2325/06 , C08F12/08
摘要： A process for the preparation of expandable polystyrene including the following steps: i°) heating an aqueous suspension including styrene monomer and at least one organic peroxide initiator of formula (I) 1-alkoxy-1-t-alkylperoxycyclohexane in which the alkoxy group contains 1 to 4 carbon atoms, the t-alkyl group contains 4 to 12 carbon atoms, and the cyclohexane ring may optionally be substituted with 1 to 3 alkyl groups each, independently having 1 to 3 carbon atoms, at a temperature ranging from 100° C. to 120° C.), ii°) adding a blowing agent selected from the group of alkanes having from 4 to 6 carbon atoms and mixtures thereof. Also, an expandable polystyrene obtainable according to such a process and to insulation parts and packaging including such an expandable polystyrene.
摘要翻译：一种制备可发性聚苯乙烯的方法，其包括以下步骤：i）加热含有苯乙烯单体和至少一种式（I）的有机过氧化物引发剂的水悬浮液，其中烷氧基含有1-烷氧基-1-叔烷基过氧环己烷 1〜4个碳原子，t-烷基含有4〜12个碳原子，环己烷环可以任选被1〜3个独立地具有1〜3个碳原子的烷基取代，在100℃ ），ii°）加入选自具有4至6个碳原子的烷烃的发泡剂及其混合物。而且，根据这种方法可获得的可发性聚苯乙烯和包括这种可发性聚苯乙烯的绝缘部件和包装。

7. 发明申请

US20150197590A1 ETHYLENE-BASED POLYMERS AND PROCESSES FOR THE SAME 审中-公开
标题翻译：乙烯基聚合物及其制备方法
公开(公告)号：US20150197590A1
公开(公告)日：2015-07-16
申请号：US14411445
申请日：2013-03-08
申请人： Dow Global Technologies LLC
发明人： John O. Osby
IPC分类号： C08F210/02 , C08L23/08
CPC分类号： C08F210/02 , C08F236/20 , C08L23/08 , C08L23/0869 , C08F10/02 , C08F2/38 , C08F220/40 , C08F2222/1013 , C08F4/38 , C08F2500/08 , C08F2500/11 , C08F2500/12 , C08F210/16 , C08F210/06 , C08F2/00
摘要： The invention provides an ethylene-based polymer formed from reacting at least the following: ethylene and at least one asymmetrical polyene, comprising an “alpha, beta unsaturated end” and a “C—C double bond end,” and wherein the reaction takes place in the presence of at least one free-radical initiator.
摘要翻译：本发明提供一种乙烯类聚合物，其通过使至少以下物质至少反应而形成：乙烯和至少一种不对称多烯，其包含“α，β不饱和末端”和“C-C双键末端”，并且其中反应发生在至少一种自由基引发剂的存在下。

8. 发明授权

US08916667B2 Ethylene-based polymers and processes to make the same 有权
标题翻译：乙烯基聚合物和工艺相同
公开(公告)号：US08916667B2
公开(公告)日：2014-12-23
申请号：US13799778
申请日：2013-03-13
申请人： Dow Global Technologies LLC
发明人： Teresa P. Karjala , Lori L. Kardos , Wallace W. Yau , Jose Ortega , Alfred E. Vigil, Jr.
IPC分类号： C08F210/00 , C08F210/02
CPC分类号： C08F110/02 , C08J5/18 , C08J2323/06 , C08F10/00 , C08F4/38 , C08F2500/04 , C08F2500/05 , C08F2500/10 , C08F2500/11 , C08F2500/12 , C08F2500/17 , C08F2500/26 , C08F2/001
摘要： An ethylene-based polymer, which is a low density polyethylene (LDPE), obtained by free radical polymerization of ethylene, and wherein the LDPE has a GPC parameter “LSP” less than 1.60.An ethylene-based polymer that comprises the following features: a) at least 0.1 amyl groups per 1000 total carbon atoms; b) a melt index of 0.01 to 0.3; c) a z-average molecular weight of Mz (conv.) of greater than 350,000 g/mol and less than 425,000 g/mol; d) a gpcBR value from 1.50 to 2.05, and e) a MWD(conv) [Mw(conv)/Mn(conv)] from 6 to 9. An ethylene-based polymer that comprises the following features: a) at least 0.1 amyl groups per 1000 total carbon atoms; b) a melt viscosity ratio (V0.1/V100), at 190° C., greater than, or equal to, 58; c) a melt viscosity at 0.1 rad/s, 190° C., greater than, or equal to, 40,000 Pa·s, and d) a gpcBR value from 1.50 to 2.25.
摘要翻译：通过乙烯的自由基聚合获得的低密度聚乙烯（LDPE）的乙烯类聚合物，其中LDPE具有小于1.60的GPC参数“LSP”。一种乙烯基聚合物，其包含以下特征：a）每1000个总碳原子至少0.1个戊基; b）熔体指数为0.01至0.3; c）大于350,000g / mol且小于425,000g / mol的Mz（转化）的z-平均分子量; d）gpcBR值为1.50至2.05，e）MWD（conv）[Mw（conv）/ Mn（conv）]为6至9.一种乙烯基聚合物，其包含以下特征：a）至少0.1 每1000个总碳原子的戊基; b）熔体粘度比（V0.1 / V100），在190℃，大于或等于58; c）0.1rad / s，190℃，大于或等于40,000Pa·s的熔体粘度，和d）gpcBR值为1.50-2.25。

9. 发明授权

US08409782B2 Photoresist composition comprising photoinitiators, and transparent thin film and liquid crystal display device using the composition 有权
标题翻译：包含光引发剂的光致抗蚀剂组合物和使用该组合物的透明薄膜和液晶显示装置
公开(公告)号：US08409782B2
公开(公告)日：2013-04-02
申请号：US12674408
申请日：2009-06-22
申请人： Keon Woo Lee , Sung Hyun Kim , Sang Kyu Kwak , Dong Kung Oh , Chang Soon Lee , Chang Ho Cho , Kyoung Hoon Min
发明人： Keon Woo Lee , Sung Hyun Kim , Sang Kyu Kwak , Dong Kung Oh , Chang Soon Lee , Chang Ho Cho , Kyoung Hoon Min
IPC分类号： G03F7/00 , G03F7/004 , G03F7/027 , G03F7/028
CPC分类号： C08F4/38 , G02F1/13394 , G02F2001/133519 , G02F2001/13398 , G03F7/0007 , G03F7/0045 , G03F7/029 , G03F7/031
摘要： A photoresist composition is provided. The photoresist composition comprises two or more kinds of photoinitiators having different activation wavelengths whose difference is at least 20 nm. The photoresist composition has high sensitivity and forms a pattern whose thickness is easy to control depending on the exposure intensity through a slit or transflective mask. Further provided are a transparent thin film formed using the photoresist composition and a liquid crystal display device comprising the thin film.
摘要翻译：提供光致抗蚀剂组合物。光致抗蚀剂组合物包含具有不同激活波长的两种或更多种光引发剂，其差异为至少20nm。光致抗蚀剂组合物具有高灵敏度，并且根据通过狭缝或透反掩模的曝光强度形成其厚度易于控制的图案。还提供了使用光致抗蚀剂组合物形成的透明薄膜和包括该薄膜的液晶显示装置。

10. 发明授权

US08283431B2 Increased polymerization reactor output by using a specific initiator system 有权
标题翻译：通过使用特定的引发剂体系增加聚合反应器的输出
公开(公告)号：US08283431B2
公开(公告)日：2012-10-09
申请号：US10553971
申请日：2004-04-27
申请人： Hans Westmijze , Lambertus Meulenbrugge , Koen Antoon Kornelis Vanduffel , Andreas Petrus Van Swieten
发明人： Hans Westmijze , Lambertus Meulenbrugge , Koen Antoon Kornelis Vanduffel , Andreas Petrus Van Swieten
IPC分类号： C08F14/06
CPC分类号： C08F4/38 , C08F14/06 , C08F2/18
摘要： The invention pertains to a process to polymerize one or more monomers wherein at most 90% w/w of a safely useable amount of a first initiator is used and a second initiator is dosed at least after the start of the polymerization, in an amount such that essentially the full cooling capacity of the polymerization reactor is used, resulting in a cost efficient process to make polymers, particularly polymers comprising polymerized vinyl chloride.
摘要翻译：本发明涉及一种使一种或多种单体聚合的方法，其中使用至多90％w / w的可安全使用量的第一引发剂，并且至少在聚合开始后给予第二引发剂，其量等于基本上使用聚合反应器的完全冷却能力，导致制造聚合物，特别是包含聚合氯乙烯的聚合物的成本有效的方法。

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