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1. 发明申请

US20180086856A1 Method and apparatus for the preparation of a polyolefin 审中-公开
公开(公告)号：US20180086856A1
公开(公告)日：2018-03-29
申请号：US15566157
申请日：2016-04-13
申请人： Linde Aktiengesellschaft
发明人： Andreas MEISWINKEL , Helmut FRITZ , Hans-Jörg ZANDER , Anton KIRZINGER , Josef FREISINGER , Can ULUBAY , Walter HESCH , Thomas WINKLER , Anina WÖHL
IPC分类号： C08F2/34 , C08F2/01 , C08F6/00 , C08F6/02 , C08L23/00 , C07F5/06
CPC分类号： C08F2/34 , C07F5/066 , C08F2/001 , C08F2/01 , C08F6/001 , C08F6/02 , C08L23/00 , C08F10/00
摘要： A method (100) is proposed for the preparation of a polyolefin from olefin monomers, wherein the olefin monomers are subjected to one or more polymerisation steps (13), in which a proportion of the olefin monomers are catalytically reacted to form the polyolefin, while the olefin monomers that are not reacted in the polymerisation step or steps (13) are at least partly transferred into one or more gaseous, monomer-containing purge streams (g, h), which additionally contain(s) one or more aluminium organic compounds, which comprise one or more co-catalysts used in the polymerisation step or steps (13) and/or one or more compounds formed from the co-catalyst(s). It is provided that, downstream of one or more olefin synthesis steps (21), the gaseous, monomer-containing purge stream or streams (g, h) are brought into contact with a crude gas mixture (p, r) formed using a product mixture from the olefin synthesis step or steps (21) and are subjected to a caustic wash (26) together with the crude gas mixture (p, r). The present invention also relates to a corresponding apparatus.

2. 发明授权

US09783654B2 Additives and methods for terminating polymerization and/or reducing viscosity of polymer solution 有权
公开(公告)号：US09783654B2
公开(公告)日：2017-10-10
申请号：US13721544
申请日：2012-12-20
申请人： CHINA PETROLEUM & CHEMICAL CORPORATION , BEIJING UNIVERSITY OF CHEMICAL TECHNOLOGY
发明人： Yixian Wu , Wei Hua , Han Zhu , Liangxing Ma , Yanqin Hao , Ximing Zhao , Guojun Zheng , Changqing Duan , Jun Qi , Qijun Mu
IPC分类号： C08K5/09 , C08F2/42 , C08F6/02 , C09K3/00
CPC分类号： C08K5/09 , C08F2/42 , C08F6/02 , C09K3/00
摘要： The present disclosure provides an additive and a method for terminating polymerization and/or reducing viscosity of polymer solution. The additive comprises a carboxylic acid, an alcohol, a salt chosen from alkali metal salts, alkaline earth metal salts, ammonium salts, and any combination thereof, and optionally, water. The method of the present disclosure comprises adding the additive according to present disclosure into a polymer solution and mixing the resulting mixture. The additive of the present disclosure can terminate living polymer chain ends efficiently and can destroy catalytic active centers and can substantially reduce the viscosity of a polymer solution.

3. 发明申请

US20170260309A1 PARTICULATE POLYVINYL ALCOHOL, PROCESS FOR MAKING AND USES OF THE SAME 审中-公开
公开(公告)号：US20170260309A1
公开(公告)日：2017-09-14
申请号：US15440718
申请日：2017-02-23
申请人： KURARAY AMERICA, INC.
发明人： Michael COLLINS , Ghebrehiwet GHEBREMESKEL , Masaki KATO , Keisuke MORIKAWA , Yoriko IMAOKA
IPC分类号： C08F216/06 , C09D129/04 , D21H19/60 , C08J3/12
CPC分类号： C08F216/06 , C08F6/008 , C08F6/02 , C08F8/12 , C08F16/06 , C08F116/06 , C08F2800/10 , C08J3/12 , C08J2329/04 , C09D129/04 , D21H19/60 , C08F118/08 , C08F218/08 , C08F220/14
摘要： The present invention relates generally to a polyvinyl alcohol composition having higher amorphous polyvinyl alcohol polymer content, a process for making such a polyvinyl alcohol composition, and various end uses thereof.

4. 发明申请

US20170088755A1 PELLICLE INCLUDING A WATER-SOLUBLE ADHESIVE AND PHOTOMASK ASSEMBLY INCLUDING THE PELLICLE 审中-公开
公开(公告)号：US20170088755A1
公开(公告)日：2017-03-30
申请号：US15254701
申请日：2016-09-01
申请人： Samsung Electronics Co., Ltd. , FINE SEMITECH CORP.
发明人： Byungchul YOO , Sungyong CHO , Jaehyuck CHOI , Jeongsu Yang , Donghoon CHUNG , Han-Shin LEE , Myungjun KIM , Ikjun KIM , Jikang KIM , Jeonghwan MIN , Kyoungchae SEO
IPC分类号： C09J133/10 , G03F1/82 , B08B1/00 , C09J133/06 , B08B3/08 , B08B3/12 , G03F1/64 , C09J133/08
CPC分类号： C09J133/10 , C08F6/02 , C08F8/44 , C08F220/06 , C09J133/02 , C09J133/068 , C09J133/08 , C09J133/26 , G03F1/64 , G03F1/82
摘要： A pellicle including a water-soluble adhesive and a photomask assembly including the pellicle are provided. A pellicle may include a membrane, a pellicle frame, and a water-soluble adhesive disposed on the pellicle frame. The water-soluble adhesive may be prepared by a mixture including a water-soluble acrylic adhesive material in an amount of about 40% to about 55% by weight of the mixture, water or a solution of water and alcohol in an amount of about 40% to about 55% by weight of the mixture, and an additive in an amount of about 1% to about 5% by weight of the mixture.

5. 发明授权

US09458274B2 Method of manufacturing terminal-modified polymer 有权
标题翻译：末端改性聚合物的制造方法
公开(公告)号：US09458274B2
公开(公告)日：2016-10-04
申请号：US14770529
申请日：2014-02-21
申请人： The Yokohama Rubber Co., Ltd.
发明人： Kazuya Uenishi , Misao Hiza
IPC分类号： C08F2/38 , C08F4/48 , C08F36/04 , C08F36/08 , C08F236/10 , C08L9/00 , C08F36/00 , C08F4/46 , C08C19/26
CPC分类号： C08F236/10 , C08C19/26 , C08C19/44 , C08F4/46 , C08F6/02 , C08F8/42 , C08F36/00 , C08F136/06 , C08F2810/40 , C08K3/04 , C08K3/06 , C08K3/22 , C08K3/36 , C08K5/09 , C08K5/18 , C08K5/31 , C08K5/47 , C08K5/548 , C08L9/00 , C08L15/00 , C08F12/08 , C08F112/08 , C08F2/44 , C08F4/48 , C08L47/00
摘要： A terminal-modified polymer is manufactured by performing a polymerization reaction of a vinyl aromatic monomer, a conjugated diene monomer or both in the presence of an anionic polymerization initiator: and then adding an alkoxy titanium compound thereinto to terminate the polymerization reaction. Alternatively, a terminal-modified polymer can also be manufactured by adding an titanium halide compound instead of the alkoxy titanium compound to terminate the polymerization reaction, and adding for a reaction with a lower alcohol having 1 to 4 carbon atoms. The resulting terminal-modified polymer can improve the dispersibility of silica used as a compounding agent in rubber compositions for automobile pneumatic tires and the like.
摘要翻译：通过在阴离子聚合引发剂的存在下进行乙烯基芳族单体，共轭二烯单体或二者的聚合反应制造末端改性聚合物，然后向其中加入烷氧基钛化合物以终止聚合反应。或者，端基改性聚合物也可以通过加入卤化钛化合物代替烷氧基钛化合物来终止聚合反应，并加入与具有1至4个碳原子的低级醇反应。所得的末端改性聚合物可以改善用作汽车充气轮胎等的橡胶组合物中作为配混剂使用的二氧化硅的分散性。

6. 发明申请

US20160229930A1 SOLUTION POLYMERIZATION PROCESS WITH IMPROVED ENERGY UTILIZATION 有权
标题翻译：具有改进能源利用的溶液聚合方法
公开(公告)号：US20160229930A1
公开(公告)日：2016-08-11
申请号：US15021796
申请日：2014-09-08
申请人： NOVA CHEMICALS (INTERNATIONAL) S.A.
发明人： Terri A. PRICE , Fazle SIBTAIN , Eric CHELUGET
IPC分类号： C08F10/02
CPC分类号： C08F10/02 , C08F6/003 , C08F6/02 , C08J11/02 , C08F2/06 , C08L23/04
摘要： A solution polymerization process that consumes less energy comprising: injecting feeds into one or more reactors to form a polyethylene in a single liquid phase, or optionally two liquid phases; deactivating the single or dual liquid phase; a first V/L separator separates the deactivated phase into a first bottom stream and a first overhead stream; the first overhead stream passes to a distillation column and the first bottom stream enters a second V/L separator, forming a second overhead stream and a second bottom stream; the second bottom stream enters a third V/L separator, forming a third overhead stream and a third bottom stream; the third bottom stream passes to polymer recovery; the second and third overhead stream are combined, condensed and purified, forming a purified solvent that is recycled to said reactors.
摘要翻译：消耗更少能量的溶液聚合方法包括：将进料注入一个或多个反应器以在单个液相或任选两个液相中形成聚乙烯; 停用单液或双液相; 第一V / L分离器将去活化相分离成第一底部流和第一塔顶流; 第一塔顶流通入蒸馏塔，第一塔底物流进入第二V / L分离器，形成第二塔顶流和第二塔底料流; 第二底部流进入第三V / L分离器，形成第三塔顶流和第三底部流; 第三个底部流进入聚合物回收; 将第二和第三塔顶流合并，浓缩和纯化，形成再循环到所述反应器的纯化溶剂。

7. 发明授权

US09382358B2 Method for producing olefin polymer 有权
标题翻译：烯烃聚合物的制备方法
公开(公告)号：US09382358B2
公开(公告)日：2016-07-05
申请号：US14126090
申请日：2012-06-28
申请人： Jun Kohiruimaki , Masao Aida , Jun Mase , Kana Minamimoto
发明人： Jun Kohiruimaki , Masao Aida , Jun Mase , Kana Minamimoto
IPC分类号： C08F6/02 , C08F10/14 , C08F210/14 , C08F4/6592 , C08F6/00 , C08F4/659
CPC分类号： C08F210/14 , C08F4/65908 , C08F4/65912 , C08F4/65927 , C08F6/008 , C08F6/02 , C08F10/14 , C08L23/0815 , C08F110/14 , C08F2500/17
摘要： A method for producing an olefin polymer including: polymerizing one or more α-olefins each having 6 to 20 carbon atoms in the presence of a metallocene catalyst to obtain an olefin polymer; deactivating and decalcifying the catalyst to obtain a decalcified polymerization reaction liquid; mixing the decalcified polymerization reaction liquid containing the olefin polymer with water; and washing the liquid with stirring at a stirring intensity of 0.1 kW/m3 or more for 1 minute or longer.
摘要翻译：一种制备烯烃聚合物的方法，包括：在金属茂催化剂存在下，聚合一种或多种具有6至20个碳原子的α-烯烃，得到烯烃聚合物; 使催化剂失活和脱钙得到脱钙聚合反应液; 将含有烯烃聚合物的脱钙聚合反应液与水混合; 并在搅拌下以0.1kW / m 3以上的搅拌强度洗涤液体1分钟以上。

8. 发明申请

US20160176994A1 DEVICE AND METHOD FOR RE-CIRCULATING RAW MATERIAL USED WHEN MANUFACTURING POLYBUTENE 有权
标题翻译：在制造聚氨酯时使用的原材料再循环的装置和方法
公开(公告)号：US20160176994A1
公开(公告)日：2016-06-23
申请号：US14908702
申请日：2014-07-29
申请人： DAELIM INDUSTRIAL CO., LTD.
发明人： Myeong Seok KIM , Min Sup PARK , Kyoung Tae MIN
IPC分类号： C08F110/08 , B01J19/24
CPC分类号： C08F110/08 , B01J8/0457 , B01J19/1862 , B01J19/24 , B01J2219/24 , C08F6/003 , C08F6/02 , C08J11/02 , C08F2/01 , C08F4/14 , C08L23/20
摘要： Disclosed are a device and a method for continuously polymerizing polybutene by removing halogen acid, which is included in a reaction raw material, by adsorbing the halogen acid using an adsorbent and then re-supplying the reaction raw material into a reactor. The device for re-circulating the raw material when manufacturing polybutene comprises a reactor, into which a catalyst and a reaction raw material (diluted with an inactive organic solvent) are supplied and polymerized to produce a reaction product; a neutralizing/washing tank for removing the catalyst from the reaction product and neutralizing the reaction product; a separation tank for separating the reaction product into organic compounds and water; a C4 distillation column for distilling an unreacted raw material and the inactive organic solvent from the organic compounds; and an impurity adsorption column for removing halogen acid from the distilled unreacted raw material and the inactive organic solvent using an adsorbent.
摘要翻译：公开了通过使用吸附剂吸附卤酸，然后将反应原料再供给到反应器中，通过除去反应原料中所含的卤素酸来连续聚合聚丁烯的装置和方法。当制备聚丁烯时，用于再循环原料的装置包括反应器，其中供应催化剂和反应原料（用惰性有机溶剂稀释）并聚合以产生反应产物; 用于从反应产物中除去催化剂并中和反应产物的中和/洗涤槽; 用于将反应产物分离成有机化合物和水的分离罐; 用于从有机化合物中蒸馏未反应的原料和无活性有机溶剂的C4蒸馏塔; 以及使用吸附剂从蒸馏的未反应原料和无活性有机溶剂中除去卤素酸的杂质吸附塔。

9. 发明授权

US09040659B2 Methods and materials for removing metals in block copolymers 有权
标题翻译：用于去除嵌段共聚物中金属的方法和材料
公开(公告)号：US09040659B2
公开(公告)日：2015-05-26
申请号：US14175203
申请日：2014-02-07
申请人： Jian Yin , Hengpeng Wu , Muthiah Thiyagarajan , SungEun Hong , Mark Neisser , Yi Cao
发明人： Jian Yin , Hengpeng Wu , Muthiah Thiyagarajan , SungEun Hong , Mark Neisser , Yi Cao
IPC分类号： C08G64/00 , B05D5/00 , B01D15/36 , B01J45/00 , C08J3/00 , B01J39/04 , B01J41/04 , B05D1/00 , B05D3/00 , C08F6/02
CPC分类号： B05D5/00 , B01D15/361 , B01J39/05 , B01J41/07 , B01J45/00 , B05D1/005 , B05D3/00 , C08F6/02 , C08J3/00 , C08L53/00
摘要： The present invention relates to a method for treating a block copolymer solution, wherein the method comprises: providing a solution comprising a block copolymer in a non aqueous solvent; and, treating the solution to remove metals using an ion exchange resin. The invention also relates to a method of forming patterns using the treated block copolymer.
摘要翻译：本发明涉及一种处理嵌段共聚物溶液的方法，其中该方法包括：在非水溶剂中提供包含嵌段共聚物的溶液; 并使用离子交换树脂处理该溶液以除去金属。本发明还涉及使用经处理的嵌段共聚物形成图案的方法。

10. 发明申请

US20150112005A1 Processes to Control Fouling and Improve Compositions 审中-公开
标题翻译：控制结垢和改善成分的过程
公开(公告)号：US20150112005A1
公开(公告)日：2015-04-23
申请号：US14569956
申请日：2014-12-15
申请人： Dow Global Technologies LLC
发明人： Anthony J. Castelluccio , Jeffrey J. Dean , Alec Y. Wang , Lindsey A. Clark , Pradeep Jain , Roger L. Kuhlman , Angela N. Taha , Larry S. Green , Gary R. Marchand , Sean W. Ewart , Jeffrey A. Sims , Chris E. Blaschke , Brandon Fails
IPC分类号： C08F210/14 , C08K5/17 , C08K5/52 , C08K5/098 , C08K5/12
CPC分类号： C08F210/14 , C08F6/02 , C08F210/16 , C08F297/08 , C08F297/083 , C08F2500/03 , C08F2500/08 , C08F2500/11 , C08F2500/12 , C08F2500/19 , C08F2500/20 , C08K5/098 , C08K5/12 , C08K5/17 , C08K5/52 , C08L23/0815 , C08L53/00 , C08L2666/02
摘要： Improved reaction processes comprise reacting a mixture to form a product comprising a metal alkyl, metal oxide, or mixture thereof and then passing said product to a post-reactor heat exchanger. The improvement comprises one or more of the following: (1) reacting said metal alkyl compound with an acid to produce a soluble metal ester; or (2) adding an ionic surfactant; or (3) adding a mixture comprising an antioxidant to the product under conditions sufficient to avoid formation of significant amounts of insoluble metal or metal compounds derived from said metal alkyl compound; or (4) purging said post-reactor heat exchanger with an inert gas under conditions to remove metal oxide from the post-reactor heat exchanger.
摘要翻译：改进的反应方法包括使混合物反应形成包含金属烷基，金属氧化物或其混合物的产物，然后将所述产物通入后反应器热交换器。改进包括以下一个或多个：（1）使所述金属烷基化合物与酸反应以产生可溶性金属酯; 或（2）加入离子表面活性剂; 或（3）在足以避免形成显着量的来自所述金属烷基化合物的不溶性金属或金属化合物的条件下，向产物中加入包含抗氧化剂的混合物; 或（4）在惰性气体下，在从后反应器热交换器中除去金属氧化物的条件下吹扫所述后反应器热交换器。

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