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    • 5. 发明授权
    • Process for production of ferromagnetic powder and apparatus therefor
    • 铁磁粉末生产方法及其设备
    • US4141763A
    • 1979-02-27
    • US784747
    • 1977-04-05
    • Masashi AonumaYasuo TamaiTatsuji KitamotoFumio Kodama
    • Masashi AonumaYasuo TamaiTatsuji KitamotoFumio Kodama
    • B22F9/24H01F1/06
    • B22F9/24H01F1/065
    • A process for producing a ferromagnetic powder comprising injecting a stream of an aqueous solution of a metal salt capable of forming a ferromagnetic substance and a stream of solution containing a reducing material for mixing into a reaction chamber such that the two solutions impinge upon one another causing an oxidation-reduction reaction between them to occur, and applying a magnetic field of 50 oe or more to the particles produced by the oxidation-reduction reaction for the period during which the particles become ferromagnetic particles after going through a superparamagnetic state and an apparatus for use in the practice of the above process comprising a reaction vessel, at least one nozzle for injecting each of a solution of a metal salt and a solution containing a reducing material into the reaction vessel and a magnet for producing a magnetic field in the reaction vessel with the nozzles being open to the magnetic field and positioned so that the solution of the metal salt and the solution of the reducing material when injected are mixed.
    • 一种制造铁磁粉末的方法,包括将能形成铁磁性物质的金属盐的水溶液流和含有还原材料的溶液流混合到反应室中,使得两种溶液彼此撞击导致 在它们之间发生氧化还原反应,并且在通过超顺磁性状态的颗粒变成铁磁颗粒的时期之后,对由氧化还原反应产生的颗粒施加50ee或更大的磁场, 用于上述方法的实践中,包括反应容器,用于将金属盐溶液和含有还原材料的溶液中的每一个注入反应容器的至少一个喷嘴和用于在反应容器中产生磁场的磁体 其中喷嘴对磁场开放并且定位成使得金属盐a的溶液 并且当注入时将还原材料的溶液混合。
    • 7. 发明授权
    • Process for producing cobalt-containing ferromagnetic iron oxide powder
    • 含钴铁磁性氧化铁粉末的生产工艺
    • US4267207A
    • 1981-05-12
    • US39028
    • 1979-05-14
    • Koji SasazawaTatsuji KitamotoGoro AkashiKouichi MasakiShinichiro Dezawa
    • Koji SasazawaTatsuji KitamotoGoro AkashiKouichi MasakiShinichiro Dezawa
    • C01G49/00C01G49/02G11B5/706H01F1/11B05D5/12
    • G11B5/70694C01G49/02G11B5/70642C01P2006/42
    • A process for producing a cobalt-containing ferromagnetic iron oxide powder suitable for magnetic recording which comprises(a) mixing cobalt ion, ferrous ion and an alkali with an aqueous dispersion of acicular ferromagnetic iron oxide nuclei under non-oxidizing conditions at a temperature of about 50.degree. C. or less;(b) heating the dispersion to a temperature of at least about 60.degree. C. but below the boiling point of the dispersion under non-oxidizing conditions to cause a reaction; and(c) treating the dispersion at a temperature of at least about 60.degree. C. but below the boiling point of the dispersion under the following conditions:(1) initially treating the dispersion under non-oxidizing conditions for about 5 minutes or more;(2) subsequentially treating the dispersion under oxidizing conditions for about 5 minutes or more prior to the termination of the reaction; and(3) a total treating time under non-oxidizing conditions and oxidizing conditions of at least about 30 minutes.
    • 一种适用于磁记录的含钴铁磁性氧化铁粉末的制造方法,其特征在于,包括:(a)在非氧化条件下,将钴离子,亚铁离子和碱与针状铁磁性氧化铁核的水分散体混合, 50℃以下; (b)在非氧化条件下将分散体加热到至少约60℃但低于分散体的沸点以引起反应; 和(c)在以下条件下,在至少约60℃但低于分散体沸点的温度下处理分散体:(1)最初在非氧化条件下处理分散体约5分钟或更长时间; (2)在反应终止之前,在氧化条件下将分散体顺序处理约5分钟或更长时间; 和(3)在非氧化条件和氧化条件下的总处理时间为至少约30分钟。
    • 8. 发明授权
    • Process for producing magnetic recording medium
    • 磁记录介质的制造方法
    • US4678682A
    • 1987-07-07
    • US496734
    • 1983-05-20
    • Takamitsu AsaiGoro AkashiTatsuji KitamotoHiroshi ChikamasaTsunehiko Sato
    • Takamitsu AsaiGoro AkashiTatsuji KitamotoHiroshi ChikamasaTsunehiko Sato
    • G11B5/845B05D3/14
    • G11B5/845
    • The perpendicular magnetic orientation of a magnetic layer containing platelet-form ferromagnetic particles coated on a web support is effectively performed by passing a web having thereon the coated magnetic layer in an undried state through a magnetic field formed by plural pairs of opposite pole type magnets disposed in the travelling direction of the web with a gap between adjacent pairs of magnets, while supplying drying air through each gap onto the surface of the travelling web to substantially complete the drying of the coated layer while the web is in the magnetic field. A partition may be inserted in each gap so that the lower end of the partition is close to the upper surface of the travelling web to divide the gap into a front section and a back section, and the drying air may be passed through these sections.
    • 通过使其上具有涂覆的磁性层的卷材在未干燥状态下通过由多对成对的相对极型磁体形成的磁场而使包含在片状载体上的含有片状铁磁颗粒的磁性层的磁性层的垂直磁性取向 在相邻成对的磁体之间具有间隙的幅材的行进方向上,同时通过每个间隙将干燥空气提供到行进幅材的表面上,以在幅材处于磁场的同时基本上完成涂覆层的干燥。 可以在每个间隙中插入隔板,使得隔板的下端靠近行进网的上表面,以将间隙分成前部和后部,并且干燥空气可以通过这些部分。