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1. 发明授权

US4599362A 2-aryl-ethyl ether derivatives and insecticidal and acaricidal agents containing said derivatives 失效
标题翻译： 2-芳基乙醚衍生物和含有所述衍生物的杀虫剂和杀螨剂
公开(公告)号：US4599362A
公开(公告)日：1986-07-08
申请号：US552871
申请日：1983-11-18
申请人： Kiyoshi Nakatani , Satoshi Numata , Tsuneo Inoue , Akira Hosono , Kengo Oda , Yutaka Kubota , Hajime Tachibana , Takatoshi Udagawa , Masatoshi Gohbara
发明人： Kiyoshi Nakatani , Satoshi Numata , Tsuneo Inoue , Akira Hosono , Kengo Oda , Yutaka Kubota , Hajime Tachibana , Takatoshi Udagawa , Masatoshi Gohbara
IPC分类号： C07C43/257 , A01N31/08 , A01N31/14 , A01N31/16 , A01N33/18 , A01N33/20 , A01N37/34 , A01N43/30 , C07B41/04 , C07C17/14 , C07C17/26 , C07C29/124 , C07C29/147 , C07C41/00 , C07C41/01 , C07C43/225 , C07C43/263 , C07C43/267 , C07C43/29 , C07C57/30 , C07C57/58 , C07C59/64 , C07C67/00 , C07C201/00 , C07C205/06 , C07C205/34 , C07C205/37 , C07C253/00 , C07C255/54 , C07C313/00 , C07C323/07 , C07C323/09 , C07C323/16 , C07C323/19 , C07D317/54 , C07D317/56
CPC分类号： C07C17/14 , A01N31/14 , A01N31/16 , C07C17/269 , C07C255/00 , C07C29/124 , C07C29/147 , C07C309/00 , C07C323/00 , C07C43/225 , C07C43/263 , C07C43/267 , C07C43/29 , C07C57/30 , C07C57/58 , C07C59/64 , C07D317/54
摘要： The present invention relates to 2-arylethyl ether or thioether derivatives represented by the following general formula [I]: ##STR1## wherein Ar stands for an aryl group, R.sup.1 stands for straight or branched chain alkyl group of 1 to 6 carbons, R.sup.2 stands for a hydrogen atom, or a methyl or ethyl group, R.sup.3 stands for a halogen atom, or a methyl or methoxyl group, R.sup.4 stands for a hydrogen or halogen atom, or a lower alkyl or lower alkoxy group, and n is an integer of 1 or 2 with the proviso that when n is 2, the groups R.sup.4 may be the same or different, and Y stands for an oxygen or sulfur atom, and also to processes for the preparation of these ethers or thioethers and a use of these ethers or thioethers.These compounds of the present invention have excellent insecticidal and acaricidal activities while the toxicity of these compounds are very low.
摘要翻译：本发明涉及由以下通式[I]表示的2-芳基乙醚或硫醚衍生物：其中Ar代表芳基，R1代表1至6个碳的直链或支链烷基 R2代表氢原子或甲基或乙基，R3代表卤原子或甲基或甲氧基，R4代表氢或卤素原子，或低级烷基或低级烷氧基，n是 1或2的整数，条件是当n为2时，基团R 4可以相同或不同，Y表示氧或硫原子，也用于制备这些醚或硫醚的方法和使用的这些醚或硫醚。本发明的这些化合物具有优异的杀虫和杀螨活性，而这些化合物的毒性非常低。

2. 发明授权

US4570005A Process for the preparation of 2-arylpropyl ether or thioether derivatives 失效
标题翻译： 2-芳基丙醚或硫醚衍生物的制备方法
公开(公告)号：US4570005A
公开(公告)日：1986-02-11
申请号：US513930
申请日：1983-07-14
申请人： Kiyoshi Nakatani , Satoshi Numata , Tsuneo Inoue , Kenji Kodaka , Tsutomu Ishii , Teruhiko Toyama , Hajime Tachibana , Takatoshi Udagawa , Masatoshi Gohbara
发明人： Kiyoshi Nakatani , Satoshi Numata , Tsuneo Inoue , Kenji Kodaka , Tsutomu Ishii , Teruhiko Toyama , Hajime Tachibana , Takatoshi Udagawa , Masatoshi Gohbara
IPC分类号： C07C43/04 , A01N25/02 , A01N25/06 , A01N25/14 , A01N25/30 , A01N31/04 , A01N31/08 , A01N31/14 , A01N31/16 , A01N33/20 , A01N35/04 , A01N37/00 , A01N37/34 , A01N37/38 , A01N43/08 , A01N43/30 , A01N47/02 , A01P7/02 , A01P7/04 , C07C17/00 , C07C17/14 , C07C43/164 , C07C43/174 , C07C43/176 , C07C43/20 , C07C43/263 , C07C43/267 , C07C43/275 , C07C43/29 , C07C45/68 , C07C49/76 , C07C49/84 , C07C57/30 , C07C57/58 , C07C59/64 , C07C69/76 , C07C205/00 , C07C319/14 , C07C321/16 , C07C321/24 , C07C323/09 , C07C323/13 , C07C323/20 , C07D307/38 , C07D307/42 , C07D317/54
CPC分类号： C07C17/14 , A01N31/04 , A01N31/14 , A01N31/16 , A01N33/20 , A01N35/04 , A01N37/38 , A01N43/08 , A01N43/30 , A01N47/02 , C07C17/35 , C07C323/00 , C07C43/174 , C07C43/20 , C07C43/263 , C07C43/267 , C07C43/29 , C07C45/68 , C07C49/84 , C07C57/30 , C07C59/64 , C07D307/38 , C07D307/42
摘要： 2-Arylpropyl ether or thioether derivatives represented by the following general formula [I]: ##STR1## wherein Ar stands for an aryl group, R stands for a methyl or ethyl group, Y stands for an oxygen or sulfur atom, and B stands for a group represented by the following formula [II]: ##STR2## or the following general formula [III]: ##STR3## wherein Z stands for an oxygen or sulfur atom or a carbonyl or methylene group, R.sup.1 stands for a hydrogen or halogen atom or a lower alkyl group or a lower alkoxy group, and n is an integer of from 1 to 5 with the proviso that when n is 2 or more, the groups R.sup.1 may be the same or different,are produced by reacting a compound represented by the following formula (V): ##STR4## with a compound represented by the following formula (VI):B--CH.sub.2 --D (VI)wherein Ar, R and B are defined above, A is a halogen atom and D is Y--H in which Y is as defined above,in the presence of a base in dimethylsulfoxide or sulfolane. The compounds thus prepared have excellent insecticidal and acaricidal activities while the toxicity of these compounds are very low.
摘要翻译：由下列通式[I]表示的2-芳基醚或硫醚衍生物：其中Ar表示芳基，R表示甲基或乙基，Y表示氧或硫原子， B表示由下式[II]表示的基团： [II]或以下通式[III]：其中Z表示氧或硫原子或羰基或亚甲基 R1表示氢或卤原子或低级烷基或低级烷氧基，n表示1〜5的整数，条件是当n为2以上时，基团R 1可以相同或不同通过使由下式（V）表示的化合物与下式（VI）表示的化合物反应：B-CH2-D（VI）其中Ar，R和B定义在碱存在下，在二甲基亚砜或环丁砜中，A是卤素原子，D是YH，其中Y如上定义。如此制备的化合物具有优异的杀虫和杀螨活性，而这些化合物的毒性非常低。

3. 发明授权

US4397864A 2-Arylpropyl ether or thioether derivatives and insecticidal and acaricidal agents containing said derivatives 失效
标题翻译： 2-芳基丙醚或硫醚衍生物和含有所述衍生物的杀虫和杀螨剂
公开(公告)号：US4397864A
公开(公告)日：1983-08-09
申请号：US254135
申请日：1981-04-14
申请人： Kiyoshi Nakatani , Satoshi Numata , Tsuneo Inoue , Kenji Kodaka , Tsutomu Ishii , Teruhiko Toyama , Hajime Tachibana , Takatoshi Udagawa , Masatoshi Gohbara
发明人： Kiyoshi Nakatani , Satoshi Numata , Tsuneo Inoue , Kenji Kodaka , Tsutomu Ishii , Teruhiko Toyama , Hajime Tachibana , Takatoshi Udagawa , Masatoshi Gohbara
IPC分类号： C07C43/04 , A01N25/02 , A01N25/06 , A01N25/14 , A01N25/30 , A01N31/04 , A01N31/08 , A01N31/14 , A01N31/16 , A01N33/20 , A01N35/04 , A01N37/00 , A01N37/34 , A01N37/38 , A01N43/08 , A01N43/30 , A01N47/02 , A01P7/02 , A01P7/04 , C07C17/00 , C07C17/14 , C07C43/164 , C07C43/174 , C07C43/176 , C07C43/20 , C07C43/263 , C07C43/267 , C07C43/275 , C07C43/29 , C07C45/68 , C07C49/76 , C07C49/84 , C07C57/30 , C07C57/58 , C07C59/64 , C07C69/76 , C07C205/00 , C07C319/14 , C07C321/16 , C07C321/24 , C07C323/09 , C07C323/13 , C07C323/20 , C07D307/38 , C07D307/42 , C07D317/54 , A61K31/36 , A61K31/085
CPC分类号： C07C17/14 , A01N31/04 , A01N31/14 , A01N31/16 , A01N33/20 , A01N35/04 , A01N37/38 , A01N43/08 , A01N43/30 , A01N47/02 , C07C17/35 , C07C323/00 , C07C43/174 , C07C43/20 , C07C43/263 , C07C43/267 , C07C43/29 , C07C45/68 , C07C49/84 , C07C57/30 , C07C59/64 , C07D307/38 , C07D307/42
摘要： The present invention relates to 2-arylpropyl ether or thioether derivatives represented by the following general formula [I]: ##STR1## wherein Ar stands for an aryl group, R stands for a methyl or ethyl group, Y stands for an oxygen or sulfur atom, and B stands for a group represented by the following formula [II]: ##STR2## or the following general formula [III]: ##STR3## wherein Z stands for an oxygen or sulfur atom or a carbonyl or methylene group, R.sup.1 stands for a hydrogen or halogen atom or a lower alkyl group or a lower alkoxy group, and n is an integer of from 1 to 5 with the proviso that when n is 2 or more, the groups R.sup.1 may be the same or different, and also to processes for the preparation or these ethers of thioethers and a use of these ethers or thioethers.These compounds of the present invention have excellent insecticidal and acaricidal activities while the toxicity of these compounds are very low.
摘要翻译：本发明涉及由以下通式[I]表示的2-芳基丙醚或硫醚衍生物：其中Ar表示芳基，R表示甲基或乙基，Y表示氧或硫原子，B代表由下式[II]表示的基团： [II]或以下通式[III]：其中Z表示氧或硫原子或羰基或亚甲基，R1表示氢或卤素原子或低级烷基或低级烷氧基，n为1〜5的整数，条件是当n为2以上时，基团R 1可以相同或不同，以及硫醚的制备方法或这些醚的使用以及这些醚或硫醚的用途。本发明的这些化合物具有优异的杀虫和杀螨活性，而这些化合物的毒性非常低。

4. 发明授权

US4552894A 2-Fluoroethoxy-substituted benzene derivatives 失效
标题翻译： 2-氟乙氧基取代的苯衍生物
公开(公告)号：US4552894A
公开(公告)日：1985-11-12
申请号：US573472
申请日：1984-01-24
申请人： Tsuneo Inoue , Kiyoshi Nakatani , Kengo Oda , Tutomu Ishii , Takatoshi Udagawa , Shiro Shiraishi
发明人： Tsuneo Inoue , Kiyoshi Nakatani , Kengo Oda , Tutomu Ishii , Takatoshi Udagawa , Shiro Shiraishi
IPC分类号： A01N31/08 , A01N31/14 , A01N31/16 , A01N39/00 , A01N43/16 , A01N43/30 , A01N43/40 , C07C43/225 , C07C43/23 , C07C43/315 , C07C45/71 , C07D317/54 , C07C51/36 , C07D317/44
CPC分类号： C07D317/54 , A01N31/14 , A01N31/16 , A01N39/00 , A01N43/40 , C07C323/00 , C07C43/225 , C07C43/23 , C07C43/315 , C07C45/71
摘要： A 2-fluoroethoxy-substituted benzene derivative represented by the general formula ##STR1## wherein X represents an oxygen or sulfur atom, R.sup.1 and R.sup.2 represent a hydrogen atom or a lower alkyl group, n represents 0 or 1, and A represents a group of the general formula ##STR2## in which R.sup.3 and R.sup.4 represent a hydrogen atom, a halogen atom, a lower alkyl group, a lower alkoxy group, a lower alkylthio group, a lower haloalkyl group, a lower haloalkylthio group or a methylenedioxy group, R.sup.5 and R.sup.6 represent a hydrogen atom or a lower alkyl group, and p and m represent 0 or 1.This compound is useful as an active ingredient of insecticidal and acaricidal agents, and can be produced by reacting a compound of the general formula ##STR3## with a compound of the general formulaA--D (IV)wherein in general formulae (III) and (IV), A, R.sup.1, R.sup.2 and n are as defined above, and one of B and D represents a a halogen atom and the other represents a group of the general formula --X--M in which X is as defined above, and M represents a hydrogen atom or an alkali metal atom or an alkaline earth metal atom, provided that when n is 0, B is the group --X--M and D is a halogen atom.
摘要翻译：由通式（I）表示的2-氟乙氧基取代的苯衍生物，其中X表示氧或硫原子，R 1和R 2表示氢原子或低级烷基，n表示0或1，A表示其中R3和R4表示氢原子，卤素原子，低级烷基，低级烷氧基，低级烷硫基，低级卤代烷基，低级卤代烷硫基，通式或亚甲二氧基，R5和R6表示氢原子或低级烷基，p和m表示0或1.该化合物可用作杀虫剂和杀螨剂的活性成分，可以通过使化合物通式为（III）的通式为其中通式（III）和（IV）中的通式为（Ⅳ）的化合物，A，R1，R2和n如上所定义，B和D之一表示卤原子，另一个表示通式-XM的基团，其中X表示如上所述，M表示氢原子或碱金属原子或碱土金属原子，条件是当n为0时，B为-X-M基团，D为卤素原子。

5. 发明授权

US4157333A Process for preparing piperonal 失效
标题翻译：胡椒醛的制备方法
公开(公告)号：US4157333A
公开(公告)日：1979-06-05
申请号：US862392
申请日：1977-12-20
申请人： Kiyoshi Nakatani , Tsuneo Inoue , Tutomu Nishizawa , Satoshi Numata , Tsutomu Ishii
发明人： Kiyoshi Nakatani , Tsuneo Inoue , Tutomu Nishizawa , Satoshi Numata , Tsutomu Ishii
IPC分类号： C07D317/54
CPC分类号： C07D317/54
摘要： A process for preparing piperonal which comprises the steps of reacting 1,2-methylenedioxybenzene with an N-alkylformanilide and a condensing agent comprising one or more compounds selected from the group consisting of phosgene, phosphorus oxychloride, phosphorus oxybromide, thionyl chloride, thionyl bromide, sulfuryl chloride, sulfuryl bromide, phosphorus trichloride, and phosphorus pentachloride, and then hydrolyzing the resulting reaction product.
摘要翻译：一种制备胡椒醛的方法，包括使1,2-亚甲二氧基苯与N-烷基酰苯胺反应的步骤和包含一种或多种选自光气，三氯氧化磷，三溴化磷，亚硫酰氯，亚硫酰溴，磺酰氯，磺酰溴，三氯化磷和五氯化磷，然后水解所得的反应产物。

6. 发明授权

US4288260A Method of heat treatments of amorphous alloy ribbons 失效
标题翻译：非晶合金带热处理方法
公开(公告)号：US4288260A
公开(公告)日：1981-09-08
申请号：US134132
申请日：1980-03-26
申请人： Harufumi Senno , Hiroshi Sakakima , Yukihiro Yanagiuchi , Tsuneo Inoue , Masatsugu Yamaguchi , Eiichi Hirota
发明人： Harufumi Senno , Hiroshi Sakakima , Yukihiro Yanagiuchi , Tsuneo Inoue , Masatsugu Yamaguchi , Eiichi Hirota
IPC分类号： C21D6/00 , C21D9/56 , C22F1/00 , H01F1/153 , H01F1/00
CPC分类号： H01F1/15341 , C21D9/56 , C21D9/564
摘要： A method of heat treatments of amorphous alloy ribbons comprises the sequential steps of; grinding amorphous alloy ribbon continuously fed at a predetermined speed (V) selectively varied in the range of 1 cm/sec.ltoreq.V.ltoreq.50 cm/sec, to uniformly finish the ribbon, and successively, heat-treating the ribbon with its surface contacting a stationary or rotating heating body having a surface temperature (T) defined in the range of (T.sub.cry -200.degree. C.).ltoreq.V.ltoreq.(T.sub.cry +50.degree. C.), where T.sub.cry is a crystallization point temperature of the alloy, to uniformly enhance the magnetic properties of the ribbon, and to remove the specific curlings inherently caused by so-called splat cooling manufacturing method, without causing any developments of brittleness of the ribbon mentioned above.
摘要翻译：非晶合金带的热处理方法包括以下步骤：在以1cm / sec×50cm / sec的范围内选择性地变化的以预定速度（V）连续进料的非晶态合金带的研磨，以使丝条均匀地完成，并且随后用其表面接触表面温度（T）在（Tcry-200℃）=（Tcry + 50℃）范围内的固定或旋转加热体，其中Tcry为结晶以均匀地提高带的磁特性，并且消除由所谓的丝锥冷却制造方法固有地引起的特定卷曲，而不会引起上述带的脆性的任何变化。

7. 发明授权

US4064224A Method of making fibrous alkali titanates 失效
标题翻译：纤维状碱式钛酸盐的制备方法
公开(公告)号：US4064224A
公开(公告)日：1977-12-20
申请号：US653120
申请日：1976-01-28
申请人： Takashi Kawamata , Tsuneo Inoue , Eiichi Hirota
发明人： Takashi Kawamata , Tsuneo Inoue , Eiichi Hirota
IPC分类号： C01G23/00 , C30B29/62
CPC分类号： C01G23/005 , C01P2002/02 , C01P2004/10 , C01P2004/54 , C01P2004/60 , C01P2004/61 , C01P2006/60
摘要： A method of making fibrous alkali titanates comprising the steps of preparing a mixture including a titanium compound and an alkali metal compound in a molar ratio of 1.0 to 8.0 in terms of TiO.sub.2 :M.sub.2 O (M: Na, K, Rb, Cs), heating said mixture at a temperature of 1200.degree. to 1600.degree. C to the molten (liquid) phase, cooling the thus heated mixture to room temperature , and washing the thus treated product. This method is advantageous because fibrous alkali titanates of large ratio of length to diameter can be easily produced in high yield.
摘要翻译：一种制备纤维状碱式钛酸盐的方法，包括以TiO 2 :M 2 O（M：Na，K，Rb，Cs）换算，摩尔比为1.0-8.0的钛化合物和碱金属化合物的混合物，加热所述混合物在1200至1600℃的温度下与熔融（液体）相一起冷却，将如此加热的混合物冷却至室温，并洗涤如此处理的产物。该方法是有利的，因为可以容易地以高产率生产长径比大的纤维状碱式钛酸盐。

8. 发明授权

US06057447A Quinoline sulfide derivatives 失效
标题翻译：喹啉硫化物衍生物
公开(公告)号：US06057447A
公开(公告)日：2000-05-02
申请号：US147605
申请日：1999-02-01
申请人： Seiichiro Kawashima , Sumio Terada , Kenichi Saito , Toshiaki Suzuki , Hiroya Sasahara , Toshihisa Kanda , Tsuneo Inoue
发明人： Seiichiro Kawashima , Sumio Terada , Kenichi Saito , Toshiaki Suzuki , Hiroya Sasahara , Toshihisa Kanda , Tsuneo Inoue
IPC分类号： C07D215/36 , A61K31/47 , C07D215/16
CPC分类号： C07D215/36
摘要： The present invention is directed to quinoline sulfide derivatives with antibacterial activities selectively against Hp, obtained by reacting quinoline-4(1H)-thione derivatives with halides and represented by the formula I ##STR1## wherein R.sub.1 represents hydrogen or halogen atom, C.sub.1 -C.sub.6 alkoxy, C.sub.1 -C.sub.6 alkylthio or di C.sub.1 -C.sub.6 alkylamino; R.sub.2 and R.sub.3 respectively represent hydrogen atom or C.sub.1 -C.sub.6 alkyl; one of R.sub.4 and R.sub.5 represents hydroxyl group and the other represents hydrogen atom or CR.sub.4 R.sub.5 represents carbonyl; and m and n are integers, m being 1 or 2, n being 0 or 1.
摘要翻译： PCT No.PCT / JP97 / 02641 Sec。 371日期1999年2月1日 102（e）1999年2月1日PCT 1997年7月30日PCT公布。第WO98 / 04529号公报日期：1998年2月5日本发明涉及具有选择性抗Hp的抗菌活性的喹啉硫化物衍生物，其通过使喹啉-4（1H） - 硫酮衍生物与卤化物反应而得到，并由式I表示，其中R1表示氢或卤素原子，C1 -C 1-6烷氧基，C 1 -C 6烷硫基或二C 1 -C 6烷基氨基; R2和R3分别代表氢原子或C1-C6烷基; R4和R5之一表示羟基，另一个表示氢原子或CR4R5表示羰基; m和n为整数，m为1或2，n为0或1。

9. 发明授权

US5362917A Method of controlling a hydroformylation reaction 失效
标题翻译：控制加氢甲酰化反应的方法
公开(公告)号：US5362917A
公开(公告)日：1994-11-08
申请号：US125795
申请日：1993-09-24
申请人： Morimasa Ogawa , Genichi Emoto , Akio Ueda , Takao Kibayashi , Keitaro Nakata , Tsuneo Inoue
发明人： Morimasa Ogawa , Genichi Emoto , Akio Ueda , Takao Kibayashi , Keitaro Nakata , Tsuneo Inoue
IPC分类号： C07C45/50
CPC分类号： C07C45/50
摘要： A method for controlling a hydroformylation reaction for producing an aldehyde by subjecting an olefin, a feed oxo gas containing hydrogen and carbon monoxide, and a recycled gas withdrawn from a reactor and returned to the reactor, to a hydroformylation reaction in the reactor in the presence of a catalyst, which comprises:setting out a target value for the partial pressure of carbon monoxide in the reaction system to control the hydroformylation reaction;detecting the partial pressure of carbon monoxide corresponding to the target value; andcomparing the detected partial pressure of carbon monoxide with the target value to adjust a flow rate of a discharged gas from the reactor; orcomparing the detected partial pressure of carbon monoxide with the target value to adjust a flow rate of the feed oxo gas.
摘要翻译：一种用于通过使烯烃，含氢气和一氧化碳的进料氧气以及从反应器中排出并返回到反应器的再循环气体在存在下在反应器中进行加氢甲酰化反应来控制用于生产醛的加氢甲酰化反应的方法的催化剂，其包括：设定反应体系中一氧化碳分压的目标值以控制加氢甲酰化反应; 检测对应于目标值的一氧化碳的分压; 并将检测到的一氧化碳分压与目标值进行比较，以调节来自反应器的排出气体的流量; 或将检测到的一氧化碳分压与目标值进行比较，以调节进料氧气的流量。

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