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1. 发明授权

US6063145A Fuel compositions containing etheramine alkoxylates 失效
标题翻译：含有醚胺烷氧基化物的燃料组合物
公开(公告)号：US6063145A
公开(公告)日：2000-05-16
申请号：US105773
申请日：1998-06-26
申请人： John M. Larkin , Wei-Yang Su , Terry L. Renken
发明人： John M. Larkin , Wei-Yang Su , Terry L. Renken
IPC分类号： C07C217/50 , C08G65/26 , C10L1/222 , C10L1/238 , C10L1/22 , C07C217/00
CPC分类号： C10L1/2225 , C07C217/50 , C08G65/2624 , C10L1/238
摘要： This invention concerns a fuel additive comprising an etheramine alkoxylate, and fuel compositions and additive concentrates made therefrom. The etheramine alkoxylate may be of formula: ##STR1## where R.sup.1 is a straight or branched alkyl, or alkylaryl; R.sup.2 is independently in each occurrence hydrogen or alkyl from 1 to 6 carbons; R.sup.3 is independently in each occurrence hydrogen or alkyl of from 1 to 6 carbons; m averages from about 2 to about 20; and x and y each independently average from about 0 to 2, where x+y averages from about 1 to about 4.
摘要翻译：本发明涉及一种包含醚胺烷氧基化物的燃料添加剂和由其制备的燃料组合物和添加剂浓缩物。醚胺烷氧基化物可以具有下式：其中R 1是直链或支链烷基或烷基芳基; R2各自独立地为氢或1至6个碳的烷基; R3各自独立地为氢或1至6个碳的烷基; m平均从约2到约20; x和y各自独立地平均为约0至2，其中x + y平均为约1至约4。

2. 发明授权

US5616811A Etheramine alkoxylates 失效
标题翻译：醚胺烷氧基化物
公开(公告)号：US5616811A
公开(公告)日：1997-04-01
申请号：US470692
申请日：1995-06-06
申请人： Jeffrey J. Vipond , John M. Larkin , Terry L. Renken , Howard M. Stridde
发明人： Jeffrey J. Vipond , John M. Larkin , Terry L. Renken , Howard M. Stridde
IPC分类号： C07C217/50 , C11D1/44 , C07C211/03
CPC分类号： C07C217/50 , C11D1/44
摘要： Etheramine alkoxylates are described which have the formula: ##STR1## where R.sup.1 is a straight or branched alkyl, aryl or alkylaryl group of 6 to 22 carbon atoms; R.sup.3 are independently hydrogen or C.sub.1 to C.sub.3 alkyl; m averages from about 1 to about 20; and x and y each independently average from about 0 to 30, where x+y averages from about 2 to about 60. These etheramine alkoxylates have surfactant properties. Further, they may be quaternized to make other compounds which will have useful surfactant properties.
摘要翻译：描述了具有下式的醚胺烷氧基化物：其中R 1是6至22个碳原子的直链或支链烷基，芳基或烷基芳基; R3独立地是氢或C1-C3烷基; m平均从约1到约20; 并且x和y各自独立地平均为约0至30，其中x + y平均为约2至约60.这些醚胺烷氧基化物具有表面活性剂性质。此外，它们可以被季铵化以制备将具有有用的表面活性剂性质的其它化合物。

3. 发明授权

US4806517A Method for making pelleted phosphated catalysts derived from group IVB transition metal oxides and catalysts thus prepared 失效
标题翻译：制备衍生自ⅣB族过渡金属氧化物和如此制备的催化剂的沉淀磷化催化剂的方法
公开(公告)号：US4806517A
公开(公告)日：1989-02-21
申请号：US24932
申请日：1987-03-12
申请人： Steven H. Vanderpool , Lewis W. Watts, Jr. , John M. Larkin , Terry L. Renken
发明人： Steven H. Vanderpool , Lewis W. Watts, Jr. , John M. Larkin , Terry L. Renken
IPC分类号： B01J27/18
CPC分类号： B01J27/18
摘要： This invention is directed to novel catalyst compositions based on a pelleted group IVb transition metal oxide to which about 0.5 to about 7 wt. % of phosphorus is thermally chemically bonded by a novel process wherein the pellets are impregnated with a liquid water-soluble phosphorus compound containing phosphorus-oxygen bonds, thermally treated after removal of unabsorbed liquid for 0.5 to 5 hours at 100.degree.-150.degree. C. to chemically bond the recited amount of phosphorus to the pellets followed by calcination at 200.degree. to 900.degree. C. to stabilize the pellets. Also disclosed is a regenerative process for preparing predominantly linear polyethylenepolyamines from ethylenediamine and monoethanolamine using the novel catalyst compositions.
摘要翻译：本发明涉及基于颗粒基团IVb过渡金属氧化物的新型催化剂组合物，其中约0.5至约7wt。磷的含量通过新方法进行热化学键合，其中将颗粒浸渍在含有磷 - 氧键的液态水溶性磷化合物中，在100-150℃下除去未吸收的液体0.5-5小时后进行热处理。将所述量的磷化学键合到颗粒中，然后在200-900℃下煅烧以稳定颗粒。还公开了使用新型催化剂组合物从乙二胺和单乙醇胺制备主要线型聚亚乙基多胺的再生方法。

4. 发明授权

US4766245A Process for the preparation of polyoxyalkylene polyamines 失效
标题翻译：聚氧化烯多胺的制备方法
公开(公告)号：US4766245A
公开(公告)日：1988-08-23
申请号：US707126
申请日：1985-03-01
申请人： John M. Larkin , Terry L. Renken
发明人： John M. Larkin , Terry L. Renken
IPC分类号： C08G65/32 , C08G65/325 , C07C85/02 , C07C85/06
CPC分类号： C08G65/3255
摘要： An improved method for the manufacture of high molecular weight polyoxyalkylene amines wherein a hydroxy-terminated polyoxyalkylene compound having a molecular weight of at least 500 is reacted with ammonia in the presence of hydrogen and Raney nickel/aluminum under anhydrous reductive amination conditions to provide the corresponding polyoxyalkylene amine in good yield and selectivity.The Raney nickel/aluminum is a nickel/aluminum alloy treated with a base, such as sodium hydroxide, so as to only partially leach the aluminum from the alloy, such that the final product contains from about 60 wt. % to about 75 wt. % of nickel and, correspondingly, from about 25 wt. % to about 40 wt. % of aluminum and is preferably used in nugget form.
摘要翻译：制备高分子量聚氧化烯胺的改进方法，其中分子量至少为500的羟基封端的聚氧化烯化合物在无水还原胺化条件下在氢和阮内镍/铝的存在下与氨反应，以提供相应的聚氧亚烷基胺具有良好的收率和选择性。阮内镍/铝是用碱如氢氧化钠处理的镍/铝合金，以便仅从合金中部分浸出铝，使得最终产物含有约60wt。％至约75wt。的镍，相应地为约25wt。％至约40wt。铝的百分比，优选以熔核形式使用。

5. 发明授权

US06888030B2 Advances in amination 有权
标题翻译：胺化进展
公开(公告)号：US06888030B2
公开(公告)日：2005-05-03
申请号：US10277551
申请日：2002-10-22
申请人： Wei-Yang Su , Wheeler C. Crawford , John M. Larkin
发明人： Wei-Yang Su , Wheeler C. Crawford , John M. Larkin
IPC分类号： C08F8/04 , C07C209/34
CPC分类号： C08F8/04 , C08F10/00
摘要： Inclusion of a branched alcohol in the catalytic hydrogenation reaction involving an aliphatic nitro compound dramatically increases the efficiency of the conversion of nitro groups into amino groups. This discovery is of particular value in the production of polyalkyleneamines via nitration of a polyalkene, such as a polybutene, and its subsequent reduction. The polyalkyleneamines so produced are useful as dispersant additives for motor oils and fuels.
摘要翻译：在涉及脂族硝基化合物的催化氢化反应中包含支链醇显着提高了硝基转化为氨基的效率。该发现在通过聚烯烃如聚丁烯的硝化生产聚亚烷基胺以及随后的还原中是特别有价值的。如此生产的聚亚烷基胺可用作机油和燃料的分散剂添加剂。

6. 发明授权

US5191139A Process for oligomerizing olefins using sulfate-activated group IV oxides 失效
标题翻译：使用硫酸盐活化的IV族氧化物使烯烃低聚的方法
公开(公告)号：US5191139A
公开(公告)日：1993-03-02
申请号：US787164
申请日：1991-11-04
申请人： John R. Sanderson , John F. Knifton , John M. Larkin
发明人： John R. Sanderson , John F. Knifton , John M. Larkin
IPC分类号： B01J21/06 , B01J27/053 , B01J29/06 , C07C2/10 , C07C2/12 , C07C9/22
CPC分类号： B01J21/066 , B01J21/06 , B01J21/063 , B01J27/053 , B01J29/06 , C07C2/10 , C07C2/12 , C07C9/22 , C07C2521/06 , C07C2529/06
摘要： An improved process is disclosed for preparing synthetic lubricant base stocks. Synthetic lubricant base stocks are prepared in good yield by oligomerizing linear olefins using a sulfate-activated Group IV oxide particularly zirconium dioxide, as the catalyst.
摘要翻译：公开了用于制备合成润滑剂基础油料的改进方法。通过使用硫酸盐活化的IV族氧化物（特别是二氧化锆）作为催化剂使线性烯烃低聚制备合成润滑剂基础油料。

7. 发明授权

US5003107A Catalytic method for the reductive amination of poly(oxytetramethyle) glycols 失效
标题翻译：用于还原胺化聚（氧四甲基）二醇的催化方法
公开(公告)号：US5003107A
公开(公告)日：1991-03-26
申请号：US452146
申请日：1989-12-18
申请人： Robert L. Zimmerman , John M. Larkin
发明人： Robert L. Zimmerman , John M. Larkin
IPC分类号： B01J23/88 , C07B61/00 , C07C213/02 , C07C217/42 , C08G65/325
CPC分类号： C07C213/02 , C08G65/3255
摘要： Poly(oxytetramethylene) diamines useful in the preparation of polyamide and polyurea elastomers are prepared by the catalytic reductive amination of a poly(oxytetramethylene) glycol feedstock under reductive amination conditions in the presence of ammonia and hydrogen using a hydrogenation/dehydrogenation catalyst composed of, on an oxide-free basis, about 70 to 75 wt. % of nickel, about 20 to about 25 wt. % of copper, about 0.5 to 5 wt. % of chromium and about 1 to 5 wt. % of molybdenum.

8. 发明授权

US4810261A Reaction product additive and ori-inhibited motor fuel composition 失效
标题翻译：反应产物添加剂和奥利抑制运动燃料组成
公开(公告)号：US4810261A
公开(公告)日：1989-03-07
申请号：US158424
申请日：1988-02-19
申请人： Rodney L. Sung , Milton D. Behrens , Michael A. Caggiano , John F. Knifton , John M. Larkin , Robert L. Zimmerman
发明人： Rodney L. Sung , Milton D. Behrens , Michael A. Caggiano , John F. Knifton , John M. Larkin , Robert L. Zimmerman
IPC分类号： C08G65/26 , C08G65/325 , C08G65/332 , C08G65/338 , C08G69/40 , C10L1/14 , C10L1/16 , C10L1/18 , C10L1/22 , C10L1/224 , C10L1/2383
CPC分类号： C10L1/224 , C08G65/2609 , C08G65/3255 , C08G65/3324 , C08G65/338 , C10L1/143 , C10L1/221 , C10L1/1641 , C10L1/165 , C10L1/1658 , C10L1/2383
摘要： A novel gasoline-soluble reaction product, a concentrate comprising the reaction product dissolved in a hydrocarbon solvent, and a haze-free, deposit-resistant and ORI-inhibited motor fuel composition comprising the reaction product is described. The reaction product is obtained by reacting a dibasic acid anhydride, a novel diamine containing block copolymers with polyoxyalkylene backbones, and a hydrocarbyl polyamine. Motor fuel compositions containing the reaction product additive of the instant invention are haze-free and show improved deposit-resistance and ORI control in comparison with motor fuels without the reaction product. Motor fuel compositions of the instant invention may optionally comprise a polyolefin polymer/copolymer component having a molecular weight range of about 500-3500.
摘要翻译：描述了一种新型汽油可溶的反应产物，包含溶解在烃溶剂中的反应产物的浓缩物和包含该反应产物的无雾度，耐沉积物和ORI抑制的运动燃料组合物。反应产物通过使二元酸酐，新型含二胺嵌段共聚物与聚氧化烯主链和烃基多胺反应获得。含有本发明反应产物添加剂的汽油燃料组合物与无反应产物相比，与无机燃料相比是无雾的，具有改进的耐沉积物和ORI控制。本发明的机动车燃料组合物可任选地包含分子量范围为约500-3500的聚烯烃聚合物/共聚物组分。

9. 发明授权

US4747851A Novel polyoxyalkylene diamine compound and ori-inhibited motor fuel composition 失效
标题翻译：新型聚氧亚烷基二胺化合物和奥利抑制运动燃料组成
公开(公告)号：US4747851A
公开(公告)日：1988-05-31
申请号：US253
申请日：1987-01-02
申请人： Rodney L. Sung , Milton D. Behrens , Michael A. Caggiano , John F. Knifton , John M. Larkin , Robert L. Zimmerman
发明人： Rodney L. Sung , Milton D. Behrens , Michael A. Caggiano , John F. Knifton , John M. Larkin , Robert L. Zimmerman
IPC分类号： C08G65/26 , C08G65/325 , C08L71/02 , C10L1/14 , C10L1/16 , C10L1/22 , C10L1/222 , C10L1/18
CPC分类号： C10L1/2225 , C08G65/2609 , C08G65/3255 , C08L71/02 , C10L1/143 , C10L1/1633 , C10L1/1658
摘要： A novel gasoline-soluble polyoxyalkylene diamine compound, a concentrate comprising the compound dissolved in a hydrocarbon solvent, and a haze-free, deposit-resistant and ORI-inhibited motor fuel composition comprising the compound is described. Motor fuel compositions comprising the novel polyoxyalkylene diamine compound of the instant invention are haze-free and show improved ORI control and carbonaceous deposit inhibition in comparison with conventional motor fuels. Motor fuel compositions of the instant invention may optionally comprise a polyolefin polymer/copolymer component having a molecular weight range of about 500-3500.
摘要翻译：描述了一种新型汽油可溶性聚氧亚烷基二胺化合物，包含溶解在烃溶剂中的化合物的浓缩物和包含该化合物的无雾度，耐沉积物和ORI抑制的运动燃料组合物。包含本发明新型聚氧化亚烷基二胺化合物的汽油燃料组合物与无机化合物相比是无雾的，并且与传统的机动燃料相比显示出改善的ORI控制和碳沉积抑制。本发明的机动车燃料组合物可任选地包含分子量范围为约500-3500的聚烯烃聚合物/共聚物组分。

10. 发明授权

US4434309A Oligomerization of predominantly low molecular weight olefins over boron trifluoride in the presence of a protonic promoter 失效
标题翻译：在质子促进剂存在下，主要是低分子量烯烃与三氟化硼的低聚
公开(公告)号：US4434309A
公开(公告)日：1984-02-28
申请号：US389737
申请日：1982-06-18
申请人： John M. Larkin , Walter H. Brader, Jr.
发明人： John M. Larkin , Walter H. Brader, Jr.
IPC分类号： C07C2/20 , C10G50/02 , C07C1/16 , C07C5/00
CPC分类号： C10G50/02 , C07C2/20 , C07C2527/1213 , C07C2531/02 , C07C2531/04
摘要： A mixture of predominantly low molecular weight alpha olefins may be oligomerized over a boron trifluoride catalyst and a protonic promoter. When the oligomers are hydrogenated they provide a synthetic lubricant base stock having excellent properties. The alpha olefins may be derived from ethylene polymerization or wax pyrolysis. An inert organic solvent may be present. Preferably, the olefin mixture is made up of greater than 50 weight weight percent of at least one low molecular weight alpha olefin having 4 to 6 carbon atoms and less than 50 weight percent of at least one higher molecular weight alpha olefin having 8 to 18 carbon atoms.
摘要翻译：主要低分子量α-烯烃的混合物可以在三氟化硼催化剂和质子促进剂上低聚。当低聚物被氢化时，它们提供具有优异性能的合成润滑剂基础油料。 α-烯烃可以衍生自乙烯聚合或蜡热解。可能存在惰性有机溶剂。优选地，烯烃混合物由大于50重量％的至少一种具有4至6个碳原子的低分子量α-烯烃和小于50重量％的至少一种具有8至18个碳原子的较高分子量α-烯烃的α-烯烃原子

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