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1. 发明授权

US4810261A Reaction product additive and ori-inhibited motor fuel composition 失效
标题翻译：反应产物添加剂和奥利抑制运动燃料组成
公开(公告)号：US4810261A
公开(公告)日：1989-03-07
申请号：US158424
申请日：1988-02-19
申请人： Rodney L. Sung , Milton D. Behrens , Michael A. Caggiano , John F. Knifton , John M. Larkin , Robert L. Zimmerman
发明人： Rodney L. Sung , Milton D. Behrens , Michael A. Caggiano , John F. Knifton , John M. Larkin , Robert L. Zimmerman
IPC分类号： C08G65/26 , C08G65/325 , C08G65/332 , C08G65/338 , C08G69/40 , C10L1/14 , C10L1/16 , C10L1/18 , C10L1/22 , C10L1/224 , C10L1/2383
CPC分类号： C10L1/224 , C08G65/2609 , C08G65/3255 , C08G65/3324 , C08G65/338 , C10L1/143 , C10L1/221 , C10L1/1641 , C10L1/165 , C10L1/1658 , C10L1/2383
摘要： A novel gasoline-soluble reaction product, a concentrate comprising the reaction product dissolved in a hydrocarbon solvent, and a haze-free, deposit-resistant and ORI-inhibited motor fuel composition comprising the reaction product is described. The reaction product is obtained by reacting a dibasic acid anhydride, a novel diamine containing block copolymers with polyoxyalkylene backbones, and a hydrocarbyl polyamine. Motor fuel compositions containing the reaction product additive of the instant invention are haze-free and show improved deposit-resistance and ORI control in comparison with motor fuels without the reaction product. Motor fuel compositions of the instant invention may optionally comprise a polyolefin polymer/copolymer component having a molecular weight range of about 500-3500.
摘要翻译：描述了一种新型汽油可溶的反应产物，包含溶解在烃溶剂中的反应产物的浓缩物和包含该反应产物的无雾度，耐沉积物和ORI抑制的运动燃料组合物。反应产物通过使二元酸酐，新型含二胺嵌段共聚物与聚氧化烯主链和烃基多胺反应获得。含有本发明反应产物添加剂的汽油燃料组合物与无反应产物相比，与无机燃料相比是无雾的，具有改进的耐沉积物和ORI控制。本发明的机动车燃料组合物可任选地包含分子量范围为约500-3500的聚烯烃聚合物/共聚物组分。

2. 发明授权

US4747851A Novel polyoxyalkylene diamine compound and ori-inhibited motor fuel composition 失效
标题翻译：新型聚氧亚烷基二胺化合物和奥利抑制运动燃料组成
公开(公告)号：US4747851A
公开(公告)日：1988-05-31
申请号：US253
申请日：1987-01-02
申请人： Rodney L. Sung , Milton D. Behrens , Michael A. Caggiano , John F. Knifton , John M. Larkin , Robert L. Zimmerman
发明人： Rodney L. Sung , Milton D. Behrens , Michael A. Caggiano , John F. Knifton , John M. Larkin , Robert L. Zimmerman
IPC分类号： C08G65/26 , C08G65/325 , C08L71/02 , C10L1/14 , C10L1/16 , C10L1/22 , C10L1/222 , C10L1/18
CPC分类号： C10L1/2225 , C08G65/2609 , C08G65/3255 , C08L71/02 , C10L1/143 , C10L1/1633 , C10L1/1658
摘要： A novel gasoline-soluble polyoxyalkylene diamine compound, a concentrate comprising the compound dissolved in a hydrocarbon solvent, and a haze-free, deposit-resistant and ORI-inhibited motor fuel composition comprising the compound is described. Motor fuel compositions comprising the novel polyoxyalkylene diamine compound of the instant invention are haze-free and show improved ORI control and carbonaceous deposit inhibition in comparison with conventional motor fuels. Motor fuel compositions of the instant invention may optionally comprise a polyolefin polymer/copolymer component having a molecular weight range of about 500-3500.
摘要翻译：描述了一种新型汽油可溶性聚氧亚烷基二胺化合物，包含溶解在烃溶剂中的化合物的浓缩物和包含该化合物的无雾度，耐沉积物和ORI抑制的运动燃料组合物。包含本发明新型聚氧化亚烷基二胺化合物的汽油燃料组合物与无机化合物相比是无雾的，并且与传统的机动燃料相比显示出改善的ORI控制和碳沉积抑制。本发明的机动车燃料组合物可任选地包含分子量范围为约500-3500的聚烯烃聚合物/共聚物组分。

3. 发明授权

US5037838A Method for the manufacture of triethylenediamine using a pelleted titania-supported tungstopyrophosphate catalyst 失效
标题翻译：使用沉淀二氧化钛负载的钨磷酸盐催化剂制备三亚乙基二胺的方法
公开(公告)号：US5037838A
公开(公告)日：1991-08-06
申请号：US515003
申请日：1990-04-26
申请人： Robert L. Zimmerman , John F. Knifton
发明人： Robert L. Zimmerman , John F. Knifton
IPC分类号： B01J27/188 , C07B61/00 , C07D487/08
CPC分类号： C07D487/08
摘要： N-hydroxyethyl piperazine is converted to triethylenediamine using a titania-supported tungstopyrophosphate catalyst.

4. 发明授权

US4825000A Phenyl glycidyl ether modified polyoxyalkylene diamines and epoxy resin compositions therefrom 失效
标题翻译：苯基缩水甘油醚改性聚氧化烯二胺及其环氧树脂组合物
公开(公告)号：US4825000A
公开(公告)日：1989-04-25
申请号：US891086
申请日：1986-07-31
申请人： John M. Larkin , Robert L. Zimmerman , Michael Cuscurida , Harold G. Waddill
发明人： John M. Larkin , Robert L. Zimmerman , Michael Cuscurida , Harold G. Waddill
IPC分类号： C08G59/50 , C07C217/08 , C08G18/32 , C08G18/50 , C08G59/00 , C08G65/26 , C08G65/28 , C08G65/32 , C08G65/322 , C08G65/325 , C08G69/26 , C08L63/00 , C07C93/06
CPC分类号： C08G69/26 , C07C217/08 , C08G18/3243 , C08G18/5024 , C08G65/2609 , C08G65/322 , C08G65/3255 , C08L63/00 , C08G2120/00
摘要： A series of polyoxyalkylene diamines modified with phenoxy groups is disclosed. This series of diamines is of the general formula: ##STR1## wherein R.sub.1 and R.sub.2 are independently hydrogen or an alkyl of 1 to 4 carbon atoms, R.sub.3 is a alkyl of 1 to 4 carbon atoms, Ph is phenyl, x ranges from 2 to 40, y ranges from 1 to 20 and z ranges from 1 to 40.These diamines are cured with liquid epoxy resins. The cured resins demonstrated improved tensile strength and modulus, elongation and flexural strength and modulus over a commercially used curative.The diamines are also useful in RIM elastomers, in polyamides and as chain extenders in polyurethane foams.
摘要翻译：公开了一系列用苯氧基改性的聚氧化烯二胺。该系列二胺具有以下通式：其中R 1和R 2独立地为氢或1至4个碳原子的烷基，R 3为1至4个碳原子的烷基，Ph为苯基， x的范围为2至40，y为1至20，z为1至40.这些二胺用液体环氧树脂固化。固化树脂表现出比商业使用的固化剂更好的拉伸强度和模量，伸长率和弯曲强度和模量。二胺也可用于RIM弹性体，聚酰胺和聚氨酯泡沫中的扩链剂。

5. 发明授权

US5003107A Catalytic method for the reductive amination of poly(oxytetramethyle) glycols 失效
标题翻译：用于还原胺化聚（氧四甲基）二醇的催化方法
公开(公告)号：US5003107A
公开(公告)日：1991-03-26
申请号：US452146
申请日：1989-12-18
申请人： Robert L. Zimmerman , John M. Larkin
发明人： Robert L. Zimmerman , John M. Larkin
IPC分类号： B01J23/88 , C07B61/00 , C07C213/02 , C07C217/42 , C08G65/325
CPC分类号： C07C213/02 , C08G65/3255
摘要： Poly(oxytetramethylene) diamines useful in the preparation of polyamide and polyurea elastomers are prepared by the catalytic reductive amination of a poly(oxytetramethylene) glycol feedstock under reductive amination conditions in the presence of ammonia and hydrogen using a hydrogenation/dehydrogenation catalyst composed of, on an oxide-free basis, about 70 to 75 wt. % of nickel, about 20 to about 25 wt. % of copper, about 0.5 to 5 wt. % of chromium and about 1 to 5 wt. % of molybdenum.

6. 发明授权

US06534555B1 Catalyst systems for polyurethane polyester foams 失效
标题翻译：用于聚氨酯聚酯泡沫的催化剂体系
公开(公告)号：US06534555B1
公开(公告)日：2003-03-18
申请号：US09950133
申请日：2001-09-10
申请人： Ernest L. Rister, Jr. , Robert A. Grigsby, Jr. , Robert L. Zimmerman
发明人： Ernest L. Rister, Jr. , Robert A. Grigsby, Jr. , Robert L. Zimmerman
IPC分类号： C08G1818
CPC分类号： C08G18/2018 , B01J31/0237 , B01J31/0247 , C08G18/1841 , C08G2101/0008
摘要： Provided are catalyst systems which produce flexible polyurethane polyester foams that are color stable, are lower in odor, and uses less catalysts than current most commonly practiced technology. The use of lower amounts of catalysts with low vapor pressure reduces worker exposure to alkaline corrosive materials, reduces pollution through less pounds of volatile organic chemicals (VOC's) and is less expensive.
摘要翻译：提供了产生柔性聚氨酯聚酯泡沫的催化剂体系，其颜色稳定，气味较低，并且使用比目前最常用的技术更少的催化剂。使用较少量的低蒸汽压的催化剂可降低工人暴露于碱性腐蚀性物质，减少污染，减少挥发性有机化学物质（VOC），并且成本较低。

7. 发明授权

US5241016A Epoxy adhesives containing aminated, long chain monoepoxide capped polyols 失效
标题翻译：含有胺化长链单环氧化物封端多元醇的环氧粘合剂
公开(公告)号：US5241016A
公开(公告)日：1993-08-31
申请号：US889879
申请日：1992-05-29
申请人： Harold G. Waddill , Robert A. Grigsby, Jr. , Michael Cuscurida , Robert L. Zimmerman
发明人： Harold G. Waddill , Robert A. Grigsby, Jr. , Michael Cuscurida , Robert L. Zimmerman
IPC分类号： C08G59/56 , C08G65/26 , C08G65/325 , C08L63/00 , C09J163/00
CPC分类号： C08G65/3255 , C08G65/2609 , C08L63/00
摘要： The invention is an epoxy resin adhesive composition. The composition comprises:A. An epoxy resin component; andB. A curative component comprising:a curing amount of a polyamine curing agent and 2 to 30 phr. of an adhesion enhancer of comprising a partially hindered polyetherpolyamine.The fast curing adhesive offers high lap shear strength and relatively high peel strength.
摘要翻译：本发明是环氧树脂粘合剂组合物。该组合物包含：A.环氧树脂组分; B.一种固化剂组分，包括：固化量的多胺固化剂和2至30phr。的包含部分受阻的聚醚多胺的粘合增强剂。快速固化粘合剂具有较高的搭接剪切强度和较高的剥离强度。

8. 发明授权

US5239041A Hindered amines to slow down reactivity in producing rim elastomers 失效
标题翻译：受阻胺减缓制备边缘弹性体的反应性
公开(公告)号：US5239041A
公开(公告)日：1993-08-24
申请号：US865170
申请日：1992-04-08
申请人： Robert A. Grigsby, Jr. , Michael Cuscurida , Robert L. Zimmerman , George P. Speranza
发明人： Robert A. Grigsby, Jr. , Michael Cuscurida , Robert L. Zimmerman , George P. Speranza
IPC分类号： C08G18/32 , C08G18/50
CPC分类号： C08G18/5024 , C08G2120/00
摘要： A process for preparing a polyurea reaction injection molded (RIM) elastomer is described. A hindered polyetherpolyamine is first obtained by reacting a polyol having two or more hydroxyl groups with an effective amount of long chain alkyl epoxide to give an at least partially hindered intermediate having hydroxyl terminations; and then aminating at least one of the hydroxyl terminations on the intermediate to primary amine groups to give an at least partially hindered polyetherpolyamine. The hindered polyetherpolyamine is then reacted with a polyisocyanate in the optional presence of a catalyst to give a polyurea RIM elastomer. The long chain alkyl group provides steric hindrance to the primary aliphatic amine group, which slows down the reactivity of the amine. The slower reactivity of the amine group is useful in RIM and RRIM compositions since it allows for longer shot or flow times, which in turn permit larger parts to be made from existing equipment.
摘要翻译：描述了制备聚脲反应注射成型（RIM）弹性体的方法。首先通过使具有两个或多个羟基的多元醇与有效量的长链烷基环氧化物反应得到受阻聚醚多胺，得到具有羟基末端的至少部分受阻的中间体; 然后胺化中间体至伯胺基团上的至少一个羟基端基，得到至少部分受阻的聚醚多胺。然后在任选的催化剂存在下，将受阻聚醚多胺与多异氰酸酯反应，得到聚脲RIM弹性体。长链烷基对主要脂族胺基提供空间位阻，这减慢了胺的反应性。胺基的较慢反应性在RIM和RRIM组合物中是有用的，因为它允许更长的喷射或流动时间，这又允许从现有设备制造更大的部件。

9. 发明授权

US5203879A Fuel composition 失效
标题翻译：燃油组成
公开(公告)号：US5203879A
公开(公告)日：1993-04-20
申请号：US938806
申请日：1992-09-01
申请人： Wei-Yang Su , Sheldon Herbstman , Joseph M. Russo , Robert L. Zimmerman , Michael Cuscurida
发明人： Wei-Yang Su , Sheldon Herbstman , Joseph M. Russo , Robert L. Zimmerman , Michael Cuscurida
IPC分类号： C07C231/10 , C07C237/08 , C08K5/357 , C10L1/22 , C10L1/222 , C10L1/224 , C10L1/2387 , C10L10/00 , C10L10/10
CPC分类号： C08K5/357 , C10L1/221 , C10L1/224 , C10L1/2387 , C10L10/06
摘要： An amido alkanolamine composition obtained by reacting, at a temperature of 10.degree. C.-200.degree. C.:(a) a 4-alkyl-2-morpholinone represented by the formula: ##STR1## in which R represents a monovalent aliphatic radical having from 1 to 10 carbon atoms, and(b) a hydrocarbyl oxypolyoxyalkylene amine represented by the formula: ##STR2## in which R' represents an alkyl, an alicyclic, or a alkylalicyclic radical having from 8 to 30 carbon atoms, x has a value from 5 to 50, and R" represents a methyl radical or a mixture of hydrogen and methyl radicals is provided.
摘要翻译：通过在10℃-200℃的温度下反应获得的酰胺链烷醇胺组合物：（a）由下式表示的4-烷基-2-吗啉酮：其中R表示具有 1〜10个碳原子的烷基，脂环族或碳原子数为8〜30的烷基脂环族基团，式中，x表示碳原子数1〜10的烃基氧基聚氧化烯胺， 5至50，并且R“表示甲基或氢和甲基的混合物。

10. 发明授权

US5075506A Continuous preparation of secondary amines from nitriles using cobalt and zirconium 失效
标题翻译：使用钴和锆连续地制备来自硝酸的二级胺
公开(公告)号：US5075506A
公开(公告)日：1991-12-24
申请号：US506747
申请日：1990-04-10
申请人： Robert L. Zimmerman
发明人： Robert L. Zimmerman
IPC分类号： B01J23/75 , C07B61/00 , C07C209/48 , C07C211/01
CPC分类号： C07C209/48
摘要： A method for producing secondary amines, particularly fatty secondary amines such as ditallowamine from fatty nitriles, such as tallow nitrile over a cobalt catalyst promoted with zirconium has been discovered. The catalyst may be supported on kieselguhr or other support. The reaction gives high selectivity or secondary amine over the coproduced primary and tertiary amines. The reaction may be conducted continuously in the presence of ammonia and hydrogen. The secondary amine proportion may be increased by a second stage using the same catalyst as the first stage, but in the absence of ammonia.

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