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1. 发明授权

US06086639A Black dye mixtures of fiber-reactive azo dyes and use thereof for dyeing hydroxy- and/or carboxamido-containing fiber material 失效
标题翻译：纤维反应性偶氮染料的黑色染料混合物及其用于染色含羟基和/或羧酰氨基的纤维材料的用途
公开(公告)号：US06086639A
公开(公告)日：2000-07-11
申请号：US265256
申请日：1999-03-09
申请人： Joachim Steckelberg , Werner Hubert Russ , Christian Schumacher , Ron Pedemonte
发明人： Joachim Steckelberg , Werner Hubert Russ , Christian Schumacher , Ron Pedemonte
IPC分类号： C09B62/51 , C09B62/513 , C09B67/22 , D06P1/384 , D06P3/10 , D06P3/66 , D06P1/38 , D06P1/382
CPC分类号： C09B67/0047 , D06P1/384 , Y10S8/918
摘要： The present invention comprises a dye mixture comprising one or more, such as one, two or three, disazo dyes conforming to the general formula (1), one or more, such as one, two or three, monoazo dyes conforming to the general formula (2), and one or more, such as one, two or three dyes of the general formulae (3) and (4) wherein the formulae (1) to (4) are defined as given in claim 1, a method for its preparation and a process for dyeing hydroxy- and/or carboxamido containing fiber material in which a inventive dye is applied to the material.
摘要翻译：本发明包括染料混合物，其包含一种或多种，例如一种，两种或三种符合通式（1）的双偶氮染料，一种或多种，如一种，两种或三种符合通式的单偶氮染料（2）和一种或多种如通式（3）和（4）的一种，两种或三种染料，其中式（1）至（4）定义如权利要求1所述，其方法为制备和染色含有本发明染料的含羟基和/或羧酰胺的纤维材料的方法。

2. 发明授权

US5760193A Triazinyl-substituted fiber-reactive azo dyes wherein the triazinyl groups bear an N-containing substituent, and methods of using same 失效
标题翻译：三嗪基取代的纤维反应性偶氮染料及其使用方法
公开(公告)号：US5760193A
公开(公告)日：1998-06-02
申请号：US749842
申请日：1996-11-15
申请人： Werner Hubert Russ , Christian Schumacher , Wolfram Reddig
发明人： Werner Hubert Russ , Christian Schumacher , Wolfram Reddig
IPC分类号： C09B62/51 , C09B62/44 , C09B62/507 , C09B62/08 , D06P1/38
CPC分类号： C09B62/4401
摘要： Fiber-reactive azo dyes, processes for their preparation and their use Azo dyes of the formula (1) given and defined below are described, which dyes contain fiber-reactive groups and dye hydroxy- and/or carboxamido-containing materials, in particular fiber materials, such as cotton, wool and synthetic polyamide fibers, in shades of high color strength and good fastness properties. ##STR1## in which D is the radical of a diazo component from the benzene or naphthalene series, K is the radical of a coupling component of the formula (2) ##STR2## in which M is hydrogen or an alkali metal, a and b are each zero or 1, R.sup.1 and R.sup.2 are each hydrogen or substituted or unsubstituted alkyl, Y is attached to --NR.sup.1 -- or --NR.sup.2 -- and is a radical of the formula (3) ##STR3## in which R is hydrogen, substituted or unsubstituted alkyl or substituted or unsubstituted phenyl, A is the radical of an amine or of an N-containing heterocycle, lower alkoxy or phenoxy, c is zero or 1, G is substituted or unsubstituted phenylene, B is lower alkylene or ethyleneoxyethylene and the group --SO.sub.2 --X is .beta.-hydroxyethylsulfonyl or a fiber-reactive group from the vinylsulfone series and Z is a heterocyclic fiber-reactive radical which is attached to --NR.sup.1 -- or --NR.sup.2 -- and is different from Y.
摘要翻译：纤维反应性偶氮染料，其制备方法及其用途描述了下文给出和定义的式（1）的偶氮染料，其中染料含有纤维反应性基团和染料含羟基和/或甲酰氨基的材料，特别是纤维材料，如棉，羊毛和合成聚酰胺纤维，色泽高，色牢度好。（1）其中D是来自苯或萘系的重氮组分的基团，K是式（2）金属的偶合组分的基团，a和b各自为0或1，R 1和 R 2各自为氢或取代或未取代的烷基，Y连接到-NR 1 - 或-NR 2 - 并且是式（3）的基团，其中R是氢，取代或未取代的烷基或被取代或未取代的未取代的苯基，A是胺或含N杂环，低级烷氧基或苯氧基的基团，c为0或1，G为取代或未取代的亚苯基，B为低级亚烷基或亚乙氧基乙烯基团，基团-SO2-X为 β-羟基乙基磺酰基或来自乙烯基砜系列的纤维反应性基团，Z是与-NR 1 - 或-NR 2 - 连接且不同于Y的杂环纤维反应性基团。

3. 发明授权

US5744622A water-soluble, fiber-reactive anthraquinone compounds 失效
标题翻译：水溶性纤维反应性蒽醌化合物
公开(公告)号：US5744622A
公开(公告)日：1998-04-28
申请号：US571573
申请日：1995-12-13
申请人： Werner Hubert Russ , Christian Schumacher
发明人： Werner Hubert Russ , Christian Schumacher
IPC分类号： C09B62/505 , D06P1/38 , D06P1/384 , C09B1/24 , C09B1/34
CPC分类号： C09B62/505 , D06P1/38
摘要： The invention relates to anthraquinone compounds of the formula (1) ##STR1## wherein the substituents are as defined in the specification. The compounds of formula (1) are water-soluble, fiber-reactive dyes useful for dyeing and printing materials, in particular fiber materials containing hydroxy, mecapto, amino and/or carboxamide groups.
摘要翻译：本发明涉及式（1）的蒽醌化合物，其中取代基如说明书中所定义。式（1）的化合物是可用于染色和印刷材料的水溶性纤维反应性染料，特别是含有羟基，甲基封端，氨基和/或羧酰胺基团的纤维材料。

4. 发明授权

US5672738A Process for the preparation of 3-(N-aryl-amino)-propyl-2'-sulfatoethyl-sulfonyl compounds 失效
标题翻译：制备3-（N-芳基 - 氨基） - 丙基-2'-磺基乙基 - 磺酰基化合物的方法
公开(公告)号：US5672738A
公开(公告)日：1997-09-30
申请号：US560539
申请日：1995-11-17
申请人： Christian Schumacher , Michael Meier , Werner Hubert Russ
发明人： Christian Schumacher , Michael Meier , Werner Hubert Russ
IPC分类号： C07B61/00 , C07C303/24 , C07C315/02 , C07C315/06 , C07C317/28 , C07C317/36 , C07C319/14 , C07C323/25 , C07D265/10 , C07F5/02
CPC分类号： C07C315/04 , C07C303/24 , C07C315/02 , C07C319/14 , C07C323/25 , C07D265/10
摘要： Process for the preparation of 3-(N-aryl-amino)-propyl-2'-sulfatoethyl-sulfonyl compounds Compounds of the formula (1) Ar--NH--(CH.sub.2).sub.3 --SO.sub.2 --(CH.sub.2).sub.2 --OSO.sub.3 M(1) are prepared by reacting a compound of the formula (2) ##STR1## with 2-mercaptoethanol to give a compound of the formula (3) Ar--NH--(CH.sub.2).sub.3 --S--(CH.sub.2).sub.2 --OH (3) at temperatures from 90.degree. to 270.degree. C. in the presence of a catalytic amount of a base, subsequently oxidizing the compound of the formula (3) to give a compound of the formula (4) Ar--NH--(CH.sub.2).sub.3 --SO.sub.2 --(CH.sub.2).sub.2 --OH(4), and finally esterifying the compound of the formula (4) with at least one molar equivalent of sulfuric acid, oleum or halosulfonic acid to give a compound of the formula (1). Compounds of the formula (1) are valuable starting compounds for the preparation of reactive dyestuffs.
摘要翻译：制备3-（N-芳基 - 氨基） - 丙基-2'-磺基乙基 - 磺酰基化合物的方法式（1）的化合物Ar-NH-（CH2）3-SO2-（CH2）2-OSO3M ）通过使式（2）的化合物与（2-）巯基乙醇反应，得到式（3）Ar-NH-（CH 2）3 -S-（CH 2）2 -OH的化合物（3）在90℃至270℃的温度下，在催化量的碱存在下，随后氧化式（3）化合物，得到式（4）化合物Ar-NH-（CH 2 ）3-SO 2 - （CH 2）2 -OH（4），最后用至少一摩尔当量的硫酸，发烟硫酸或卤代磺酸酯化式（4）的化合物，得到式（1）的化合物，。式（1）的化合物是用于制备活性染料的有价值的起始化合物。

5. 发明授权

US07381256B2 Mixtures of fiber-reactive azo dyes, their production and their use 失效
标题翻译：纤维反应性偶氮染料的混合物，其制备及其用途
公开(公告)号：US07381256B2
公开(公告)日：2008-06-03
申请号：US11547734
申请日：2005-04-09
申请人： Stefan Meier , Uwe Reiher , Werner Hubert Russ , Christian Schumacher
发明人： Stefan Meier , Uwe Reiher , Werner Hubert Russ , Christian Schumacher
IPC分类号： C09D11/00 , C09B62/085 , C09B67/22
CPC分类号： C09B67/0052
摘要： The present invention relates to a dye mixture which comprises at least one dye of the general formula (I) and at least one dye of the general formula (II) in which D1, D2, W1, W2, Y1, Y2, R1 to R6, M, m and n are defined as indicated in claim 1, to processes for preparing them, to their use, and to inks comprising them for digital printing.
摘要翻译：本发明涉及染料混合物，其包含至少一种通式（I）的染料和至少一种通式（II）的染料，其中D 1，D 2， W 1，W 2，Y 1，Y 2，R 1，对于R 6，M，m和n如权利要求1所述定义，用于制备它们的用途和用于数字印刷的包含它们的油墨的方法。

6. 发明授权

US5780602A Dyestuff mixtures of fiber-reactive azo dyestuffs and their use for dyeing fiber material containing hydroxyl and/or carboxamide groups 失效
标题翻译：纤维反应性偶氮染料的染料混合物及其用于染色含有羟基和/或羧酰胺基团的纤维材料的用途
公开(公告)号：US5780602A
公开(公告)日：1998-07-14
申请号：US924746
申请日：1997-09-05
申请人： Christian Schumacher , Werner Hubert Russ
发明人： Christian Schumacher , Werner Hubert Russ
IPC分类号： C09B62/51 , C09B67/22 , C09B67/38 , C09B67/40 , D06P3/10 , D06P3/66 , D06P1/384
CPC分类号： C09B62/51 , C09B67/0047
摘要： Mixtures of fiber-reactive azo dyestuffs with which black dyeings, including prints, are obtained on fiber materials containing hydroxy and/or carboxamide groups, such as cellulosic fiber materials, wool and synthetic polyamide fibers, are described. These dyestuffs mixtures comprise one or more dyestuffs of the following formulae (1) and (2): ##STR1## in which the substituents have the meaning given in the specification.
摘要翻译：描述了纤维反应性偶氮染料与含有羟基和/或羧酰胺基团的纤维材料（如纤维素纤维材料，羊毛和合成聚酰胺纤维）上得到的黑色染色（包括印花）的混合物。这些染料混合物包含一种或多种下列通式（1）和（2）的染料：说明书中的（2） n。

7. 发明授权

US5777111A Process for the preparation of 3-(N-Aryl-amino)-propyl-2'-sulfato-ethylsulfonyl compounds 失效
标题翻译： 3-（N-芳基 - 氨基） - 丙基-2'-磺酰基 - 乙基磺酰基化合物的制备方法
公开(公告)号：US5777111A
公开(公告)日：1998-07-07
申请号：US862549
申请日：1997-05-23
申请人： Christian Schumacher , Michael Meier , Werner Hubert Russ
发明人： Christian Schumacher , Michael Meier , Werner Hubert Russ
IPC分类号： C07B61/00 , C07C303/24 , C07C315/02 , C07C315/06 , C07C317/28 , C07C317/36 , C07C319/14 , C07C323/25 , C07D265/10 , C07D413/12
CPC分类号： C07C315/04 , C07C303/24 , C07C315/02 , C07C319/14 , C07C323/25 , C07D265/10
摘要： A compound of the formula (2a) ##STR1## in which Ar.sup.1 is 2-sulfophenyl, 3-sulfophenyl, 4-sulfophenyl, 2,5-disulfophenyl, 3-sulfo-4-aminophenyl, 4-sulfo-3-aminophenyl, 3-methoxy-5-sulfophenyl, 3-sulfo-4-methylphenyl, 3-sulfo-4-methoxyphenyl, 2,5-disulfo-4-methylphenyl, 2,5-disulfo-4-methoxyphenyl, 2,5-disulfo-4-aminophenyl, 5,7-disulfo-naphth-2-yl, 4,8-disulfo-naphth-2-yl, 3,6,8-trisulfo-napth-2-yl, 4,6,8-trisulfo-naphth-2-yl, 8-sulfonaphth-1-yl, 6-sulfo-naphth-1-yl or 7-sulfo-naphth-1-yl.
摘要翻译：其中Ar1是2-磺基苯基，3-磺基苯基，4-磺基苯基，2,5-二磺基苯基，3-磺基-4-氨基苯基，4-磺基-3-氨基苯基，氨基苯基，3-甲氧基-5-磺基苯基，3-磺基-4-甲基苯基，3-磺基-4-甲氧基苯基，2,5-二磺基-4-甲基苯基，2,5-二磺基-4-甲氧基苯基，二磺基-4-氨基苯基，5,7-二磺基萘-2-基，4,8-二磺基 - 萘-2-基，3,6,8-三磺基萘-2-基，三磺基萘-2-基，8-磺基-1-基，6-磺基 - 萘-1-基或7-磺基 - 萘-1-基。

8. 发明申请

US20080194817A1 Reactive Dyestuffs, Method for the Production Thereof, and Use of the Same 审中-公开
标题翻译：活性染料，其生产方法及其用途
公开(公告)号：US20080194817A1
公开(公告)日：2008-08-14
申请号：US11909684
申请日：2006-03-21
申请人： Stefan Meier , Uwe Reiher , Werner Hubert Russ
发明人： Stefan Meier , Uwe Reiher , Werner Hubert Russ
IPC分类号： C07D251/12
CPC分类号： C09D11/328 , C09B62/4415
摘要： Dyes of the hereinbelow indicated and defined formula (1) where R and M are each as defined in claim 1, process for their preparation and their use for dyeing and printing hydroxyl- and carboxamido-containing material.
摘要翻译：下面指出和定义的式（1）的染料，其中R和M各自如权利要求1中所定义，其制备方法及其用于染色和印刷含羟基和羧酰氨基的材料的用途。

9. 发明授权

US07632316B2 Reactive dyestuff, method for production thereof and use of the same 有权
标题翻译：活性染料，其制造方法及其用途
公开(公告)号：US07632316B2
公开(公告)日：2009-12-15
申请号：US11915955
申请日：2006-05-24
申请人： Stefan Meier , Uwe Reiher , Werner Hubert Russ , Günther Schwaiger
发明人： Stefan Meier , Uwe Reiher , Werner Hubert Russ , Günther Schwaiger
IPC分类号： C09B62/00
CPC分类号： C09B62/4413 , C09B67/0052
摘要： The present invention relates to dyes of the general formula (1) where M and X are each as defined in claim 1, dye mixtures comprising one or more of the dyes of the general formula (1) and also one or more further fiber-reactive dyes, processes for their preparation, their use and printing inks comprising same.
摘要翻译：本发明涉及通式（1）的染料，其中M和X各自如权利要求1所定义，染料混合物包含一种或多种通式（1）的染料以及一种或多种另外的纤维反应性染料，它们的制备方法，它们的用途和包含它们的印刷油墨。

10. 发明申请

US20080280053A1 Reactive Dyes Containing Divalent Sulfur in Non-Reactive Side Chain at Trizine Nucleus 审中-公开
标题翻译：在三重核的非反应性侧链中含有二价硫的活性染料
公开(公告)号：US20080280053A1
公开(公告)日：2008-11-13
申请号：US11719756
申请日：2005-11-15
申请人： Anthony Lawrence , Werner Hubert Russ , Warren J. Ebenezer
发明人： Anthony Lawrence , Werner Hubert Russ , Warren J. Ebenezer
IPC分类号： B05D1/02 , C09B29/00
CPC分类号： C09D11/328 , C09B62/04
摘要： The present invention refers to dyestuffs of the formula (I) wherein R1, R2 are independently H, optionally substituted alkyl or optionally substituted aryl, R3 is optionally substituted alkyl or optionally substituted aryl, an organic acyl group (i.e. acetyl, propionyl, benzoyl etc.) or an organic thioacyl group (i.e. 10 thioacetyl, thiopropionyl, thiobenzoyl etc.), all of which may or may not bear a reactive group able to form a dye-fibre bond, R4 is any coloured organic group, which may or may not bear a reactive group able to form a dye-fibre bond, L is any carbon containing linking group that is aliphatic, aromatic, or a combined alkyl-aryl group such as benzyl or phenethyl, X is halogen or tertiary ammonium or an optionally substitute aryl amine, processes for the preparation of said dyestuffs and their use for dyeing and printing hydroxy- and/or carboxamido-containing fiber materials.
摘要翻译：本发明涉及式（I）的染料，其中R 1，R 2独立地为H，任意取代的烷基或任选取代的芳基，R 3，任选取代的烷基或任选取代的芳基，有机酰基（即乙酰基，丙酰基，苯甲酰基等）或有机硫代酰基（即10个硫代乙酰基，硫代丙酰基，硫代苯甲酰基等），所有这些可能或不可能承载能够形成染料纤维键的反应性基团，R 4是任何有色有机基团，其可以或不具有能够形成染料 - 纤维键的反应性基团，L是任何碳含有连接基团，其为脂族，芳族或组合的烷基 - 芳基如苄基或苯乙基，X为卤素或叔铵或任选取代的芳基胺，制备所述染料的方法及其用于染色和印刷羟基 - 和/或含羧酰氨基的纤维材料。

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