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1. 发明公开

US20230399286A1 IMPROVED PROCESS FOR PREPARING METHYL METHACRYLATE AND/OR METHACRYLIC ACID BY REDUCED BACK MIXING DURING CONVERSION 审中-公开
公开(公告)号：US20230399286A1
公开(公告)日：2023-12-14
申请号：US18249917
申请日：2021-10-07
申请人： Röhm GmbH
发明人： Ufuk KOCKESEN , Patrick Wings , Steffen Krill , Florian Klasovsky
IPC分类号： C07C69/54 , C07C67/20 , C07C51/06 , C07C57/04 , C07C231/06 , C07C231/12 , C07C303/24
CPC分类号： C07C69/54 , C07C67/20 , C07C51/06 , C07C57/04 , C07C231/06 , C07C231/12 , C07C303/24
摘要： A process for preparing methyl methacrylate (MMA) and/or methacrylic acid (MAS) having improved yield, involves amidation, conversion, and hydrolysis/esterification. Especially high yields are obtained during the amidation and in the subsequent so-called conversion.

2. 发明授权

US10836717B2 Reagents for fluorosulfating alcohols or amines 有权
公开(公告)号：US10836717B2
公开(公告)日：2020-11-17
申请号：US16103824
申请日：2018-08-14
申请人： BIODURO, LLC , PFIZER, INC.
发明人： Hua Zhou , Paramita Mukherjee , Rongqiang Liu , Christopher W. Am Ende , Tianjing Deng
IPC分类号： C07C303/24 , C07C305/26 , C07C381/00 , C07B45/00 , C07D311/16 , C07D491/10 , C07D213/65 , C07D413/04 , C07C227/10 , C07C307/00 , C07D239/88 , C07D215/32 , C07D211/96 , C07D209/88 , C07D249/18
CPC分类号： C07C381/00 , C07B45/00 , C07C227/10 , C07C303/24 , C07C305/26 , C07C307/00 , C07D209/88 , C07D211/96 , C07D213/65 , C07D215/32 , C07D239/88 , C07D249/18 , C07D311/16 , C07D413/04 , C07D491/10 , C07C303/24 , C07C305/26 , C07C227/10 , C07C229/60
摘要： Disclosed herein are compounds of formula Ar—N(SO2F)2, wherein Ar is selected from an optionally substituted aryl, an optionally substituted five-membered heteroaryl, or an optionally substituted six-membered heteroaryl. Also disclosed are methods of synthesizing the above compounds by reacting a compound of formula Ar—NH—R9 with MN(SO2F)2.

3. 发明授权

US09994497B2 Process for making renewable surfactant intermediates and surfactants from fats and oils and products thereof 有权
公开(公告)号：US09994497B2
公开(公告)日：2018-06-12
申请号：US14629526
申请日：2015-02-24
申请人： The Procter & Gamble Company
发明人： Jeffrey John Scheibel , Scott Leroy Cron , Stephen Anthony DeRose , Ryan Michael West , Phillip Kyle Vinson , Thomas Earl Williams , Kevin Lee Garber , Praveen Kumar Depa
IPC分类号： C10G3/00 , C07C29/16 , C07C303/14 , C10G29/20 , C07C2/64 , C07C5/333 , C11D1/14 , C11D1/22 , C11D1/37 , C07C5/327 , C11D3/34 , C07C303/24 , C10G35/00
CPC分类号： C07C2/64 , C07C5/327 , C07C5/333 , C07C29/16 , C07C303/14 , C07C303/24 , C07C309/62 , C10G3/00 , C10G3/42 , C10G3/50 , C10G29/205 , C10G35/00 , C10G2300/1011 , C10G2300/1014 , C10G2300/1051 , C10G2400/30 , C11D1/146 , C11D1/22 , C11D1/37 , C11D3/34 , C07C11/02 , C07C15/107 , C07C305/04 , C07C33/20
摘要： The present invention relates generally to methods for producing renewable detergent compounds. More specifically, the invention relates to methods for producing detergent intermediates, including bio-linear alkylbenzene (LAB), bio-alcohols, and long chain bio-paraffins, from natural oils.

4. 发明申请

US20180079713A1 THERMAL CONVERSION VESSEL USED IN A PROCESS FOR AMIDIFICATION OF ACETONE CYANOHYDRIN 审中-公开
公开(公告)号：US20180079713A1
公开(公告)日：2018-03-22
申请号：US15820632
申请日：2017-11-22
申请人： Arkema France
发明人： Yves Bernardin , Xavier MARCARIAN , Romain BILLON
IPC分类号： C07C231/12 , C07C305/06 , B01J14/00 , C07C235/06 , C07C233/09 , C07C231/06 , C07C69/54 , C07C67/20 , C07C57/04 , C07C51/08 , C07C303/24 , B01J19/00 , B01J19/02 , B01J19/24
CPC分类号： C07C231/12 , B01J14/00 , B01J19/0013 , B01J19/002 , B01J19/006 , B01J19/02 , B01J19/245 , B01J19/249 , B01J2219/0004 , B01J2219/00058 , B01J2219/00063 , B01J2219/00065 , B01J2219/00162 , B01J2219/00166 , B01J2219/00182 , B01J2219/0027 , B01J2219/00272 , B01J2219/00768 , B01J2219/0286 , B01J2219/029 , B01J2219/182 , B01J2219/1943 , B01J2219/2475 , C07C51/08 , C07C57/04 , C07C67/20 , C07C69/54 , C07C231/06 , C07C233/09 , C07C235/06 , C07C303/24 , C07C305/06
摘要： The invention relates to a thermal conversion vessel (200) used during amidification step of acetone cyanohydrin (ACH), in the industrial process for production of a methyl methacrylate (MMA) or methacrylic acid (MAA). The thermal conversion vessel (200) is used for converting an hydrolysis mixture of α-hydroxyisobutyramide (HIBAM), α-sulfatoisobutyramide (SIBAM), 2-methacrylamide (MACRYDE) and methacrylique acid (MAA), into a mixture of 2-methacrylamide (MACRYDE). It comprises: at least one compartment (C1, C2, C3, . . . Ci) comprising an inner wall (206a, 206b, 206i) separating said compartment into two communicating parts (C1a, C1b) by a passage provided between the bottom of said vessel and said inner wall, said compartment having a space above said inner wall, for separating gas phase from liquid phase during thermal conversion, said compartment being connected to an outlet valve (204a, 204b, . . . 204i). Such vessel allows obtaining a high yield thermal conversion in very safe conditions.

5. 发明授权

US09890116B2 Process for the preparation of a sulfated derivative of 3,5-diiodo-O-[3-iodophenyl]-L-tyrosine 有权
公开(公告)号：US09890116B2
公开(公告)日：2018-02-13
申请号：US14110237
申请日：2012-04-05
申请人： Pier Lucio Anelli , Maria Argese , Luciano Lattuada , Sonia Gazzetto , Laura Galimberti , Valeria Boi , Livio Cavalieri , Fulvia Vella
发明人： Pier Lucio Anelli , Maria Argese , Luciano Lattuada , Sonia Gazzetto , Laura Galimberti , Valeria Boi , Livio Cavalieri , Fulvia Vella
IPC分类号： C07C303/24 , A61K9/20 , A61K31/198 , C07D495/04 , C07C227/16 , C07F1/04
CPC分类号： C07C303/24 , A61K9/2054 , A61K31/198 , C07C227/16 , C07D495/04 , C07F1/04 , C07C305/24 , C07C229/36
摘要： The present invention relates to a process for the preparation of the mono sodium salt of the derivative 3,5-diiodo-O-[3-iodo-4-(sulphooxy)phenyl]-L-tyrosine (T3S) by starting from the corresponding phenolic compound, in the presence of chloro-sulfonic acid and dimethylacetamide as a solvent. The so obtained T3S compound may conveniently be isolated in a pure form as a solid in good yields. The present invention further relates to the process for T3S preparation, wherein the starting reagent is T2 and further comprising the formulation of such compound in tablets. Furthermore, the invention discloses non-radioactive immunoassays based on T3S derivatives.

6. 发明授权

US09260368B2 Process for producing MMA and/or MAA from acetone cyanohydrin and sulfuric acid 有权
标题翻译：由丙酮氰醇和硫酸生产MMA和/或MAA的方法
公开(公告)号：US09260368B2
公开(公告)日：2016-02-16
申请号：US14430648
申请日：2013-09-09
申请人： Rohm and Haas Company
发明人： Andrew M. Lemonds , Minh N. Ngo , Muhunthan Sathiosatham , Donald Lee Zolotorofe
IPC分类号： C07C51/06 , C07C67/20 , C07C303/24 , C07C231/06 , C07C231/12 , C07C67/08
CPC分类号： C07C51/06 , C07C67/08 , C07C67/20 , C07C231/06 , C07C231/12 , C07C303/24 , C07C235/06 , C07C305/06 , C07C233/09 , C07C57/04 , C07C69/54
摘要： A multistage process for the preparation of methacrylic acid and esters thereof via the hydrolysis of ACH, cracking the hydrolysis products, and converting the cracked products to the desired acid or ester, wherein the average temperature in the first hydrolysis reactor is from 55 C to 70 C.
摘要翻译：用于通过ACH的水解制备甲基丙烯酸及其酯的多阶段方法，裂解水解产物，并将裂化产物转化为所需的酸或酯，其中第一水解反应器中的平均温度为55℃至70℃ C。

7. 发明申请

US20150183731A1 Cyclic process for the production of taurine from monoethanolamine 审中-公开
标题翻译：从单乙醇胺生产牛磺酸的循环方法
公开(公告)号：US20150183731A1
公开(公告)日：2015-07-02
申请号：US13998958
申请日：2013-12-30
申请人： Songzhou Hu
发明人： Songzhou Hu
IPC分类号： C07C303/02 , C07C303/28 , C07C303/42 , C07C303/44
CPC分类号： C07C303/02 , C07C303/24 , C07C303/42 , C07C309/14 , C07C305/06
摘要： A method is disclosed for the production of taurine in high yield by a cyclic process of reacting monoethanolamine, sulfuric acid, and ammonium sulfite in the presence of additives to inhibit the hydrolysis of 2-aminoethyl hydrogen sulfate intermediate. The cyclic process is economical and little waste is generated.
摘要翻译：公开了通过在添加剂存在下使单乙醇胺，硫酸和亚硫酸铵反应的环状方法以高产率生产牛磺酸的方法，以抑制2-氨基乙基硫酸氢盐中间体的水解。循环过程是经济的，并且产生很少的浪费。

8. 发明申请

US20150166937A1 LAUNDRY DETERGENT COMPOSITION AND METHOD OF MAKING THEREOF 审中-公开
标题翻译：洗衣粉洗涤剂组合物及其制备方法
公开(公告)号：US20150166937A1
公开(公告)日：2015-06-18
申请号：US14402327
申请日：2013-05-24
申请人： SHELL OIL COMPANY
发明人： Robert Hardy Ellison , Elizabeth Elaine Endler , Carol Jean Klem , Abraham Robert De Kraker , Sharla Nance Papitto , Catherine Semien , Paul Theodore Sharko
IPC分类号： C11D3/34 , C11D11/00 , C11D3/20
CPC分类号： C11D3/3409 , C07C2/26 , C07C303/24 , C11D1/146 , C11D3/2017 , C11D11/0017 , C07C305/04 , C07C11/02
摘要： A mixture of sulfates is made by dimerizing one or more even numbered alpha olefins to produce one or more vinylidenes; hydroformylating the vinylidene(s) to produce a mixture of alcohols; and sulfating the mixture of alcohols to form alcohol sulfates. The sulfates are useful in laundry detergents and other surfactants.
摘要翻译：硫酸盐的混合物是通过使一个或多个偶数α-烯烃二聚而制备一种或多种亚乙烯; 将亚乙烯基加成甲酰化以产生醇的混合物; 并将醇的混合物硫酸化以形成醇硫酸盐。硫酸盐可用于洗衣洗涤剂和其它表面活性剂。

9. 发明授权

US09040745B2 Process for producing fluorosulfuric acid aromatic-ring esters 有权
标题翻译：制备氟代硫酸芳环酯的方法
公开(公告)号：US09040745B2
公开(公告)日：2015-05-26
申请号：US14128362
申请日：2012-06-15
申请人： Akihiro Ishii , Takehisa Ishimaru , Takako Yamazaki , Manabu Yasumoto
发明人： Akihiro Ishii , Takehisa Ishimaru , Takako Yamazaki , Manabu Yasumoto
IPC分类号： C07C303/24
CPC分类号： C07C303/24 , C07C305/26
摘要： A production process of a fluorosulfuric acid aromatic-ring ester according to the present invention includes reaction of an aromatic-ring hydroxyl compound with sulfuryl fluoride (SO2F2) in the presence of a tertiary amine except pyridine and methylpyridine. The sulfuryl fluoride, used as the reactant in the production process according to the present invention, is widely adapted as a fumigant and is easily available on a large scale. Further, the target compound can be obtained rapidly with a high yield under moderate reaction conditions in the production process according to the present invention. In this way, all of the prior art problems can be solved in the production process according to the present invention. The production process according to the present invention is thus particularly useful for industrial production of the fluorosulfuric acid aromatic-ring ester.
摘要翻译：根据本发明的氟代硫酸芳环酯的制备方法包括在除吡啶和甲基吡啶之外的叔胺存在下，芳环羟基化合物与硫酰氟（SO 2 F 2）的反应。在根据本发明的生产方法中用作反应物的硫酰氟被广泛地用作熏蒸剂，并且容易获得大量。此外，在本发明的制造方法中，在中等反应条件下，可以快速获得目标化合物。以这种方式，可以在根据本发明的制造方法中解决所有现有技术问题。因此，本发明的制造方法特别适用于氟代硫酸芳香环酯的工业化生产。

10. 发明授权

US08278476B2 Process for producing α-substituted ester 有权
标题翻译： α-取代酯的制备方法
公开(公告)号：US08278476B2
公开(公告)日：2012-10-02
申请号：US13127955
申请日：2009-10-22
申请人： Akihiro Ishii , Manabu Yasumoto
发明人： Akihiro Ishii , Manabu Yasumoto
IPC分类号： C07C69/612
CPC分类号： C07B53/00 , C07B55/00 , C07B2200/07 , C07C67/343 , C07C303/24 , C07C69/612 , C07C305/26
摘要： There is provided a process for producing an α-substituted ester by reaction of a fluorosulfuric acid ester of α-hydroxyester with a Grignard reagent in the presence of a zinc catalyst. It is newly found that the reaction for production of α-substituted esters, in which the raw reaction substrate is limited to expensive trifluoromethanesulfonic acid esters, can proceed favorably with the use of fluorosulfuric acid esters suitable for mass-production uses. By the use of the fluorosulfuric acid ester high in optical purity, it is possible to obtain the α-substituted ester with high optical purity upon inversion of the asymmetric carbon configuration. The process of the present invention can solve all of the prior art problems and can be applied for industrial uses.
摘要翻译：提供了在锌催化剂存在下，通过α-羟基酯的氟代硫酸酯与格氏试剂的反应制备α-取代的酯的方法。新发现，通过使用适合于批量生产用途的氟代硫酸酯，可以有利地进行生产反应底物被限制为昂贵的三氟甲磺酸酯的α-取代酯的反应。通过使用光学纯度高的氟代硫酸酯，可以通过不对称碳结构的反转获得具有高光学纯度的α-取代的酯。本发明的方法可以解决所有现有技术的问题，并且可以应用于工业用途。

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