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    • 5. 发明授权
    • Post chemical mechanical polishing cleaning solution for 2.45T CoFeNi structures of thin film magnetic heads
    • 用于2.45T薄膜磁头的CoFeNi结构的化学机械抛光清洗溶液
    • US06984613B1
    • 2006-01-10
    • US10931385
    • 2004-08-31
    • Hung-Chin GuthrieMing JiangNick Lara
    • Hung-Chin GuthrieMing JiangNick Lara
    • C11D17/00
    • C11D3/0073C11D9/007C11D9/30C11D11/0047
    • The present invention is directed to methods for polishing and cleaning a wafer having CoFeNi structures within alumina fill to achieve corrosion-free, smooth, and planar surface. A preferred chemical mechanical polishing (CMP) method includes a CMP polishing compound including alumina abrasive particulates, 1H-Benzotriazole (BTA), and hydrogen peroxide (H2O2). A cleaning solution for CoFeNi structures in alumina fill of the present invention preferably includes 4-Methyl-1H-Benzotriazole in a concentration range of from 1% to 5%, 5-Methyl-1H-Benzotriazole in a concentration range of from 1% to 5%, hydrogenated 4-Methyl-1H-Benzotriazole in a concentration range of from 1% to 5%, hydrogenated 5-Methyl-1H-Benzotriazole in a concentration range of from 1% to 5%, sodium octanoate in a concentration range of from 5% to 10%, and water in a concentration range of from 65% to 95%. The cleaning solution is typically used with DI water to create an applied solution having a range of from 0.1% to 10% by volume of the cleaning solution.
    • 本发明涉及在氧化铝填充物内抛光和清洗具有CoFeNi结构的晶片以实现无腐蚀,平滑和平坦的表面的方法。 优选的化学机械抛光(CMP)方法包括CMP抛光化合物,其包括氧化铝磨粒,1H-苯并三唑(BTA)和过氧化氢(H 2 O 2 O 2)。 本发明的氧化铝填充物中的CoFeNi结构的清洗液优选含有浓度范围为1%〜5%的4-甲基-1H-苯并三唑,浓度范围为1%〜5%的5-甲基-1H-苯并三唑 5%的浓度范围为1%至5%的氢化的4-甲基-1H-苯并三唑,浓度范围为1%至5%的氢化的5-甲基-1H-苯并三唑,浓度范围为 5%至10%,浓度范围为65%至95%的水。 清洁溶液通常与去离子水一起使用以产生具有0.1至10体积%范围的清洁溶液的施用溶液。
    • 6. 发明申请
    • Chemical mechanical polishing process for 2.45T CoFeNi structures of thin film magnetic heads
    • 2.45T CoFeNi薄膜磁头结构的化学机械抛光工艺
    • US20060042173A1
    • 2006-03-02
    • US10931846
    • 2004-08-31
    • Hung-Chin GuthrieMing JiangNick Lara
    • Hung-Chin GuthrieMing JiangNick Lara
    • B24D3/02B24B7/30C09C1/68
    • C09K3/1463C09G1/02
    • The present invention is directed to methods for polishing and cleaning a wafer having CoFeNi structures within alumina fill to achieve corrosion-free, smooth, and planar surface. A preferred chemical mechanical polishing (CMP) method includes a CMP polishing compound including alumina abrasive particulates, 1H-Benzotriazole (BTA), and hydrogen peroxide (H2O2) in a concentration working range of 4% to 12%. In a preferred embodiment the H2O2 concentration is approximately 6% and the pH is approximately 4.0 at polishing pressure 6 psi. A cleaning solution for CoFeNi structures in alumina fill of the present invention preferably includes 4-Methyl-1H-Benzotriazole, 5-Methyl-1H-Benzotriazole, hydrogenated 4-Methyl-1H-Benzotriazole, hydrogenated 5-Methyl-1H-Benzotriazole, sodium octanoate, and water.
    • 本发明涉及在氧化铝填充物内抛光和清洗具有CoFeNi结构的晶片以实现无腐蚀,平滑和平坦的表面的方法。 优选的化学机械抛光(CMP)方法包括CMP抛光化合物,其包括氧化铝磨料颗粒,1H-苯并三唑(BTA)和过氧化氢(H 2 O 2 O 2) 浓度范围为4%〜12%。 在优选的实施方案中,在抛光压力6psi下,H 2 O 2 O 2浓度为约6%,pH为约4.0。 本发明的氧化铝填充物中的CoFeNi结构的清洗液优选包括4-甲基-1H-苯并三唑,5-甲基-1H-苯并三唑,氢化的4-甲基-1H-苯并三唑,氢化的5-甲基-1H-苯并三唑,钠 辛酸盐和水。
    • 7. 发明授权
    • Chemical mechanical polishing process for 2.45T CoFeNi structures of thin film magnetic heads
    • 2.45T CoFeNi薄膜磁头结构的化学机械抛光工艺
    • US07306638B2
    • 2007-12-11
    • US10931846
    • 2004-08-31
    • Hung-Chin GuthrieMing JiangNick Lara
    • Hung-Chin GuthrieMing JiangNick Lara
    • C09G1/02C09G1/04
    • C09K3/1463C09G1/02
    • The present invention is directed to methods for polishing and cleaning a wafer having CoFeNi structures within alumina fill to achieve corrosion-free, smooth, and planar surface. A preferred chemical mechanical polishing (CMP) method includes a CMP polishing compound including alumina abrasive particulates, 1H-Benzotriazole (BTA), and hydrogen peroxide (H2O2) in a concentration working range of 4% to 12%. In a preferred embodiment the H2O2 concentration is approximately 6% and the pH is approximately 4.0 at polishing pressure 6 psi. A cleaning solution for CoFeNi structures in alumina fill of the present invention preferably includes 4-Methyl-1H-Benzotriazole, 5-Methyl-1H-Benzotriazole, hydrogenated 4-Methyl-1H-Benzotriazole, hydrogenated 5-Methyl-1H-Benzotriazole, sodium octanoate, and water.
    • 本发明涉及在氧化铝填充物内抛光和清洗具有CoFeNi结构的晶片以实现无腐蚀,平滑和平坦的表面的方法。 优选的化学机械抛光(CMP)方法包括CMP抛光化合物,其包括氧化铝磨料颗粒,1H-苯并三唑(BTA)和过氧化氢(H 2 O 2 O 2) 浓度范围为4%〜12%。 在优选的实施方案中,在抛光压力6psi下,H 2 O 2 O 2浓度为约6%,pH为约4.0。 本发明的氧化铝填充物中的CoFeNi结构的清洗液优选包括4-甲基-1H-苯并三唑,5-甲基-1H-苯并三唑,氢化的4-甲基-1H-苯并三唑,氢化的5-甲基-1H-苯并三唑,钠 辛酸盐和水。
    • 10. 发明授权
    • Run-to-run control of backside pressure for CMP radial uniformity optimization based on center-to-edge model
    • 基于中心到边缘模型的用于CMP径向均匀性优化的背侧压力的运行控制控制
    • US07722436B2
    • 2010-05-25
    • US11832455
    • 2007-08-01
    • Hung-Chin GuthrieMing JiangYeak-Chong Wong
    • Hung-Chin GuthrieMing JiangYeak-Chong Wong
    • B24B49/00
    • B24B49/03B24B37/042
    • During planarization of wafers, the thickness of a layer of a wafer is measured at a number of locations, after the wafer has been planarized by chemical mechanical polishing. The thickness measurements are used to automatically determine, from a center to edge profile model to which the measurements are fit, a parameter that controls chemical mechanical polishing, called “backside pressure.” Backside pressure is determined in some embodiments by a logic test based on the center-to-edge profile model, coefficient of determination R-square of the model, and current value of backside pressure. Note that a “backside pressure” set point is adjusted only if the fit of the measurements to the model is good, e.g. as indicated by R-square being greater than a predetermined limit. Next, the backside pressure that has been determined from the model is used in planarizing a subsequent wafer.
    • 在晶片的平坦化期间,在通过化学机械抛光对晶片进行平面化之后,在多个位置测量晶片层的厚度。 厚度测量用于自动确定从测量结合到的中心到边缘轮廓模型,控制称为“后侧压力”的化学机械抛光的参数。背面压力在一些实施例中通过基于 中心到边缘轮廓模型,模型的确定系数R平方和背侧压力的当前值。 注意,仅当对模型的测量的拟合良好时才调整“背侧压力”设定点。 如R平方所示大于预定极限。 接下来,将从模型确定的背面压力用于平面化后续晶片。