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1. 发明授权

US5179156A Rubber composition 失效
标题翻译：橡胶组成
公开(公告)号：US5179156A
公开(公告)日：1993-01-12
申请号：US859803
申请日：1992-03-30
申请人： Hiroyoshi Takao , Hiroyuki Harada , Kiyoyuki Sugimori , Nobuyuki Yoshida , Masahiro Fukuyama , Hideaki Yamada , Junichi Koshiba
发明人： Hiroyoshi Takao , Hiroyuki Harada , Kiyoyuki Sugimori , Nobuyuki Yoshida , Masahiro Fukuyama , Hideaki Yamada , Junichi Koshiba
IPC分类号： C08F210/18 , C08L23/16
CPC分类号： C08F210/18
摘要： Herein is disclosed a vulcanizable rubber composition comprising a copolymer rubber constituted of ethylene, propylene and nonconjugated polyene, wherein ethylene/propylene molar ratio is 78/22 to 97/3 and the total content of propylene and nonconjugated polyene is 6 to 30% by mole in said copolymer rubber. By the use of the rubber composition of the present invention, a vulcanized product excellent in tensile strength, heat resistance, oil resistance, compression set resistance and flex behavior can be obtained. The vulcanized product can be used as automobile parts and other innumerable articles such as socket cover, heat resistant hose, electric wire, condenser cap, heat resistant belt, vibration-proof rubber, hoses, weather strip, seal sponge, black side wall of tire, etc.
摘要翻译：本文公开了一种可硫化橡胶组合物，其包含由乙烯，丙烯和非共轭多烯构成的共聚物橡胶，其中乙烯/丙烯摩尔比为78/22至97/3，丙烯和非共轭多烯的总含量为6〜30摩尔％在所述共聚物橡胶中。通过使用本发明的橡胶组合物，可以获得抗拉强度，耐热性，耐油性，耐压缩变形性和挠曲性能优异的硫化产品。硫化产品可用作汽车零件和其他无数件产品，如插座盖，耐热软管，电线，冷凝盖，耐热带，防振橡胶，软管，耐候条，密封海绵，轮胎黑色侧壁等等

2. 发明授权

US5118773A Rubber composition 失效
公开(公告)号：US5118773A
公开(公告)日：1992-06-02
申请号：US784079
申请日：1991-10-30
申请人： Hiroyoshi Takao , Hiroyuki Harada , Kiyoyuki Sugimori , Nobuyuki Yoshida , Masahiro Fukuyama , Hideaki Yamada , Junichi Koshiba
发明人： Hiroyoshi Takao , Hiroyuki Harada , Kiyoyuki Sugimori , Nobuyuki Yoshida , Masahiro Fukuyama , Hideaki Yamada , Junichi Koshiba
IPC分类号： C08F4/68 , C08F210/18 , C08L23/16
CPC分类号： C08L23/16 , C08F210/18 , C08L2203/202 , C08L2312/00
摘要： Herein is disclosed a vulcanizable rubber composition comprising a copolymer rubber constituted of ethylene, propylene and nonconjugated polyene, wherein ethylene/propylene molar ratio is 78/22 to 97/3 and the total content of propylene and nonconjugated polyene is 6 to 30% by mole in said copolymer rubber. By the use of the rubber composition of the present invention, a vulcanized product excellent in tensile strength, heat resistance, oil resistance, compression set resistance and flex behavior can be obtained. The vulcanized product can be used as automobile parts and other innumerable articles such as socket cover, heat resistant hose, electric wire, condenser cap, heat resistant belt, vibration-proof rubber, hoses weather strip, seal sponge, black side wall of tire, etc.

3. 发明授权

US5245007A Method for purifying ethylene-.alpha.-olefin copolymer 失效
标题翻译：纯化乙烯 - （ALPHA） - 烯烃共聚物的方法
公开(公告)号：US5245007A
公开(公告)日：1993-09-14
申请号：US805651
申请日：1991-12-12
申请人： Keisaku Yamamoto , Kizuku Wakatsuki , Kiyoyuki Sugimori , Hayato Saba , Katsunari Inagaki
发明人： Keisaku Yamamoto , Kizuku Wakatsuki , Kiyoyuki Sugimori , Hayato Saba , Katsunari Inagaki
IPC分类号： C08F6/02
CPC分类号： C08F6/02
摘要： A method for purifying an ethylene-.alpha.-olefin olefin having at least 3 carbon atoms, or ethylene with an .alpha.-olefin having at least 3 carbon atoms and a nonconjugated diene compound, in a hydrocarbon solvent in the presence of a catalyst comprising a vanadium compound, an organoaluminum compound, and a halogenated ester compound, the method including a step of mixing and stirring the polymerization reaction mixture obtained by the polymerization reaction in an aqueous alkaline solution in such an amount as to give an aqueous phase having a pH of not lower than 10.0 after mixing and stirring, is disclosed. A method for purifying an ethylene-.alpha.-olefin copolymer is also disclosed, including a step of an oxidation treatment of the polymerization reaction mixture in an aqueous alkaline solution in such an amount as to give an aqueous phase having a pH of not lower than 10.0 after the oxidation treatment.

4. 发明授权

US5191041A Catalyst for olefinic hydrocarbon polymerization and process and producing olefinic hydrocarbon polymer 失效
标题翻译：用于烯烃聚合的催化剂和制备和生产烯烃聚合物
公开(公告)号：US5191041A
公开(公告)日：1993-03-02
申请号：US821037
申请日：1992-01-16
申请人： Hayato Saba , Keisaku Yamamoto , Akio Imai , Kiyoyuki Sugimori , Kizuku Wakatsuki
发明人： Hayato Saba , Keisaku Yamamoto , Akio Imai , Kiyoyuki Sugimori , Kizuku Wakatsuki
IPC分类号： C08F10/00
CPC分类号： C08F10/00
摘要： An inert hydrocarbon solvent-soluble catalyst for polymerization of olefinic hydrocarbons and a process for producing an olefinic polymer using the same are disclosed, the catalyst being composed of (A) a reaction product obtained by reacting (a) at least one vanadium compound represented by formula:VO(OR).sub.m X.sub.3-mwherein R represents a hydrocarbon group; X represents a halogen atom; and m represents a real number of from 0 to 3, and (b) a dihydroxy hydrocarbon compound constituted of a straight chain hydrocarbon skeleton containing from 2 to 12 carbon atoms and having a hydroxyl group at each of both terminals thereof and at least one hydrocarbon branch bonded to said hydrocarbon skeleton in an inert hydrocarbon solvent at an (a) to (b) molar ratio of from 1:0.5 to 1:1.4 and (B) at least one organoaluminum compound represented by formula:R'.sub.n AlX'.sub.3-nwherein R' represents a hydrocarbon group; X' represents a halogen atom; and n represents a real number more than 0 and less than 3. Olefinic hydrocarbon polymers having narrow distributions of molecular weight and composition can be produced with high efficiency and high polymerization activity without being accompanied by obstruction or contamination of equipment due to precipitation of a catalyst.
摘要翻译：公开了一种用于烯烃聚合的惰性烃溶剂可溶性催化剂和使用其的制备烯烃聚合物的方法，该催化剂由（A）通过使（a）至少一种钒化合物式：VO（OR）mX3-m其中R表示烃基; X表示卤原子; m表示0〜3的实数，（b）由含有2〜12个碳原子的直链烃骨架构成的二羟基烃化合物，其两末端具有羟基，至少一个烃在（a）至（b）摩尔比为1:0.5至1:1.4的惰性烃溶剂中与所述烃骨架键合的至少一种有机铝化合物，和（B）至少一种由式：R'nAlX'3- n其中R'表示烃基; X'表示卤原子; 并且n表示大于0且小于3的实数。可以以高效率和高聚合活性生产具有窄分子量和组成分布的烯属烃聚合物，而不伴随催化剂沉淀引起的设备阻塞或污染。

5. 发明授权

US5122493A Catalyst for olefinic hydrocarbon polymerization and process for producing olefinic hydrocarbon polymer 失效
标题翻译：烯烃聚合催化剂和生产烯烃聚合物的方法
公开(公告)号：US5122493A
公开(公告)日：1992-06-16
申请号：US675823
申请日：1991-03-27
申请人： Hayato Saba , Keisaku Yamamoto , Akio Imai , Kiyoyuki Sugimori , Kizuku Wakatsuki
发明人： Hayato Saba , Keisaku Yamamoto , Akio Imai , Kiyoyuki Sugimori , Kizuku Wakatsuki
IPC分类号： C08F4/60 , C08F4/68 , C08F10/00
CPC分类号： C08F10/00
摘要： An inert hydrocarbon solvent-soluble catalyst for polymerization of olefinic hydrocarbons and a process for producing an olefinic polymer using the same are disclosed, the catalyst being composed of (A) a reaction product obtained by reacting (a) at least one vanadium compound represented by formula:VO(OR).sub.m X.sub.3-mwherein R represents a hydrocarbon group; X represents a halogen atom; and m represents a real number of from 0 to 3, and (b) a dihydroxy hydrocarbon compound constituted of a straight chain hydrocarbon skeleton containing from 2 to 12 carbon atoms and having a hydroxyl group at each of both terminals thereof and at least one hydrocarbon branch bonded to said hydrocarbon skeleton in an inert hydrocarbon solvent at an (a) to (b) molar ratio of from 1:0.5 to 1:1.4 and (B) at least one organoaluminum compound represented by formula:R'.sub.n AlX'.sub.3-nwherein R' represents a hydrocarbon group X' represents a halogen atom; and n represents a real number more than 0 and less than 3. Olefinic hydrocarbon polymers having narrow distributions of molecular weight and composition can be produced with high efficiency and high polymerization activity without being accompanied by obstruction or contamination of equipment due to precipitation of a catalyst.

6. 发明授权

US5082908A Ethylene-.alpha.-olefin copolymer and process for producing the same 失效
标题翻译：乙烯 - （ALPHA） - 烯烃共聚物及其制造方法
公开(公告)号：US5082908A
公开(公告)日：1992-01-21
申请号：US363654
申请日：1989-06-08
申请人： Akio Imai , Kiyoyuki Sugimori , Keisaku Yamamoto , Minoru Takane
发明人： Akio Imai , Kiyoyuki Sugimori , Keisaku Yamamoto , Minoru Takane
IPC分类号： C08F4/68 , C08F210/00
CPC分类号： C08F210/00
摘要： An ethylene-.alpha.-olefin copolymer is disclosed, which comprises ethylene and an .alpha.-olefin having from 3 to 10 carbon atoms, has an ethylene/.alpha.-olefin molar ratio of from 88/12 to 98/2, and which has a number average molecular weight of from 35,000 to 80,000 and a weight average molecular weight/number average molecular weight ratio of from 1.8/1 to 3.0/1 as determined by gel permeation chromatography. A process for producing the ethylene-.alpha.-olefin copolymer is also disclosed. The ethylene-.alpha.-olefin copolymer exhibits excellent transparency and excellent low-temperature heat-sealing properties. The process is advantageous from the standpoint of equipment, energy and cost.

7. 发明授权

US4981760A Ethylene-alpha-olefin copolymer and films obtained therefrom 失效
标题翻译：乙烯-α-烯烃共聚物和由其获得的膜
公开(公告)号：US4981760A
公开(公告)日：1991-01-01
申请号：US378000
申请日：1989-07-11
申请人： Yukio Naito , Kohzoh Miyazaki , Yuji Gotoh , Masashi Hamba , Akio Imai , Kiyoyuki Sugimori
发明人： Yukio Naito , Kohzoh Miyazaki , Yuji Gotoh , Masashi Hamba , Akio Imai , Kiyoyuki Sugimori
IPC分类号： B32B27/32 , C08F10/00 , C08F110/02 , C08F210/02 , C08F210/16 , C08F297/08 , C08J5/18 , C08L23/00 , C08L23/06 , C08L23/08
CPC分类号： C08J5/18 , C08F210/02 , C08F210/16 , C08F297/08 , C08L23/0815 , C08F110/02 , C08J2323/08 , C08L23/06 , Y10T428/31855 , Y10T428/31938
摘要： An ethylene-.alpha.-olefin copolymer comprising ethylene and an .alpha.-olefin having from 3 to 10 carbon atoms, the copolymer having an .alpha.-olefin content of from 1.0 to 8.0 mol %, a density of from 0.900 to 0.930 g/cm.sup.3, and a melt flow rate of from 0.1 to 100 g/10 min., the programed-temperature thermogram of said copolymer as determined with a differential scanning calorimeter after being completely melted and then gradually cooled showing an endothermic peak (a) in a range of from 75.degree. to 100.degree. C. and an endothermic peak (b) in a range of from 120.degree. to 140.degree. C., with the ratio of an endotherm at the endothermic peak (b), .DELTA.Hb, to an endotherm at the endothermic peak (a), .DELTA.Ha, i.e., .DELTA.Hb/.DELTA.Ha, being from 0.03 to 2.0. The copolymer provides a film exhibiting excellent physical properties required for packaging film.

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