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1. 发明授权

US4981760A Ethylene-alpha-olefin copolymer and films obtained therefrom 失效
标题翻译：乙烯-α-烯烃共聚物和由其获得的膜
公开(公告)号：US4981760A
公开(公告)日：1991-01-01
申请号：US378000
申请日：1989-07-11
申请人： Yukio Naito , Kohzoh Miyazaki , Yuji Gotoh , Masashi Hamba , Akio Imai , Kiyoyuki Sugimori
发明人： Yukio Naito , Kohzoh Miyazaki , Yuji Gotoh , Masashi Hamba , Akio Imai , Kiyoyuki Sugimori
IPC分类号： B32B27/32 , C08F10/00 , C08F110/02 , C08F210/02 , C08F210/16 , C08F297/08 , C08J5/18 , C08L23/00 , C08L23/06 , C08L23/08
CPC分类号： C08J5/18 , C08F210/02 , C08F210/16 , C08F297/08 , C08L23/0815 , C08F110/02 , C08J2323/08 , C08L23/06 , Y10T428/31855 , Y10T428/31938
摘要： An ethylene-.alpha.-olefin copolymer comprising ethylene and an .alpha.-olefin having from 3 to 10 carbon atoms, the copolymer having an .alpha.-olefin content of from 1.0 to 8.0 mol %, a density of from 0.900 to 0.930 g/cm.sup.3, and a melt flow rate of from 0.1 to 100 g/10 min., the programed-temperature thermogram of said copolymer as determined with a differential scanning calorimeter after being completely melted and then gradually cooled showing an endothermic peak (a) in a range of from 75.degree. to 100.degree. C. and an endothermic peak (b) in a range of from 120.degree. to 140.degree. C., with the ratio of an endotherm at the endothermic peak (b), .DELTA.Hb, to an endotherm at the endothermic peak (a), .DELTA.Ha, i.e., .DELTA.Hb/.DELTA.Ha, being from 0.03 to 2.0. The copolymer provides a film exhibiting excellent physical properties required for packaging film.

2. 发明授权

US5122493A Catalyst for olefinic hydrocarbon polymerization and process for producing olefinic hydrocarbon polymer 失效
标题翻译：烯烃聚合催化剂和生产烯烃聚合物的方法
公开(公告)号：US5122493A
公开(公告)日：1992-06-16
申请号：US675823
申请日：1991-03-27
申请人： Hayato Saba , Keisaku Yamamoto , Akio Imai , Kiyoyuki Sugimori , Kizuku Wakatsuki
发明人： Hayato Saba , Keisaku Yamamoto , Akio Imai , Kiyoyuki Sugimori , Kizuku Wakatsuki
IPC分类号： C08F4/60 , C08F4/68 , C08F10/00
CPC分类号： C08F10/00
摘要： An inert hydrocarbon solvent-soluble catalyst for polymerization of olefinic hydrocarbons and a process for producing an olefinic polymer using the same are disclosed, the catalyst being composed of (A) a reaction product obtained by reacting (a) at least one vanadium compound represented by formula:VO(OR).sub.m X.sub.3-mwherein R represents a hydrocarbon group; X represents a halogen atom; and m represents a real number of from 0 to 3, and (b) a dihydroxy hydrocarbon compound constituted of a straight chain hydrocarbon skeleton containing from 2 to 12 carbon atoms and having a hydroxyl group at each of both terminals thereof and at least one hydrocarbon branch bonded to said hydrocarbon skeleton in an inert hydrocarbon solvent at an (a) to (b) molar ratio of from 1:0.5 to 1:1.4 and (B) at least one organoaluminum compound represented by formula:R'.sub.n AlX'.sub.3-nwherein R' represents a hydrocarbon group X' represents a halogen atom; and n represents a real number more than 0 and less than 3. Olefinic hydrocarbon polymers having narrow distributions of molecular weight and composition can be produced with high efficiency and high polymerization activity without being accompanied by obstruction or contamination of equipment due to precipitation of a catalyst.

3. 发明授权

US5082908A Ethylene-.alpha.-olefin copolymer and process for producing the same 失效
标题翻译：乙烯 - （ALPHA） - 烯烃共聚物及其制造方法
公开(公告)号：US5082908A
公开(公告)日：1992-01-21
申请号：US363654
申请日：1989-06-08
申请人： Akio Imai , Kiyoyuki Sugimori , Keisaku Yamamoto , Minoru Takane
发明人： Akio Imai , Kiyoyuki Sugimori , Keisaku Yamamoto , Minoru Takane
IPC分类号： C08F4/68 , C08F210/00
CPC分类号： C08F210/00
摘要： An ethylene-.alpha.-olefin copolymer is disclosed, which comprises ethylene and an .alpha.-olefin having from 3 to 10 carbon atoms, has an ethylene/.alpha.-olefin molar ratio of from 88/12 to 98/2, and which has a number average molecular weight of from 35,000 to 80,000 and a weight average molecular weight/number average molecular weight ratio of from 1.8/1 to 3.0/1 as determined by gel permeation chromatography. A process for producing the ethylene-.alpha.-olefin copolymer is also disclosed. The ethylene-.alpha.-olefin copolymer exhibits excellent transparency and excellent low-temperature heat-sealing properties. The process is advantageous from the standpoint of equipment, energy and cost.

4. 发明授权

US5191041A Catalyst for olefinic hydrocarbon polymerization and process and producing olefinic hydrocarbon polymer 失效
标题翻译：用于烯烃聚合的催化剂和制备和生产烯烃聚合物
公开(公告)号：US5191041A
公开(公告)日：1993-03-02
申请号：US821037
申请日：1992-01-16
申请人： Hayato Saba , Keisaku Yamamoto , Akio Imai , Kiyoyuki Sugimori , Kizuku Wakatsuki
发明人： Hayato Saba , Keisaku Yamamoto , Akio Imai , Kiyoyuki Sugimori , Kizuku Wakatsuki
IPC分类号： C08F10/00
CPC分类号： C08F10/00
摘要： An inert hydrocarbon solvent-soluble catalyst for polymerization of olefinic hydrocarbons and a process for producing an olefinic polymer using the same are disclosed, the catalyst being composed of (A) a reaction product obtained by reacting (a) at least one vanadium compound represented by formula:VO(OR).sub.m X.sub.3-mwherein R represents a hydrocarbon group; X represents a halogen atom; and m represents a real number of from 0 to 3, and (b) a dihydroxy hydrocarbon compound constituted of a straight chain hydrocarbon skeleton containing from 2 to 12 carbon atoms and having a hydroxyl group at each of both terminals thereof and at least one hydrocarbon branch bonded to said hydrocarbon skeleton in an inert hydrocarbon solvent at an (a) to (b) molar ratio of from 1:0.5 to 1:1.4 and (B) at least one organoaluminum compound represented by formula:R'.sub.n AlX'.sub.3-nwherein R' represents a hydrocarbon group; X' represents a halogen atom; and n represents a real number more than 0 and less than 3. Olefinic hydrocarbon polymers having narrow distributions of molecular weight and composition can be produced with high efficiency and high polymerization activity without being accompanied by obstruction or contamination of equipment due to precipitation of a catalyst.
摘要翻译：公开了一种用于烯烃聚合的惰性烃溶剂可溶性催化剂和使用其的制备烯烃聚合物的方法，该催化剂由（A）通过使（a）至少一种钒化合物式：VO（OR）mX3-m其中R表示烃基; X表示卤原子; m表示0〜3的实数，（b）由含有2〜12个碳原子的直链烃骨架构成的二羟基烃化合物，其两末端具有羟基，至少一个烃在（a）至（b）摩尔比为1:0.5至1:1.4的惰性烃溶剂中与所述烃骨架键合的至少一种有机铝化合物，和（B）至少一种由式：R'nAlX'3- n其中R'表示烃基; X'表示卤原子; 并且n表示大于0且小于3的实数。可以以高效率和高聚合活性生产具有窄分子量和组成分布的烯属烃聚合物，而不伴随催化剂沉淀引起的设备阻塞或污染。

5. 发明授权

US07795438B2 Processes for producing 1-benzyl-4-[(5,6-dimethoxy-1indanon)-2-yl]methylpiperidine and hydrochloride 有权
标题翻译： 1-苄基-4 - [（5,6-二甲氧基-1茚满酮）-2-基]甲基哌啶和盐酸盐的制备方法
公开(公告)号：US07795438B2
公开(公告)日：2010-09-14
申请号：US10580908
申请日：2005-04-27
申请人： Akio Imai , Hiroshi Nishimura
发明人： Akio Imai , Hiroshi Nishimura
IPC分类号： C07D211/32
CPC分类号： C07D211/32 , B01J25/02
摘要： Processes for preparing 1-benzyl-4-[(5,6-dimethoxy-lindanon)-2-yl]methylpiperidine (donepezil), which is useful as an intermediate for medicines, and for producing 1-benzyl-4-[(5,6-dimethoxy-1-indanon)-2-yl]methylpiperidine hydrochloride (donepezil hydrochloride), which is useful as a medicine. The process for donepezil hydrochloride production comprises catalytically hydrogenating the compound represented by the structural formula (III) [1-benzyl-4-[(5,6-dimethoxy-lindanon)-2-ylidene]methylpiperidine] with a Raney nickel catalyst under mild conditions and subsequently treating it with hydrochloric acid. Thus, impurities are further diminished. The operations are simple and the process is suitable for industrial production.
摘要翻译：用于制备1-苄基-4 - [（5,6-二甲氧基 - 茚满酮）-2-基]甲基哌啶（多奈哌齐）的方法，其可用作药物的中间体，并用于制备1-苄基-4 - [（5 ，6-二甲氧基-1-茚满酮）-2-基]甲基哌啶盐酸盐（盐酸多奈哌齐），其可用作药物。盐酸多奈哌齐的方法包括用温和的阮内镍催化剂催化氢化由结构式（III）[1-苄基-4 - [（5,6-二甲氧基 - 茚满酮）-2-亚基]甲基哌啶]代表的化合物然后用盐酸处理。因此，杂质进一步减少。操作简单，适用于工业生产。

6. 发明申请

US20090171094A1 1-BENZYL-4-[(5, 6-DIMETHOXY- 1- INDANON)- 2- YL]-METHYL PIPERIDINE P-TOLUENESULFONATE OR CRYSTAL THEREOF 审中-公开
标题翻译： 1-苄基-4 - [（5,6-二甲氧基-1-茚满酮）-2-基] - 甲基哌啶对甲苯磺酸酯或其结晶
公开(公告)号：US20090171094A1
公开(公告)日：2009-07-02
申请号：US11994494
申请日：2006-07-12
申请人： Kazuhide Ashizawa , Akio Imai
发明人： Kazuhide Ashizawa , Akio Imai
IPC分类号： C07D211/32
CPC分类号： C07D211/32
摘要： 1-Benzyl-4-[(5,6-dimethoxy-1-indanon)-2-yl]methylpiperidine p-toluenesulfonate or a solvate thereof.
摘要翻译： 1-苄基-4 - [（5,6-二甲氧基-1-茚满酮）-2-基]甲基哌啶对甲苯磺酸盐或其溶剂合物。

7. 发明申请

US20080306272A1 ONE-POT METHODS FOR PREPARING CINNAMIDE DERIVATIVES 审中-公开
标题翻译：用于制备氰化物衍生物的一种方法
公开(公告)号：US20080306272A1
公开(公告)日：2008-12-11
申请号：US12121454
申请日：2008-05-15
申请人： Naoyuki Shimomura , Seiji Yoshikawa , Yoshihiko Hisatake , Akio Imai
发明人： Naoyuki Shimomura , Seiji Yoshikawa , Yoshihiko Hisatake , Akio Imai
IPC分类号： C07D401/02
CPC分类号： C07D401/10 , Y02P20/55
摘要： A compound represented by the following formula (1): wherein R represents a 4-fluorophenyl group and the like; Q represents —CH(CH3)— and the like; and n represents 1 and the like and a pharmaceutically acceptable salt thereof can be prepared in one-pot by reacting a compound represented by the following formula (2): wherein R1 represents a 4-fluorophenyl group and the like; and Q and n have the same meaning as described above, with 3-methoxy-4-(4-methyl-1H-imidazol-1-yl)benzaldehyde in the presence of a base and, if necessary, removing a protecting group.
摘要翻译：由下式（1）表示的化合物：其中R表示4-氟苯基等; Q表示-CH（CH 3） - 等; 和n表示1等的化合物及其药学上可接受的盐可以通过使由下式（2）表示的化合物反应而制备：其中R1表示4-氟苯基等; 和Q和n具有与上述相同的含义，与3-甲氧基-4-（4-甲基-1H-咪唑-1-基）苯甲醛在碱存在下反应，如果需要，除去保护基。

8. 发明申请

US20070088055A1 Process for producing 1-benzyl-4-[ (5,6-dimethoxy-1-indanon)-2-yl]methylpiperidine or hydrochloride thereof 失效
标题翻译： 1-苄基-4 - [（5,6-二甲氧基-1-茚满酮）-2-基]甲基哌啶或其盐酸盐的制备方法
公开(公告)号：US20070088055A1
公开(公告)日：2007-04-19
申请号：US11546444
申请日：2006-10-12
申请人： Akio Imai
发明人： Akio Imai
IPC分类号： C07D211/06 , A61K31/445
CPC分类号： C07D211/32
摘要： 1-Benzyl-4-[(5,6-dimethoxy-1-indanon)-2-yl]methylpiperidine or hydrochloride thereof, which is useful as a drug, can be produced in high purity by safer and easier operations suitable for industrial production by subjecting 1-benzyl-4-[(5,6-dimethoxy-1-indanon)-2-ylidene]methyl-piperidine or a solvate thereof to catalytic hydrogenation in the presence of a palladium-alumina catalyst and if necessary, converting the thus obtained compound to its hydrochloride.
摘要翻译：可用作药物的1-苄基-4 - [（5,6-二甲氧基-1-茚满酮）-2-基]甲基哌啶或其盐酸盐可以通过适合于工业生产的更安全和更容易的操作而以高纯度制备通过在钯 - 氧化铝催化剂的存在下使1-苄基-4 - [（5,6-二甲氧基-1-茚满酮）-2-亚基]甲基 - 哌啶或其溶剂合物进行催化氢化，如果需要，从而得到化合物至其盐酸盐。

9. 发明授权

US06187883B1 Solid catalyst component for &agr;-olefin polymerization, catalyst for &agr;-olefin polymerization, and process for producing &agr;-olefin polymer 失效
标题翻译：用于α-烯烃聚合的固体催化剂组分，用于α-烯烃聚合的催化剂和用于生产α-烯烃聚合物的方法
公开(公告)号：US06187883B1
公开(公告)日：2001-02-13
申请号：US08910830
申请日：1997-08-13
申请人： Makoto Satoh , Teruyoshi Kiyota , Akio Imai
发明人： Makoto Satoh , Teruyoshi Kiyota , Akio Imai
IPC分类号： C08F444
CPC分类号： C08F10/00 , C08F110/06 , Y10S526/908 , C08F4/6565 , C08F2500/17 , C08F2500/18
摘要： The present invention relates to a solid catalyst component for &agr;-olefin polymerization having a narrow particle size distribution of not less than 6.0 in terms of the value of N in a Rosin-Rammler function of particle size distribution and giving a catalytic activity of not less than 10,000 ((g-polymer produced/g-solid catalyst component)/hour) in polymerization. The catalyst component is obtained by a process which comprises reducing a titanium compound with an organomagnesium compound in the presence of an organosilicon compound and an ester to obtain a solid product, then treating the solid product with: (a) a mixture of titanium tetrachloride and an ether, (b) an organic acid halide, and (c) a mixture of titanium tetrachloride and an ether optionally containing an ester.
摘要翻译：本发明涉及一种用于α-烯烃聚合的固体催化剂组分，其具有窄的粒度分布，在松散Rammler的粒度分布函数中的N值不小于6.0，并且给出的催化活性不低于（（g-聚合物生产/ g-固体催化剂组分）/小时）。催化剂组分通过包括在有机硅化合物和酯存在下还原钛化合物以获得固体产物的方法获得，然后用以下物质处理固体产物：（a）四氯化钛和醚，（b）有机酰卤，和（c）任选含有酯的四氯化钛和醚的混合物。

10. 发明授权

US5854164A Method for preparing catalyst component for olefin polymerization, catalyst for olefin polymerization and process for producing olefin polymer with the catalyst 失效
标题翻译：烯烃聚合催化剂组分的制备方法，烯烃聚合用催化剂和催化剂生产烯烃聚合物的方法
公开(公告)号：US5854164A
公开(公告)日：1998-12-29
申请号：US731439
申请日：1996-10-15
申请人： Hiroyuki Shiraishi , Eiji Nakaishi , Takahiro Hino , Akio Imai
发明人： Hiroyuki Shiraishi , Eiji Nakaishi , Takahiro Hino , Akio Imai
IPC分类号： C08F4/651 , C08F4/653 , C08F4/654 , C08F10/00 , C08F210/16
CPC分类号： C08F10/00 , C08F210/16
摘要： A solid catalyst component (A) for olefin polymerization comprising Mg, Ti, a halogen and a cyclic organic nitrogen compound (C), a solid catalyst comprising the solid catalyst component and an organoaluminum compound, and a process for producing an olefin polymer with the catalyst. According to the present invention, there can be provided an olefin polymerization catalyst having a high catalyst activity per titanium enough to make the removal of catalyst residues unnecessary and a process for producing an olefin polymer having a low content of low molecular weight component with the catalyst.
摘要翻译：包含Mg，Ti，卤素和环状有机氮化合物（C）的固体催化剂组分（A），包含固体催化剂组分和有机铝化合物的固体催化剂，以及烯烃聚合物的制备方法催化剂。根据本发明，可以提供一种对每个钛具有高催化活性的烯烃聚合催化剂，足以使催化剂残留物不必要地除去，以及用催化剂制备低含量低分子量组分的烯烃聚合物的方法。

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