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1. 发明授权

US5679613A Chlorofluoro(hydro)carbon conversion process 失效
标题翻译：氯氟（氢）碳转化工艺
公开(公告)号：US5679613A
公开(公告)日：1997-10-21
申请号：US414236
申请日：1995-03-31
申请人： Hans-Walter Swidersky , Johannes Eicher , Thomas Born , Carsten Brosch , Werner Rudolph
发明人： Hans-Walter Swidersky , Johannes Eicher , Thomas Born , Carsten Brosch , Werner Rudolph
IPC分类号： B01J27/10 , B01J27/12 , B01J27/125 , B01J27/128 , C07B61/00 , C07C17/20 , C07C17/358 , C07C19/12 , B01J27/06
CPC分类号： B01J27/128 , B01J27/10 , B01J27/12 , B01J27/125 , C07C17/358
摘要： A process for preparing R113a from Rl13, and R123 from R123a or R123b by rearrangement over AlCl.sub.3, in which when the reaction mixture is heated sudden start-up of the reaction, which often causes large amounts of heat to be released and the reaction to run away, is prevented by using a specially activated AlCl.sub.3, which has been activated by means of a metal halide selected from the group consisting of NaF.multidot.nHF with 0
摘要翻译：通过在AlCl 3上重排从R133制备R113a的R123和R123a或R123b的R123，其中当反应混合物被加热突然启动时，这通常导致大量的热被释放并且反应进行通过使用已经通过选自具有0

2. 发明授权

US5430201A Chlorofluoro (hydro) carbon conversion process 失效
标题翻译：氯氟（氢）碳转化工艺
公开(公告)号：US5430201A
公开(公告)日：1995-07-04
申请号：US323015
申请日：1994-10-14
申请人： Hans-Walter Swidersky , Johannes Eicher , Thomas Born , Carsten Brosch , Werner Rudolph
发明人： Hans-Walter Swidersky , Johannes Eicher , Thomas Born , Carsten Brosch , Werner Rudolph
IPC分类号： B01J27/10 , B01J27/12 , B01J27/125 , B01J27/128 , C07B61/00 , C07C17/20 , C07C17/358 , C07C19/12 , C07C19/08
CPC分类号： B01J27/128 , B01J27/10 , B01J27/12 , B01J27/125 , C07C17/358
摘要： A process for preparing R113a from R113, and R123 from R123a or R123b by rearrangement over AlCl.sub.3, in which when the reaction mixture is heated sudden start-up of the reaction, which often causes large amounts of heat to be released and the reaction to run away, is prevented by using a specially activated AlCl.sub.3, which has been activated by means of a metal halide selected from the group consisting of NaF.nHF with 0
摘要翻译：从R113制备R113a的方法，R123a或R123b的R123通过在AlCl 3上重排而制备，其中当反应混合物被加热突然启动时，这通常导致大量的热量被释放并且反应运行通过使用已经通过选自具有0

3. 发明授权

US5315046A Process for preparing ethane derivatives 失效
标题翻译：制备乙烷衍生物的方法
公开(公告)号：US5315046A
公开(公告)日：1994-05-24
申请号：US658658
申请日：1991-02-21
申请人： Guenter Fernschild, deceased , Werner Rudolph , Carsten Brosch
发明人： Guenter Fernschild, deceased , Werner Rudolph , Carsten Brosch
IPC分类号： B01J27/12 , C07B61/00 , C07C17/08 , C07C17/087 , C07C17/20 , C07C17/21 , C07C17/38 , C07C19/08 , C07C19/12 , C07C19/14
CPC分类号： C07C19/14 , C07C17/087 , C07C17/206 , C07C17/208 , C07C17/21 , C07C19/12
摘要： A process for preparing ethane derivatives containing the trifluoromethyl group in good yield is described which is carried out in liquid phase and is particularly suitable for preparing CF.sub.3 CHCl.sub.2 (R123).
摘要翻译：描述了以良好的收率制备含有三氟甲基的乙烷衍生物的方法，其以液相进行，特别适用于制备CF 3 CHCl 2（R123）。

4. 发明申请

US20120070749A1 Process for the preparation of 4-fluoro-4-R-5-R'-1,3-dioxolane-2-ones 审中-公开
标题翻译： 4-氟-4-R-5-R'-1,3-二氧戊环-2-酮的制备方法
公开(公告)号：US20120070749A1
公开(公告)日：2012-03-22
申请号：US13321270
申请日：2010-05-26
申请人： Martin Bomkamp , Jens Olschimke , Carsten Brosch , Andreas Grossmann
发明人： Martin Bomkamp , Jens Olschimke , Carsten Brosch , Andreas Grossmann
IPC分类号： H01M10/056 , C07C69/63 , C09K3/00 , C07D317/38
CPC分类号： H01M10/0525 , C07C68/02 , C07C69/96 , C07D317/42 , H01M10/0567 , H01M10/0568 , H01M10/0569
摘要： The present invention concerns 4-fluoro-4-R-5-R′-1,3-dioxolane-2-ones, wherein R is an alkyl group and R′ is H or a C1 to C3 alkyl group, their manufacture, solvent mixtures for lithium ion batteries containing them and conductive salt solutions for lithium ion batteries, e.g. solutions containing LiPF6.
摘要翻译：本发明涉及4-氟-4-R-5-R'-1,3-二氧戊环-2-酮，其中R是烷基，R'是H或C1-C3烷基，它们的制备，溶剂含锂离子电池的混合物和锂离子电池的导电盐溶液，例如含LiPF6的溶液。

5. 发明申请

US20110177693A1 Reversible Water-Free Process for the Separation of Acid-Containing Gas Mixtures 有权
标题翻译：用于分离含酸气体混合物的可逆无水工艺
公开(公告)号：US20110177693A1
公开(公告)日：2011-07-21
申请号：US13078060
申请日：2011-04-01
申请人： Jens Olschimke , Carsten Brosch , Andreas Grossmann
发明人： Jens Olschimke , Carsten Brosch , Andreas Grossmann
IPC分类号： H01L21/461 , C07C53/40 , C01B25/10 , C07C53/48 , C07C53/50
CPC分类号： B01D53/1456 , B01D53/1493 , B01D2257/2042 , B01D2257/2045 , B01D2257/2047 , C01B7/0737 , C01B7/093 , C01B7/195 , Y02E60/324
摘要： Gas mixtures which comprise acids like HF, HCl or HBr and other constituents, especially gas mixtures which comprise or consist of carboxylic acid fluorides, C(O)F2 or phosphorous pentafluoride and HCl and optionally HF, can be separated by ionic liquids. The process is performed reversibly. Ionic liquids are applied the anion of which corresponds to a stronger acid than the acid to be removed. Highly purified products, for example, highly purified carbonyl fluoride can be obtained.
摘要翻译：特别是包含羧酸氟化物C（O）F2或五氟化磷，HCl和任选的HF的含氟气体混合物的气体混合物可以被离子液体分离出来。该过程是可逆的。使用离子液体的阴离子对应于比要除去的酸更强的酸。可以得到高纯度的产品，例如高度纯化的碳酰氟。

6. 发明申请

US20090211449A1 Method for separating gas 有权
标题翻译：气体分离方法
公开(公告)号：US20090211449A1
公开(公告)日：2009-08-27
申请号：US11666581
申请日：2005-10-20
申请人： Jens Olschimke , Saskia Braukmüller , Carsten Brosch
发明人： Jens Olschimke , Saskia Braukmüller , Carsten Brosch
IPC分类号： B01D53/14
CPC分类号： C01B7/0737 , B01D53/1456 , B01D53/1493 , B01D2257/2042 , B01D2257/2045 , C01B7/0731 , C01B7/093 , C01B7/195 , C07C51/47 , C07D233/64 , C07C53/48 , C07C53/46 , C07C53/40
摘要： Gas mixtures containing HF, HCl or HBr and other constituents, in particular gas mixtures containing carboxylic acid fluorides, C(O)F2 or phosphorus pentafluoride and HCl and possibly HF, can be fractionated by means of ionic liquids.
摘要翻译：含有HF，HCl或HBr和其他组分的气体混合物，特别是含有羧酸氟化物，C（O）F 2或五氟化磷和HCl以及可能的HF的气体混合物可以通过离子液体分级。

7. 发明授权

US07145046B2 Production of fluorine compounds 失效
标题翻译：生产氟化合物
公开(公告)号：US07145046B2
公开(公告)日：2006-12-05
申请号：US10632103
申请日：2003-08-01
申请人： Max Braun , Carsten Brosch
发明人： Max Braun , Carsten Brosch
IPC分类号： C07C17/20 , C07C17/02 , C07C17/04 , C07C17/08 , C07C17/087
CPC分类号： C01B17/4561 , C01B17/4576 , C07B39/00 , C07C17/206 , C07C67/307 , C07C69/63
摘要： Inorganic and organic compounds containing fluorine can be produced, for example, from corresponding chlorine-containing compounds by chlorine/fluorine exchange using fluorinating agents. Monocyclic or bicyclic compounds containing at least two nitrogen atoms, at least one of which is incorporated into the ring system, can be used as catalysts or fluorinating agents for chlorine/fluorine exchange reactions to produce sulfurylchlorofluoride, sulfurylfluoride or a carboxylic acid fluoride. It is likewise possible to carry out HF addition to unsaturated carbon-carbon bonds or chlorine/fluorine exchange at carbon atoms. For example, monochloro or dichloro malonic acid esters can be converted to difluoro malonic acid esters. Work-up of the reaction mixture can be simplified by using suitable solvents which force the reaction mixture to exist in two phases.
摘要翻译：含氟的无机和有机化合物可以例如通过使用氟化剂的氯/氟交换从相应的含氯化合物制备。含有至少两个氮原子（其中至少一个被引入环系中）的单环或双环化合物可以用作氯/氟交换反应的催化剂或氟化剂，以产生磺酰氯，磺酰氟或羧酸氟化物。同样可以在碳原子处进行HF添加到不饱和碳 - 碳键或氯/氟交换。例如，一氯或二氯丙二酸酯可以转化为二氟丙二酸酯。反应混合物的后处理可以通过使用强制反应混合物在两相中存在的合适的溶剂来简化。

8. 发明授权

US07282120B2 UV-activated chlorination process 失效
标题翻译：紫外线活化氯化法
公开(公告)号：US07282120B2
公开(公告)日：2007-10-16
申请号：US11008109
申请日：2004-12-10
申请人： Max Braun , Kerstin Eichholz , Stefan Palsherm , Carsten Brosch
发明人： Max Braun , Kerstin Eichholz , Stefan Palsherm , Carsten Brosch
IPC分类号： C07B63/00 , C07C17/00
CPC分类号： C07C17/10 , C07C17/04 , C07C17/395 , C07C19/01 , C07C19/12 , C07C19/08
摘要： A method of producing alkanes containing chlorine by addition of chlorine to C—C double bonds or C—C triple bonds or by exchange of hydrogen for chlorine by contacting the starting compound in the gas or liquid phase with elemental chlorine and irradiating the reaction mixture with UV light having a wavelength of λ≧280 nm. In this way pentachloroethane can be produced from trichloroethylene, CFC-113 from HCFC-123 or HFC-133a, CFC-112a from HCFC-142b, or HCFC-123 from HCFC-133a. The method also is suitable for separating photochlorinatable impurities from HFC-365-mfc to obtain purified HFC-365-mfc. Advantages include high yields and excellent selectivity.
摘要翻译：通过将氯气加入到CC双键或CC三键中，或通过使气相或液相中的起始化合物与元素氯接触并将反应混合物与具有 λ> 280nm波长。以这种方式，可以从三氯乙烯，来自HCFC-123的CFC-113或HFC-133a，来自HCFC-142b的CFC-112a或来自HCFC-133a的HCFC-123制备五氯乙烷。该方法也适用于从HFC-365-mfc分离光可氯化杂质，得到纯化的HFC-365-mfc。优点包括高产率和极好的选择性。

9. 发明申请

US20060036118A1 Catalyst synthesis of halogenated compounds with catalyst regeneration with elemental halogen 失效
标题翻译：用元素卤素催化剂再生催化合成卤化物
公开(公告)号：US20060036118A1
公开(公告)日：2006-02-16
申请号：US11259138
申请日：2005-10-27
申请人： Max Braun , Carsten Brosch
发明人： Max Braun , Carsten Brosch
IPC分类号： C07C17/013
CPC分类号： C07C17/206 , B01J27/08 , B01J27/32 , B01J38/42 , C01G30/007 , C07C17/00 , C07C17/087 , C07C17/21 , Y02P20/584 , C07C19/08 , C07C19/12 , C07C19/10
摘要： Catalysts such as antimony halides, which are useful in fluorination reactions involving hydrogen fluoride, may be reduced during the reaction and require regeneration. Regenerative oxidation is usually carried out by introducing elemental halogen, preferably fluorine or chlorine, into the reaction mixture. In accordance with the invention elemental halogen is prevented from coming into contact with starting materials or intermediate products which are reactive therewith. This is preferably achieved by withdrawing part of the reaction mixture from the reactor, mixing the withdrawn part with chlorine or fluorine in order to regenerate the catalyst, and thereafter returning the withdrawn part to the reactor.
摘要翻译：可用于涉及氟化氢的氟化反应中的锑卤化物等催化剂可在反应期间减少并需要再生。再生氧化通常通过将元素卤素，优选氟或氯引入反应混合物中来进行。根据本发明，防止元素卤素与与其反应的原料或中间产物接触。优选通过将部分反应混合物从反应器中取出，将取出的部分与氯或氟混合以使催化剂再生，然后将引出的部分返回到反应器中来实现。

10. 发明授权

US06720465B2 Preparation of highly pure fluorine compounds 失效
标题翻译：高纯氟化合物的制备
公开(公告)号：US06720465B2
公开(公告)日：2004-04-13
申请号：US10086636
申请日：2002-03-04
申请人： Max Braun , Carsten Brosch , Heinz Gress
发明人： Max Braun , Carsten Brosch , Heinz Gress
IPC分类号： C07C1738
CPC分类号： C07C19/08 , C07C17/383 , C07C17/395
摘要： A process for preparing purified, saturated, partially fluorinated or perfluorinated hydrocarbon compounds from crude products which are contaminated with impurity compounds which absorb light at a wavelength of &lgr;>200 nm by irradiating the crude product with UV radiation of a wavelength of &lgr;>200 nm and thereafter recovering highly pure, partially fluorinated or perfluorinated hydrocarbon compounds from the irradiated reaction product, for example, by simple vacuum distillation.
摘要翻译：从粗产物制备纯化，饱和，部分氟化或全氟化烃化合物的方法，其通过用波长λ> 200nm的UV辐射照射粗产物而被波长λ> 200nm的吸收光的杂质化合物污染然后例如通过简单的真空蒸馏从照射的反应产物中回收高纯度，部分氟化的或全氟化的烃化合物。

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