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1. 发明申请

US20170340986A1 DISTILLATION PROCESS COMPRISING AT LEAST TWO DISTILLATION STEPS TO OBTAIN PURIFIED HALOGENATED CARBOXYLIC ACID HALIDE, AND USE OF THE PURIFIED HALOGENATED CARBOXYLIC ACID HALIDE 审中-公开
公开(公告)号：US20170340986A1
公开(公告)日：2017-11-30
申请号：US15527436
申请日：2015-11-17
申请人： SOLVAY SA
发明人： Max Josef BRAUN
IPC分类号： B01D3/14 , C07C53/48 , C07C51/64
CPC分类号： B01D3/143 , C07C51/64 , C07C53/48
摘要： The present invention concerns a process for the production of a fluorinated carboxylic halide having a reduced content of impurities, a fraction of the fluorinated carboxylic halide having a reduced content of impurities, and its use in the manufacture of agriculturally and pharmaceutically active compounds or their intermediates.

2. 发明申请

US20170267622A1 Distillation process comprising at least two distillation steps to obtain purified halogenated carboxylic acid halide, and use of the purified halogenated carboxylic acid halide 有权
公开(公告)号：US20170267622A1
公开(公告)日：2017-09-21
申请号：US15505755
申请日：2015-08-13
申请人： SOLVAY SA
发明人： Max Josef BRAUN
IPC分类号： C07C51/64
CPC分类号： C07C51/64 , C07C53/48 , C07C53/50
摘要： The present invention concerns a process for the obtention of a halogenated carboxylic halide having a reduced content of impurities, a fraction of the halogenated carboxylic halide having a reduced content of impurities, and its use in the manufacture of agriculturally and pharmaceutically active compounds.

3. 发明授权

US09234133B2 Etching gas 有权
标题翻译：蚀刻气体
公开(公告)号：US09234133B2
公开(公告)日：2016-01-12
申请号：US14455128
申请日：2014-08-08
申请人： Central Glass Company, Limited
发明人： Naoto Takada , Isamu Mori
IPC分类号： H01L21/302 , C09K13/00 , H01L21/3065 , C07C53/48 , H01L21/311 , C23F1/12
CPC分类号： C09K13/00 , C07C53/48 , C23F1/12 , H01L21/3065 , H01L21/31116
摘要： Disclosed is an etching gas provided containing CHF2COF. The etching gas may contain, as an additive, at least one kind of gas selected from O2, O3, CO, CO2, F2, NF3, Cl2, Br2, I2, XFn (In this formula, X represents Cl, I or Br. n represents an integer satisfying 1≦n≦7.), CH4, CH3F, CH2F2, CHF3, N2, He, Ar, Ne, Kr and the like, from CH4, C2H2, C2H4, C2H6, C3H4, C3H6, C3H8, HI, HBr, HCl, CO, NO, NH3, H2 and the like, or from CH4, CH3F, CH2F2 and CHF3. This etching gas is not only excellent in etching performances such as the selection ratio to a resist and the patterning profile but also easily available and does not substantially by-produce CF4 that places a burden on the environment.
摘要翻译：公开了提供含有CHF 2 COF的蚀刻气体。蚀刻气体可以含有选自O 2，O 3，CO，CO 2，F 2，NF 3，Cl 2，Br 2，I 2，X F n中的至少一种气体作为添加剂（在该式中，X表示Cl，I或Br。 n表示从CH 4，C 2 H 2，C 2 H 4，C 2 H 6，C 3 H 4，C 3 H 6，C 3 H 8，H 1，CH 3，CH 3，CH 3，CH 3，CH 3，，HBr，HCl，CO，NO，NH3，H2等，或来自CH4，CH3F，CH2F2和CHF3。该蚀刻气体不仅具有优异的蚀刻性能，例如抗蚀剂的选择比和图案形貌，而且易于获得，并且基本上不产生对环境造成负担的CF4。

4. 发明授权

US09156771B2 Process for the preparation of enolate salts of 4-fluoro-2-hydroxymethylene-3 oxo-butyrates 有权
标题翻译：制备4-氟-2-羟基亚甲基-3-氧代 - 丁酸酯的烯醇盐的方法
公开(公告)号：US09156771B2
公开(公告)日：2015-10-13
申请号：US13809739
申请日：2011-07-11
申请人： Martina Eichenberger , Paul Hanselmann , Florencio Zaragoza Dörwald
发明人： Martina Eichenberger , Paul Hanselmann , Florencio Zaragoza Dörwald
IPC分类号： C07C51/58 , C07C51/62 , C07C67/14 , C07C67/31 , C07C67/343 , C07C69/14 , C07C69/738
CPC分类号： C07C67/31 , C07C51/58 , C07C51/62 , C07C67/14 , C07C67/343 , C07C69/14 , C07C69/738 , C07C53/48 , C07C59/21
摘要： Enolate salts of 4-fluoro-2-hydroxymethylene-3-oxobutyrates of formula wherein R1 is C1-10 alkyl, R2 and R3 are independently hydrogen or fluorine, M is an alkali or alkaline earth metal, and n is 1 or 2, are prepared from enolate salts of the corresponding 4-fluoro-3-oxobutyrates and carbon monoxide. The enolate salts of formula I can be alkylated or acylated to obtain the corresponding enol ethers and esters. The 4-fluoro-3-oxobutyrate starting material can be prepared from 1,1-difluoroethyl methyl ethers by SbF5-catalyzed fluoromethane elimination followed by halogen exchange with lithium chloride, reacting the thus obtained fluoroacetyl chloride with ketene and quenching with the appropriate alcohol R1—OH.
摘要翻译： 4-氟-2-羟基亚甲基-3-氧代丁酸烯醇盐，其中R 1是C 1-10烷基，R 2和R 3独立地是氢或氟，M是碱金属或碱土金属，n是1或2是由相应的4-氟-3-氧代丁酸乙酯和一氧化碳的烯醇盐制备。式I的烯醇盐可以被烷基化或酰化以得到相应的烯醇醚和酯。 4-氟-3-氧代丁酸酯原料可以由1,1-二氟乙基甲基醚通过SbF 5催化的氟甲烷消除制备，随后与氯化锂进行卤素交换，使得到的氟乙酰氯与乙烯酮反应，并用适当的醇R 1 -哦。

5. 发明申请

US20150246899A1 PROCESS FOR THE PREPARATION OF DABIGATRAN ETEXILATE OR PHARMACEUTICALLY ACCEPTABLE SALT THEREOF 审中-公开
标题翻译：制备DABIGATRAN ETEXILATE或其药学上可接受的盐的方法
公开(公告)号：US20150246899A1
公开(公告)日：2015-09-03
申请号：US14430303
申请日：2013-09-30
申请人： RANBAXY LABORATORIES LIMITED
发明人： Anandam Vempali , Sudhir Singh Sanwal , Balaguru Murugesan , Swargam Sathyanarayana , Rajesh Kumar Thaper , Mohan Prasad
IPC分类号： C07D401/12 , C07C53/48 , C07C53/10 , C07D213/75 , C07C309/19
CPC分类号： C07D401/12 , C07C53/10 , C07C53/48 , C07C309/19 , C07D213/75
摘要： The present invention relates to a process for the preparation of dabigatran etexilate. The present invention also relates to trifluoroacetate salt of dabigatran etexilate and a process for its preparation. The present invention further relates to crystalline Form I and crystalline Form II of trifluoroacetate salt of dabigatran etexilate and processes for their preparation. The present invention further relates to a process for the preparation of pharmaceutically acceptable salts, including methanesulfonate salt, of dabigatran etexilate.
摘要翻译：本发明涉及制备达比加群酯的方法。本发明还涉及达比加群酯的三氟乙酸盐及其制备方法。本发明还涉及达比加群酯的三氟乙酸盐的晶型I和结晶形式II及其制备方法。本发明还涉及制备达比加群酯的药学上可接受的盐，包括甲磺酸盐的方法。

6. 发明申请

US20140031588A1 Method for Purifying Difluoroacetic Acid Chloride 有权
标题翻译：纯化二氟乙酸氯化物的方法
公开(公告)号：US20140031588A1
公开(公告)日：2014-01-30
申请号：US14000754
申请日：2012-03-28
申请人： Naoto Takada , Masamune Okamoto , Hideaki Imura
发明人： Naoto Takada , Masamune Okamoto , Hideaki Imura
IPC分类号： C07C51/64
CPC分类号： C07C51/64 , C07C51/58 , C07C51/60 , C07C53/48
摘要： A method for purifying difluoroacetic acid chloride, including the step of bringing a difluoroacetic acid chloride composition that contains at least difluoroacetic acid fluoride into contact with calcium chloride at a temperature enabling reaction thereof thereby converting difluoroacetic acid fluoride into difluoroacetic acid chloride.
摘要翻译：一种纯化二氟乙酰氯的方法，包括使含有至少二氟乙酸氟化物的二氟乙酰氯组合物与氯化钙接触的步骤，使其反应，从而将二氟乙酸氟化物转化为二氟乙酸氯化物。

7. 发明授权

US08187489B1 Biodegradable ionic liquids for aircraft deicing 有权
标题翻译：用于飞机除冰的可生物降解的离子液体
公开(公告)号：US08187489B1
公开(公告)日：2012-05-29
申请号：US13069671
申请日：2011-03-23
申请人： Matthew C. Davis
发明人： Matthew C. Davis
IPC分类号： C09K3/18 , C07C209/00
CPC分类号： C09K3/185 , C07C53/06 , C07C53/10 , C07C53/122 , C07C53/48 , C07C57/03 , C07C59/06 , C07C59/19 , C07C215/40 , C07C229/08
摘要： A process and deicing composition.
摘要翻译：过程和除冰组合物。

8. 发明申请

US20090253905A1 PROCESS FOR THE PREPARATION OF ONIUM SALTS WITH ALKYL- OR ARYLSULFONATE ANIONS OR ALKYL- OR ARYLCARBOXYLATE ANIONS HAVING A LOW HALIDE CONTENT 审中-公开
标题翻译：用碱金属离子或芳基磺酸盐阴离子或碱金属或芳香族羧酸盐阴离子制备低盐含量的方法
公开(公告)号：US20090253905A1
公开(公告)日：2009-10-08
申请号：US11721617
申请日：2005-11-18
申请人： Nikolai (Mykola) Ignatyev , Urs Weiz-Biermann , Andriy Kucheryna , Helge Willner
发明人： Nikolai (Mykola) Ignatyev , Urs Weiz-Biermann , Andriy Kucheryna , Helge Willner
IPC分类号： C07D265/30 , C07D233/54 , C07D213/20 , C07D295/02 , C07F7/02 , C07D249/04 , C07D239/02 , C07D237/02 , C07D241/02 , C07D277/20 , C07D263/02 , C07D231/02 , C07D249/08
CPC分类号： C07D295/023 , C07C51/412 , C07C51/60 , C07C279/04 , C07C303/32 , C07D207/04 , C07D213/06 , C07D213/20 , C07D213/74 , C07D233/54 , C07D295/037 , C07F9/5407 , C07C53/18 , C07C53/48 , C07C309/04 , C07C309/06 , C07C309/29 , C07C309/30
摘要： The invention relates to a method for producing onium salts comprising alkyl anions or aryl sulfonate anions or alkyl carboxylate anions or acryl carboxylate anions by reacting an onium halide with an alkyl silyl ester or trialkyl silyl ester of an alkyl sulfonic acid or aryl sulfonic acid or an alkyl carboxylic acid or aryl carboxylic acid or the anhydrides thereof.
摘要翻译：本发明涉及一种通过使卤鎓鎓与烷基磺酸或芳基磺酸的烷基甲硅烷基酯或三烷基甲硅烷基酯反应来制备包含烷基阴离子或芳基磺酸根阴离子或羧酸烷基酯阴离子或羧酸烷基酯阴离子的方法，烷基羧酸或芳基羧酸或其酸酐。

9. 发明申请

US20050113606A1 Continuous production of chlorodifluoroacetyl fluoride via chlorotrifluoroethylene oxidation 审中-公开
标题翻译：通过氯三氟乙烯氧化连续生产氯二氟乙酰氟
公开(公告)号：US20050113606A1
公开(公告)日：2005-05-26
申请号：US10718475
申请日：2003-11-20
申请人： Robert Bell , Timothy Demmin , David Bradley , David Nalewajek
发明人： Robert Bell , Timothy Demmin , David Bradley , David Nalewajek
IPC分类号： C07C51/21 , C07C51/58
CPC分类号： C07C51/58 , C07C53/48
摘要： The invention pertains to a process for preparing chlorodifluoroacetyl fluoride (CDAF) by oxidation of chlorotrifluoroethylene (CTFE) in a solvent using a continuously stirred tank reactor. It provides a process for the production of chlorodifluoroacetyl fluoride by comprises reacting a solvent solution of chlorotrifluoroethylene with oxygen in a reactor to form a product which comprises chlorodifluoroacetyl fluoride. The reacting may be conducted in a continuous or batch mode.
摘要翻译：本发明涉及通过使用连续搅拌釜式反应器在溶剂中氧化三氟氯乙烯（CTFE）来制备氯二氟乙酰氟（CDAF）的方法。它提供了一种生产氯二氟乙酰氟的方法，包括在反应器中使氯三氟乙烯的溶剂溶液与氧反应形成包含氯二氟乙酰氟的产物。反应可以以连续或间歇的方式进行。

10. 发明授权

US3880923A Production of alpha-chlorocarboxylic acid chlorides 失效
标题翻译：生产α-氯代羧酸氯化物
公开(公告)号：US3880923A
公开(公告)日：1975-04-29
申请号：US42637273
申请日：1973-12-19
申请人： BASF AG
发明人： SCHEIDMEIR WALTER , BRESSEL ULRICH , HOHENSCHUTZ HEINZ
IPC分类号： C07C53/46 , C07C51/00 , C07C51/62 , C07C67/00 , C07C53/14
CPC分类号： C07C51/62 , C07C53/48
摘要： An improved process for the production of Alpha chlorocarboxylic acid chlorides by reaction of a carboxylic acid chloride with chlorine at elevated temperature, wherein the improvement consists in carrying out the reaction in the presence of sulfuric acid. Alpha -chlorocarboxylic acid chlorides are suitable for the production of plant protection agents.
摘要翻译：通过羧酸酰氯与氯在升高的温度下反应制备α-氯代羧酸氯化物的改进方法，其中改进在于在硫酸存在下进行反应。 α-氯代羧酸氯化物适用于生产植物保护剂。

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