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1. 发明申请

US20080249307A1 Method for Producing Ethylene Amines 失效
标题翻译：生产乙烯胺的方法
公开(公告)号：US20080249307A1
公开(公告)日：2008-10-09
申请号：US12089775
申请日：2006-10-06
申请人： Gunther van Cauwenberge , Johann-Peter Melder , Kirsten Dahmen , Klemens Massonne , Steffen Oehlenschlager , Kai Michael Exner
发明人： Gunther van Cauwenberge , Johann-Peter Melder , Kirsten Dahmen , Klemens Massonne , Steffen Oehlenschlager , Kai Michael Exner
IPC分类号： C07D241/04 , C07C209/08
CPC分类号： C07C209/08 , C07C211/10 , C07C211/14
摘要： Processes are described comprising: (i) providing a reactant comprising 1,2-dichloroethane; and (ii) reacting the reactant with ammonia to form a reaction product comprising one or more ethylene amines and hydrogen chloride, wherein the reaction is carried out in the presence of an organic, nitrogen- or phosphorus-containing compound which reacts with the hydrogen chloride to form an ionic liquid.
摘要翻译：描述了方法，其包括：（i）提供包含1,2-二氯乙烷的反应物; 和（ii）使反应物与氨反应以形成包含一种或多种亚乙基胺和氯化氢的反应产物，其中该反应在与氯化氢反应的有机，含氮或磷的化合物存在下进行以形成离子液体。

2. 发明申请

US20080293973A1 Process for the Synthesis of Dmapa 有权
标题翻译：合成Dmapa的过程
公开(公告)号：US20080293973A1
公开(公告)日：2008-11-27
申请号：US12092684
申请日：2006-10-31
申请人： Martin Ernst , Steffen Oehlenschlager , Frank Kuhnke , Karl-Heinz Ross , Roland Deeg , Johann-Peter Melder
发明人： Martin Ernst , Steffen Oehlenschlager , Frank Kuhnke , Karl-Heinz Ross , Roland Deeg , Johann-Peter Melder
IPC分类号： C07C209/48 , B01J19/00
CPC分类号： B01J8/20 , B01D3/14 , B01J2219/00006 , B01J2219/00029 , B01J2219/0004 , C07C209/48 , C07C211/11
摘要： The present invention relates to a process for the industrial preparation of a diamine starting from a corresponding alkenyl nitrile comprising at least one C-C double bond, which comprises the steps (a) reaction of the alkenyl nitrile with a corresponding monoamine in a first reactor so that the monoamine adds exothermically onto the at least one double bond to form an aminoalkyl nitrile, with the monoamine and water being charged initially and the alkenyl nitrile being fed in; (b) evaporation of unreacted alkenyl nitrile and monoamine to increase the concentration of the aminoalkyl nitrile product in the bottoms of the first reactor; (c) transfer of the aminoalkyl nitrile bottom product from step (b) to a second reactor; (d) batchwise catalytic hydrogenation of the aminoalkyl nitrile transferred in step (c) to the diamine in the second reactor, with each batch being obtained by initially charging a catalyst suitable for the hydrogenation of nitriles to amines and also water, the desired diamine and a base, introducing hydrogen into the second reactor and feeding in the aminoalkyl nitrile transferred in step (c); and (e) isolation of the diamine and, if appropriate, repetition of the steps (a) to (e). The invention further relates to an apparatus for preparing these diamines and the use of the apparatuses. A preferred diamine is 3-dimethylaminopropylamine (DMAPA).
摘要翻译：本发明涉及从包含至少一个CC双键的相应烯基腈开始工业制备二胺的方法，其包括步骤（a）在第一反应器中使链烯基腈与相应的单胺反应，使得单胺在至少一个双键上放热添加以形成氨基烷基腈，最初加入单胺和水，并加入链烯基腈; （b）蒸发未反应的烯基腈和单胺以增加第一反应器底部氨基烷基腈产物的浓度; （c）将氨基烷基腈底部产物从步骤（b）转移至第二反应器; （d）将步骤（c）中转移的氨基烷基腈分批催化氢化为第二反应器中的二胺，每个批次通过首先将适合于将腈氢化成的催化剂加入到胺中而得到，并且还需要水，所需的二胺和碱，将氢气引入第二反应器并进料步骤（c）中转移的氨基烷基腈; 和（e）分离二胺，如果合适，重复步骤（a）至（e）。本发明还涉及一种用于制备这些二胺的装置和该装置的用途。优选的二胺是3-二甲基氨基丙胺（DMAPA）。

3. 发明申请

US20100015012A1 METHOD FOR PRODUCING AROMATIC AMINES OR ALIPHATIC AMINO ALCOHOLS 审中-公开
标题翻译：生产芳族氨基酸或氨基氨基醇的方法
公开(公告)号：US20100015012A1
公开(公告)日：2010-01-21
申请号：US12505238
申请日：2009-07-17
申请人： Dominic Vanoppen , Frederik Van Laar , Thomas Beuermann , Georg Krug , Steffen Oehlenschlager , Ekkehard Schwab , Hartwig Voss , Konrad Morgenschweis , Ulrich Penzel , Dietrich Tittelbach-Helmrich
发明人： Dominic Vanoppen , Frederik Van Laar , Thomas Beuermann , Georg Krug , Steffen Oehlenschlager , Ekkehard Schwab , Hartwig Voss , Konrad Morgenschweis , Ulrich Penzel , Dietrich Tittelbach-Helmrich
IPC分类号： B01J19/00
CPC分类号： B01J19/0033 , B01J8/006 , B01J8/007 , B01J8/22 , B01J19/002 , B01J2208/00637 , B01J2219/002 , B01J2219/00225 , B01J2219/00263 , C07C209/36 , G01N21/31 , C07C211/51
摘要： The invention relates to a process for preparing aromatic amines by hydrogenation of nitroaromatics in the presence of catalysts, in which a fluid reaction mixture which comprises amines and from which the catalysts are separated off is formed in a reactor. After the catalysts have been separated off, a measurement of the absorption of UV/VIS radiation by the reaction mixture is carried out to determine the concentration of nitro and nitroso compounds in the reaction mixture.
摘要翻译：本发明涉及通过在催化剂存在下氢化硝基芳族化合物来制备芳族胺的方法，其中在反应器中形成包含胺并在其中分离催化剂的流体反应混合物。催化剂分离后，进行反应混合物对UV / VIS辐射吸收的测定，以确定反应混合物中硝基和亚硝基化合物的浓度。

4. 发明申请

US20080177111A1 METHOD FOR THE PRODUCTION OF AMINES 有权
标题翻译：生产氨基酸的方法
公开(公告)号：US20080177111A1
公开(公告)日：2008-07-24
申请号：US12057617
申请日：2008-03-28
申请人： Frederik van Laar , Ekkehard Schwab , Steffen Oehlenschlager , Hartwig Voss , Wolfgang Mackenroth , Konrad Morgenschweis , Ulrich Penzel , Bernd Weidner
发明人： Frederik van Laar , Ekkehard Schwab , Steffen Oehlenschlager , Hartwig Voss , Wolfgang Mackenroth , Konrad Morgenschweis , Ulrich Penzel , Bernd Weidner
IPC分类号： C07C209/00
CPC分类号： C07C209/36 , B01J21/18 , B01J23/892 , B01J37/03 , B01J37/14 , B01J37/18 , C07C211/51
摘要： The present invention provides a process for hydrogenating aromatic nitro compounds to the corresponding amines in the presence of hydrogenation catalysts, which comprises using hydrogenation catalysts in which nickel and platinum are present on a support in the form of an alloy having an atomic ratio of nickel to platinum in the alloy of between 30:70 and 70:30.
摘要翻译：本发明提供了在氢化催化剂存在下将芳族硝基化合物氢化成相应的胺的方法，该方法包括使用氢化催化剂，其中镍和铂以合金的形式存在于载体上，其原子比为镍与合金中的铂在30:70和70:30之间。

5. 发明申请

US20080146848A1 Method for Producing Aromatic Amines or Aliphatic Amino Alcohols 失效
标题翻译：生产芳香胺或脂族氨基醇的方法
公开(公告)号：US20080146848A1
公开(公告)日：2008-06-19
申请号：US11816658
申请日：2006-02-22
申请人： Dominic Vanoppen , Frederik van Laar , Thomas Beuemann , Georg Krug , Steffen Oehlenschlager , Ekkehard Schwab , Hartwig Voss , Konrad Morgenschweis , Ulrich Penzel , Dietrich Tittelbach-Helmrich
发明人： Dominic Vanoppen , Frederik van Laar , Thomas Beuemann , Georg Krug , Steffen Oehlenschlager , Ekkehard Schwab , Hartwig Voss , Konrad Morgenschweis , Ulrich Penzel , Dietrich Tittelbach-Helmrich
IPC分类号： C07C211/50 , B01J14/00
CPC分类号： B01J19/0033 , B01J8/006 , B01J8/007 , B01J8/22 , B01J19/002 , B01J2208/00637 , B01J2219/002 , B01J2219/00225 , B01J2219/00263 , C07C209/36 , G01N21/31 , C07C211/51
摘要： The invention relates to a process for preparing aromatic amines by hydrogenation of nitroaromatics in the presence of catalysts, in which a fluid reaction mixture which comprises amines and from which the catalysts are separated off is formed in a reactor. After the catalysts have been separated off, a measurement of the absorption of UV/VIS radiation by the reaction mixture is carried out to determine the concentration of nitro and nitroso compounds in the reaction mixture.
摘要翻译：本发明涉及通过在催化剂存在下氢化硝基芳族化合物来制备芳族胺的方法，其中在反应器中形成包含胺并在其中分离催化剂的流体反应混合物。催化剂分离后，进行反应混合物对UV / VIS辐射吸收的测定，以确定反应混合物中硝基和亚硝基化合物的浓度。

6. 发明申请

US20070149814A1 Method for the production of amines 审中-公开
标题翻译：制备胺的方法
公开(公告)号：US20070149814A1
公开(公告)日：2007-06-28
申请号：US10575924
申请日：2004-10-15
申请人： Frederik van Laar , Ekkehard Schwab , Steffen Oehlenschlager , Hartwig Voss , Wolfgang Mackenroth , Konrad Morgenschweis , Ulrich Penzel , Bernd Weidner
发明人： Frederik van Laar , Ekkehard Schwab , Steffen Oehlenschlager , Hartwig Voss , Wolfgang Mackenroth , Konrad Morgenschweis , Ulrich Penzel , Bernd Weidner
IPC分类号： C07C209/36 , B01J21/00
CPC分类号： C07C209/36 , B01J21/18 , B01J23/892 , B01J37/03 , B01J37/14 , B01J37/18 , C07C211/51
摘要： The present invention provides a process for hydrogenating aromatic nitro compounds to the corresponding amines in the presence of hydrogenation catalysts, which comprises using hydrogenation catalysts in which nickel and platinum are present on a support in the form of an alloy having an atomic ratio of nickel to platinum in the alloy of between 30:70 and 70:30.
摘要翻译：本发明提供了在氢化催化剂存在下将芳族硝基化合物氢化成相应的胺的方法，该方法包括使用氢化催化剂，其中镍和铂以合金的形式存在于载体上，其原子比为镍与合金中的铂在30:70和70:30之间。

7. 发明申请

US20050177003A1 Method for the production of amines 有权
标题翻译：制备胺的方法
公开(公告)号：US20050177003A1
公开(公告)日：2005-08-11
申请号：US10500862
申请日：2003-01-30
申请人： Dominic Vanoppen , Ekkehard Schwab , Frederik Laar , Hartwig Voss , Steffen Oehlenschlager , Wolfgang Mackenroth , Konrad Morgenschweis , Ulrich Penzel
发明人： Dominic Vanoppen , Ekkehard Schwab , Frederik Laar , Hartwig Voss , Steffen Oehlenschlager , Wolfgang Mackenroth , Konrad Morgenschweis , Ulrich Penzel
IPC分类号： C07C29/36 , C07C209/36 , C07C209/86
CPC分类号： C07C209/36 , C07C209/86 , C07C211/50 , C07C211/46
摘要： The invention provides a process for preparing amines by catalytic hydrogenation of nitroaromatics and subsequent removal of the catalysts from the reaction mixture, which contains at least one aromatic amine and water, which comprises carrying out the removal of the catalysts by means of membrane filtration, which is carried out at a pressure on the suspension side of from 5 to 50 bar, a pressure difference between the suspension side and the permeate side of at least 0.3 bar and a flux rate on the suspension side of from 1 to 6 m/s.
摘要翻译：本发明提供了一种通过硝基芳族化合物的催化氢化和随后从含有至少一种芳族胺和水的反应混合物中除去催化剂来制备胺的方法，其包括通过膜过滤进行催化剂的除去，在悬浮侧的压力为5至50巴，悬浮液侧和渗透侧之间的压力差为至少0.3巴，悬浮侧的通量速率为1至6m / s。

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