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1. 发明授权

US4874849A Asymmetric 1:2-chromium complex dyes containing two azo dyes, one containing an acetoacetanilide coupling component 失效
标题翻译：含有两种偶氮染料的不对称1：2-铬络合物染料，一种含有乙酰乙酰苯胺偶联组分
公开(公告)号：US4874849A
公开(公告)日：1989-10-17
申请号：US944621
申请日：1986-12-19
申请人： Gerhard Back , Fabic Beffa , Ulrich Schlesinger , Alois Puntener
发明人： Gerhard Back , Fabic Beffa , Ulrich Schlesinger , Alois Puntener
IPC分类号： C09B45/26 , D06P1/10 , D06P3/32
CPC分类号： C09B45/26 , D06P1/10 , D06P3/322
摘要： Dyes suitable for dyeing wool, polyamide and leather in orange, brown or olive-brown shades are disclosed, the dyes having the formula ##STR1## wherein A and D are each independently of the other a benzene or napththalene radical of a diazo component, which component carries the hydroxyl or carboxyl group in the ortho-position to the azo group;B is the radical of a coupling component which carries the group X adjacent to the azo group;X is oxygen or a radical of the formula --R--, in which R is hydrogen or C.sub.1 -C.sub.4 alkyl;Y is a radical of the formula ##STR2## in which formulae R.sup.1 and R.sup.5 are each independently of the other hydrogen or sulfo, R.sup.4 is hydrogen or nitro, R.sup.6 is hydrogen, methyl, methoxy or chlorine and R.sup.2 and R.sup.3 are each independently of the other hydrogen, halogen, nitro or sulfo;Ar.sup.1 is a benzene or napththalene radical which is unsubstituted or substituted by halogen, nitro, sulfo, C.sub.1 -C.sub.4 -alkyl or C.sub.1 -C.sub.4 -alkoxy;m is 0 or 1;n is an integer from 1 to 7; andKa.sup..sym. is a cation.
摘要翻译：公开了适用于以橙色，棕色或橄榄棕色色调染色羊毛，聚酰胺和皮革的染料，具有式“IMAGE”的染料，其中A和D各自独立地为重氮组分的苯或萘基，其中成分在偶氮基的邻位含有羟基或羧基; B是携带邻近偶氮基团的基团X的偶合组分的基团; X是氧或式-R-的基团，其中R是氢或C 1 -C 4烷基; Y是式中的基团，其中R 1和R 5各自独立地为氢或磺基，R 4是氢或硝基，R 6是氢，甲基，甲氧基或氯，R2和R3各自独立地为氢，卤素，硝基或磺基; Ar1是未被取代或被卤素，硝基，磺基，C 1 -C 4 - 烷基或C 1 -C 4 - 烷氧基取代的苯或萘基; m为0或1; n为1〜7的整数; 而Ka（+）是阳离子。

2. 发明授权

US4818246A Process for improving the light-fastness of leather dyeings 失效
标题翻译：提高皮革染色牢度的方法
公开(公告)号：US4818246A
公开(公告)日：1989-04-04
申请号：US097269
申请日：1987-09-17
申请人： Alois Puntener , Gerhard Back , Josef Koller
发明人： Alois Puntener , Gerhard Back , Josef Koller
IPC分类号： D06P1/642 , D06P1/673 , D06P3/32 , D06P5/00 , D06P5/10
CPC分类号： D06P5/10 , D06P1/6423 , D06P1/67341 , D06P3/32
摘要： For improving the light-fastness of leather dyed with anionic dyes, the leather is treated, before, during or after dyeing, with a compound of copper.
摘要翻译：为了提高用阴离子染料染色的皮革的耐光性，在染色之前，期间或之后用铜化合物处理皮革。

3. 发明授权

US5229502A Preparation of 1:2 chromium complexes one sulfo substituted and one sulfonamido or the like substituted azo dyes 失效
标题翻译： 1：2铬复合物的制备一个SULFO取代和一个磺酰胺或类似的替代AZO染色体
公开(公告)号：US5229502A
公开(公告)日：1993-07-20
申请号：US483144
申请日：1990-02-21
申请人： Gerhard Back , Alois Puntener
发明人： Gerhard Back , Alois Puntener
IPC分类号： C09B45/16 , C09B45/01 , C09B55/00 , D06P1/10 , D06P1/13
CPC分类号： C09B45/01 , C09B55/001
摘要： A process is described for the preparation of pure, asymmetric 1:2 chromium complex dyes containing at least two groups which impart solubility in water, which process comprises reacting a mixture of two dyes of the formulaeF.sub.1 --(SO.sub.3 H).sub.t (1)andF.sub.2 --SO.sub.2 --Y (2)in which the symbols are as defined in claim 1 with a chromium donor in a molar ratio of 0.85:1.0 to 1.2:1.0 in a one-pot process under pressure at a temperature above 100.degree. C. and at a pH between 0 and 2 and then continuing the reaction at a slightly acid, neutral or slightly alkaline pH. The dyes obtained by the process according to the invention are suitable for dyeing, in particular, wool, silk, leather and synthetic polyamide fibres.
摘要翻译：描述了制备含有至少两个赋予水溶解度的基团的纯不对称1：2铬络合物染料的方法，该方法包括使式F1-（SO3H）t（1）和 F2-SO2-Y（2），其中符号如权利要求1中所定义，其中铬供体的摩尔比为0.85:1.0至1.2:1.0，在一锅法中在高于100℃的压力下进行。并且在0和2之间的pH下，然后在稍微酸性，中性或微碱性pH下继续反应。通过本发明方法得到的染料适用于染色，特别是羊毛，丝绸，皮革和合成聚酰胺纤维。

4. 发明授权

US5001227A Fibre-reactive 1:1 chromium complex azo or azomethine dyes having a bidentate chelating group and a monofunctional neutral ligand 失效
公开(公告)号：US5001227A
公开(公告)日：1991-03-19
申请号：US669942
申请日：1984-11-09
申请人： Hans U. Schutz , Ulrich Schlesinger , Gerhard Back
发明人： Hans U. Schutz , Ulrich Schlesinger , Gerhard Back
IPC分类号： C09B62/012 , C09B62/095 , C09B62/255 , C09B62/477
CPC分类号： C09B62/477 , C09B62/095
摘要： The invention relates to chromium complexes of the formula ##STR1## in which L is H.sub.2 O, NH.sub.3, R.sub.2 --OH, R.sub.2 --NH.sub.2, (R.sub.2).sub.2 NH, (R.sub.2).sub.3 N or pyridine, wherein R.sub.2 is C.sub.1-6 -alkyl unsubstituted or substituted by halogen, C.sub.1-4 -alkoxy or amino, B is 8-hydroxyquinoline, 5-chloro-8-hydroxyquinoline, 5-hydroxyacridine, 6-hydroxy-4,7-phenanthroline, pyridine-2-carboxylic acid, 8-carboxyquinoline, 5,7-dibromo-8-hydroxyquinoline, o-hydroxyaniline, o-hydroxynaphthylamine, proline, glycine, serine, aspartic acid or R.sub.1 --CH(NH.sub.2)--COOH, wherein R.sub.1 is C.sub.1-6 -alkyl unsubstituted or substituted by halogen, C.sub.1-4 -alkoxy or amino, D is benzene or naphthalene, Y is the nitrogen atom or the CH group, K, in the event that Y is the nitrogen atom, is naphthol, naphthylamine, 5-pyrazolone, 5-aminopyrazole, 1-phenyl- or 1-naphthyl-5-aminopyrazole, 1-phenyl- or 1-naphthyl-5-pyrazolone, 2,6-dihydroxy-3-cyano- or -3-carboxamido-4-alkylpyridine, 6-hydroxypyrid-2-one, acetoacetanilide, benzoylacetanilide or phenol, or, in the event that Y is the CH group K is o-hydroxybenzaldehyde or o-hydroxynaphthaldehyde, D and K independently of each other are unsubstituted or substituted by C.sub.1-5 -alkyl, C.sub.1-4 -alkoxy, acylamino having 1 to 6 carbon atoms, benzoylamino, amino, monoalkylamino or dialkylamino each having 1 to 4 carbon atoms, phenylamino, alkoxycarbonyl having 1 to 4 carbon atoms in the alkoxy, radical, nitro, cyano, trifluoromethyl, halogen, sulfamoyl, carbamoyl, ureido, hydroxyl, C.sub.1-4 -alkylsulfonyl, carboxyl, sulfomethyl, phenylazo or naphthylazo, and D and K contain the --(CO).sub.0-1 --O-- and --[O or N(R)]-- adjacent to the --N.dbd.Y-- and R is hydrogen, C.sub.1-4 -alkyl or phenyl, Ka is a cation, X is acryloyl, monohalogenoacryloyl, dihalogenoacryloyl, trihalogenoacryloyl, monohalogenomethacryloyl, dihalogenomethacryloyl, trihalogenomethacryloyl, monohalogenopropionyl, dihalogenopropionyl, phenylsulfonylpropionyl, methylsulfonylpropionyl, vinylsulfonyl, .beta.-chloroethylsulfonyl, .beta.-sulfatoethylsulfonyl, monohalogenopyrimidyl, dihalogenopyrimidyl, trihalogenopyrimidyl, monohalogenotriazinyl, dihalogenotriazinyl, X is bonded to D, K or B, D and K, D and B or K and B directly or via ##STR2## or --CH.sub.2 --N(R)--, m is 1, 2 or 3 and n is 1 or 2. These chromium complexes are suitable for dyeing nitrogen-containing or hydroxy-containing materials and they produce level dyeings having good all-round fastness properties.

5. 发明授权

US4813972A Fiber-reactive chromium complexes and their preparation and use for polyamide, leather and cotton 失效
标题翻译：纤维反应性铬配合物及其制备和用于聚酰胺，皮革和棉花
公开(公告)号：US4813972A
公开(公告)日：1989-03-21
申请号：US105344
申请日：1987-10-07
申请人： Hans U. Schutz , Ulrich Schlesinger , Gerhard Back
发明人： Hans U. Schutz , Ulrich Schlesinger , Gerhard Back
IPC分类号： C09B62/44 , C09B62/002 , C09B62/012 , C09B62/04 , C09B62/095 , C09B62/20 , C09B62/255 , C09B62/465 , C09B62/477 , C09B62/503 , C09B62/515 , D06P1/382 , D06P1/384 , C09B62/01 , D06P1/38 , D06P3/10
CPC分类号： C09B62/477 , C09B62/012 , Y10S8/917 , Y10S8/918 , Y10S8/924
摘要： The invention relates to chromium complexes of the formula ##STR1## in which A is the radical of a dicyclically metallizable azo or azomethine dye, B is the radical of a potentially at least bidentate bianionic complexible organic compound which contains no azo or azomethine group, L is a colorless monofunctional ligand, X is a fibre-reactive radical, Ka is a cation, K is 0 or 1, m is 1, 2 or 3, n is 1 or 2, and the X radical and the SO.sub.3.sup..crclbar. Ka group are each bonded to the radicals A and B, to a process for preparing the chromium complexes of the formula (1), and to a combined preparation and dyeing process.
摘要翻译：本发明涉及式（1）的铬配合物，其中A是双环可金属化的偶氮或偶氮甲碱染料的基团，B是不含偶氮或偶氮甲碱的潜在至少二齿双键络合的有机化合物的基团基团，L是无色单官能配体，X是纤维反应性基团，Ka是阳离子，K是0或1，m是1,2或3，n是1或2，X基团和SO 3（ - ）Ka基团各自键合到基团A和B，与制备式（1）的铬络合物的方法以及组合的制备和染色方法。

6. 发明授权

US4990598A Fibre-reaction 1:1 chromium complex azo or azomethine dyes having a bidentate chelating group and a monofunctional neutral ligand 失效
标题翻译：纤维反应1：1铬复合偶氮或偶氮甲碱染料，具有双齿螯合基团和单官能中性配体
公开(公告)号：US4990598A
公开(公告)日：1991-02-05
申请号：US669214
申请日：1984-11-07
申请人： Hans U. Schutz , Ulrich Schlesinger , Gerhard Back
发明人： Hans U. Schutz , Ulrich Schlesinger , Gerhard Back
IPC分类号： C09B45/16 , C09B62/002 , C09B62/012 , C09B62/255 , C09B62/44 , C09B62/477 , D06P1/38 , D06P1/382 , D06P1/384
CPC分类号： C09B62/0025 , C09B62/012 , D06P1/38 , Y10S534/01
摘要： The invention relates to chromium complexes of the formula ##STR1## in which A is the radical of a dicyclically metallizable azo or azomethine dye, B is the radical of a monoanionic bidentate complexible organic compound which is bonded to the chromium atom via oxygen atoms, L is a colorless monofunctional ligand, X is halogen-substituted C.sub.1-4 -alkanoyl, C.sub.1-4 -alkenoyl, halogen-substituted C.sub.1-4 -alkenoyl, monohalogenopyrimidinyl, dihalogenopyrimidinyl or trihalogenopyrimidinyl which is bonded to A and/or B via ##STR2## and R.sub.5 is hydrogen or C.sub.1-4 -alkyl, Ka is a cation, m is 1, 2 or 3, n is 1 or 2 and the SO.sub.3.sup..crclbar. Ka group is bonded to A and/or B. These chromium complexes are suitable for dyeing nitrogen-containing or hydroxy-containing materials and they produce level dyeings having good all-round fastness properties.
摘要翻译：本发明涉及式为“IMAGE”的铬络合物，其中A为双链可偶氮偶氮或偶氮甲碱染料的基团，B为通过氧原子与铬原子键合的单阴离子二齿可络合有机化合物的基团，L 是无色单官能配体，X是卤素取代的C 1-4 - 烷酰基，C 1-4 - 烯酰基，卤素取代的C 1-4 - 烯酰基，一卤代嘧啶基，二卤代嘧啶基或三卤基嘧啶基，其通过键合到A和/或B上， R5为氢或C1-4烷基，Ka为阳离子，m为1,2或3，n为1或2，SO3（ - ）Ka基团与A和/或B键合。这些铬络合物为适用于含氮或含羟基材料的染色，并且它们产生具有良好全面牢固性能的水平染色。

7. 发明授权

US4678851A Metal dye complexes containing an azo or azomethine dye and a colorless ligand with the C.dbd.N--N.dbd.C group 失效
标题翻译：含有偶氮或偶氮甲碱染料的金属染料络合物和C = N-N = C基团的无色配位体
公开(公告)号：US4678851A
公开(公告)日：1987-07-07
申请号：US717743
申请日：1985-03-28
申请人： Gerhard Back , Hans U. Schutz , Ulrich Schlesinger
发明人： Gerhard Back , Hans U. Schutz , Ulrich Schlesinger
IPC分类号： C09B45/04 , C09B62/002 , C09B62/012 , C09B62/477 , C09B62/032 , C09B62/095
CPC分类号： C09B62/0025 , C09B62/012
摘要： Metal complex dyes that produce level, fast dyeings on textile materials are provided according to the formula ##STR1## wherein: D is a benzene, naphthalene or heterocyclic radical of a diazo component;Y is nitrogen or --CH;K is the radical of a coupling component if Y is nitrogen, or an o-hydroxyaldehyde radical if Y is --CH:Ka is a cation;Me is chromium or cobalt;Z.sub.1 is --O-- or --COO-- ortho to N.dbd.YZ.sub.2 is --O-- or --NR vicinal to N.dbd.Y, wherein R is hydrogen or substituted or unsubstituted C.sub.1 -C.sub.4 alkyl or phenyl;X is a fiber reactive radical bound directly to or through an amino or amino-containing group to the complex;R.sub.1 is a direct bond or substituted or unsubstituted C.sub.1 -C.sub.8 -alkyl, C.sub.1 -C.sub.8 -alkenyl, or aryl radical or heterocyclic radical containing 1 to 3 sulfur, oxygen or nitrogen atoms;R.sub.2 is hydrogen or substituted or unsubstituted C.sub.1 -C.sub.8 -alkyl or aryl;R.sub.3 is hydrogen or substituted or unsubstituted C.sub.1 -C.sub.8 alkyl, aryl or amino radical, or a heterocyclic radical containing 1 to 3 sulfur, oxygen or nitrogen atoms;V is a direct bond or oxygen;Q is oxygen or sulfur;w is 0 or 1;n is 0, 1, 2, 3 or 4, andp is 0, 1, 2with the proviso that the sum of n+p is at least 1.
摘要翻译：根据下式提供在纺织材料上产生水平，快速染色的金属络合染料，其中：D是重氮组分的苯，萘或杂环基; Y是氮或-CH; 如果Y是氮，K是偶联组分的基团，如果Y是-CH，则是羟基醛基团：Ka是阳离子; 我是铬或钴; Z 1是-O-或-COO-邻位于N = Y Z2是-O-或-NR邻近N = Y，其中R是氢或取代或未取代的C 1 -C 4烷基或苯基; X是与复合物直接或通过氨基或含氨基的基团键合的纤维反应性基团; R1是直接键或含有1至3个硫，氧或氮原子的取代或未取代的C 1 -C 8 - 烷基，C 1 -C 8 - 烯基或芳基或杂环基; R2是氢或取代或未取代的C1-C8-烷基或芳基; R 3是氢或取代或未取代的C 1 -C 8烷基，芳基或氨基，或含有1至3个硫，氧或氮原子的杂环基; V是直接键或氧; Q是氧或硫; w为0或1; n为0,1,2,3或4，p为0,1,2，条件是n + p的和为至少1。

8. 发明授权

US4723001A Fibre-reactive chromium complexes and their preparation and use 失效
标题翻译：纤维反应铬配合物及其制备与应用
公开(公告)号：US4723001A
公开(公告)日：1988-02-02
申请号：US888281
申请日：1986-07-24
申请人： Hans U. Schutz , Ulrich Schlesinger , Gerhard Back
发明人： Hans U. Schutz , Ulrich Schlesinger , Gerhard Back
IPC分类号： C09B62/44 , C09B62/002 , C09B62/012 , C09B62/04 , C09B62/095 , C09B62/20 , C09B62/255 , C09B62/465 , C09B62/477 , C09B62/503 , C09B62/515 , D06P1/382 , D06P1/384 , C09B62/675 , D06P1/38
CPC分类号： C09B62/477 , C09B62/012 , Y10S8/917 , Y10S8/918 , Y10S8/924
摘要： The invention relates to chromium complexes of the formula ##STR1## in which B is the radical of a bidentate bianionic compound, L is H.sub.2 O, NH.sub.3, alkanol, alkylamine, dialkylamine, trialkylamine or pyridine, D is a benzene or naphthalene diazo component, Y is the nitrogen atom or the CH group, K is a coupling component, R is hydrogen, alkyl or phenyl, X is a fibre-reactive group,Ka is a cation, m is 1, 2 or 3, n is 1 or 2 and k is 0 or 1.These chromium complexes are suitable for dyeing nitrogen-containing or hydroxy-containing materials and they produce level dyeings having good all-round fastness properties.
摘要翻译：本发明涉及式“IMAGE”的铬络合物，其中B是二齿双键化合物的基团，L是H 2 O，NH 3，链烷醇，烷基胺，二烷基胺，三烷基胺或吡啶，D是苯或萘重氮组分，Y 是氮原子或CH基团，K是偶合组分，R是氢，烷基或苯基，X是纤维反应性基团，Ka是阳离子，m是1,2或3，n是1或2， k为0或1.这些铬络合物适用于含氮或含羟基材料的染色，并且它们产生具有良好全面牢固性能的水平染色。

9. 发明授权

US4818248A Process for dyeing natural or synthetic polyamide fibre materials with 1:1 metal complex dyes in presence of alkali metal fluordsilicate or amindnlum silicate 失效
标题翻译：在碱金属氟硅酸盐或氨纶硅酸盐存在下用1：1金属络合物染料染色天然或合成聚酰胺纤维材料的方法
公开(公告)号：US4818248A
公开(公告)日：1989-04-04
申请号：US102942
申请日：1987-09-30
申请人： Gerhard Back , Walter Mosimann
发明人： Gerhard Back , Walter Mosimann
IPC分类号： D06P1/36 , D06P1/10 , D06P1/607 , D06P1/673 , D06P3/06 , D06P3/14 , D06P3/16 , D06P3/20 , D06P3/24 , C09B67/24
CPC分类号： D06P3/06 , D06P1/6076 , D06P1/6735 , D06P3/16 , D06P3/241 , Y10S8/917
摘要： The present invention relates to a process for dyeing natural or synthetic polyamide fibre material from an aqueous liquor with dyes, in the presence of an alkali metal salt or an ammonium salt and in the presence of an assistant, which process comprises dyeing said fibre material with at least one sulfonated 1:1 metal complex dye or with a mixture containing at least one sulfonated 1:1 metal complex dye and at least one sulfonated metal-free dye, in the presence of 10 to 45 percent by weight of an alkali fluorosilicate or ammonium fluorosilicate or a mixture thereof, based on the amount of the 1:1 metal complex dye employed, and in the presence of an assistant at a pH value of 3 to 5.The process of the invention is suitable for dyeing natural or synthetic polyamide materials to give non-skittery and level dyeings of good fastness properties.
摘要翻译：本发明涉及一种使用染料，在碱金属盐或铵盐存在下，在助剂的存在下从含水液体中染色天然或合成聚酰胺纤维材料的方法，该方法包括用所述纤维素材料至少一种磺化的1:1金属络合物染料或含有至少一种磺化的1:1金属络合物染料和至少一种磺化金属的染料的混合物，在10至45重量％的氟硅酸盐存在下，或基于所使用的1:1金属络合物染料的量，以及在pH值为3至5的助剂存在下，氟硅酸铵或其混合物。本发明的方法适用于染色天然或合成聚酰胺材料赋予无纺布和水平染色牢度好的坚牢度。

10. 发明授权

US4680385A Metal dye complexes containing an azo or azomethine dye and a colorless ligand with the C.dbd.N--N.dbd.C group 失效
标题翻译：含有偶氮或偶氮甲碱染料的金属染料络合物和C = N-N = C基团的无色配位体
公开(公告)号：US4680385A
公开(公告)日：1987-07-14
申请号：US717733
申请日：1985-03-28
申请人： Gerhard Back
发明人： Gerhard Back
IPC分类号： C09B45/14 , C09B45/16 , C09B45/20 , C09B55/00 , C09B45/06 , D06P1/10 , D06P3/24
CPC分类号： C09B45/20 , C09B45/16 , C09B55/00
摘要： Metal complex dyes that produce level, fast dyeings on textile materials are provided according to the formula ##STR1## wherein: D is a benzene, naphthalene or heterocyclic radical of a diazo component;Y is nitrogen or --CH;K is the radical of a coupling component if Y is nitrogen, or an o-hydroxyaldehyde radical if Y is --CH;Ka is a cation;Me is chromium or cobalt;Z.sub.1 is --O-- or --COO-- ortho to N.dbd.YZ.sub.2 is --O-- or --NR vicinal to N.dbd.Y, wherein R is hydrogen or a C.sub.1 -C.sub.4 alkyl or phenyl radical;R.sub.1 is a direct bond or a C.sub.1 -C.sub.8 -alkyl, C.sub.1 -C.sub.8 -alkenyl, or aryl radical or heterocyclic radial containing 1 to 3 sulfur, oxygen or nitrogen atoms;R.sub.2 is hydrogen or C.sub.1 -C.sub.8 -alkyl or aryl radical;R.sub.3 is hydrogen or a C.sub.1 -C.sub.8 alkyl, aryl or amino radical, or a heterocyclic radical containing 1 to 3 sulfur, oxygen or nitrogen atoms;V is a direct bond or oxygen;Q is oxygen or sulfur; andw is 0 or 1.
摘要翻译：根据下式提供在纺织材料上产生水平，快速染色的金属络合染料，其中：D是重氮组分的苯，萘或杂环基; Y是氮或-CH; 如果Y是氮，K是偶联组分的基团，如果Y是-CH，则是邻羟基醛基; 嘉是阳离子; 我是铬或钴; Z 1是-O-或-COO-邻，N = Y Z2是-O-或-NR邻近于N = Y，其中R是氢或C1-C4烷基或苯基; R1是直接键或C1-C8-烷基，C1-C8-烯基或芳基或含有1至3个硫，氧或氮原子的杂环; R2是氢或C1-C8-烷基或芳基; R 3是氢或C 1 -C 8烷基，芳基或氨基，或含有1至3个硫，氧或氮原子的杂环基; V是直接键或氧; Q是氧或硫; w为0或1。

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