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1. 发明授权

US08163114B2 Netshape manufacturing processes and compositions 有权
标题翻译： Netshape制造工艺和成分
公开(公告)号：US08163114B2
公开(公告)日：2012-04-24
申请号：US10819898
申请日：2004-04-07
申请人： Costas Gogos , Ming-Wan Young , Rajesh Dave , Robert Pfeffer , David Todd , Bainian Qian , Theodore Davidson
发明人： Costas Gogos , Ming-Wan Young , Rajesh Dave , Robert Pfeffer , David Todd , Bainian Qian , Theodore Davidson
IPC分类号： D03D23/00
CPC分类号： C08J3/20 , C06B21/0025 , C06B21/0083 , C06B45/02
摘要： Techniques and processes that combine particulate coating processes with particulate handling steps resulting in the formation of free-flowing particulates for introduction into energetic product vessels to affect an in-situ, net-shape manufactured product. The processes involve selecting suitably sized materials, processing such materials such that they are surface-coated and/or locally “structured” particulates, and pouring, preferably “dry” pouring, these processed materials into an energetic product vessel and infusing the filled vessel with a polymerizable and surface-compatible monomer or oligomer which flows into the unoccupied volume, followed by polymerization of the monomer, which then becomes the binder giving mechanical integrity to the final, net-shape energetic composition.
摘要翻译：将颗粒涂层工艺与颗粒处理步骤相结合的技术和工艺，导致形成自由流动的颗粒，以引入高能产品容器中，以影响原位的网状制造产品。这些方法包括选择适当尺寸的材料，加工这些材料使得它们被表面涂覆和/或局部“结构化”的颗粒，并将这些加工的材料倾倒，优选地“干”地浇注到高能产品容器中并将填充的容器注入流动到未占据体积的可聚合和表面相容的单体或低聚物，随后聚合单体，然后其变成粘合剂，给最终的网状能量组合物提供机械完整性。

2. 发明申请

US20050228075A1 Ordered particle structures and methods of making same 审中-公开
标题翻译：有序粒子结构及其制作方法
公开(公告)号：US20050228075A1
公开(公告)日：2005-10-13
申请号：US10878656
申请日：2004-06-28
申请人： Costas Gogos , Ming-Wan Young , Rajesh Dave , Robert Pfeffer , Theodore Davidson , David Todd , Bainian Qian , Jun Yang
发明人： Costas Gogos , Ming-Wan Young , Rajesh Dave , Robert Pfeffer , Theodore Davidson , David Todd , Bainian Qian , Jun Yang
IPC分类号： C06B21/00 , C06B45/02 , C08J3/20 , C08K7/00 , C10L5/00 , D03D23/00
CPC分类号： C08J3/20 , C06B21/0025 , C06B21/0083 , C06B45/02
摘要： Techniques and methods of formation of ordered mixtures of particles by “clustering”. Clustering comprises local “structuring” consisting of a large “host” and smaller “guest” particles by various techniques. Small amounts of polymer are coated onto solid particles by various means. In one embodiment, an ordered mixture is created wherein the material that is of lesser quantity is of small particle size (the “B” particles) and the “A” particles are of larger size. The “B” particles are then coated onto a single A particle. By creating this ordered structure, each composite particle has the proper or stoichiometric amount of all ingredients. This dry composite material produced is appropriately used in various applications such as pharmaceutical formulations in the form of tablets, capsules, oral suspensions, inhalant, parenteral formulations and the like; energetics manufacture such as but not limited to explosives, propellants and pyrotechnics; agricultural products including but not limited to fertilizers, herbicides and pesticides; nutritional supplements and the like.
摘要翻译：通过“聚类”形成有序粒子混合物的技术和方法。聚类包括通过各种技术由大型“主机”和较小的“客体”粒子组成的本地“结构化”。少量聚合物通过各种方式涂覆在固体颗粒上。在一个实施方案中，产生有序混合物，其中少量的材料具有较小的粒度（“B”颗粒）和“A”颗粒的尺寸较大。然后将“B”颗粒涂覆到单个A颗粒上。通过创建这种有序结构，每个复合颗粒具有适当或化学计量的所有成分。生产的这种干燥复合材料适用于各种应用，例如片剂，胶囊，口服悬浮液，吸入剂，肠胃外制剂等药物制剂; 能源制造，例如但不限于爆炸物，推进剂和烟火; 农产品包括但不限于化肥，除草剂和农药; 营养补品等。

3. 发明申请

US20050224148A1 Netshape manufacturing processes and compositions 有权
标题翻译： Netshape制造工艺和成分
公开(公告)号：US20050224148A1
公开(公告)日：2005-10-13
申请号：US10819898
申请日：2004-04-07
申请人： Costas Gogos , Ming-Wan Young , Rajesh Dave , Robert Pfeffer , David Todd , Bainian Qian , Theodore Davidson
发明人： Costas Gogos , Ming-Wan Young , Rajesh Dave , Robert Pfeffer , David Todd , Bainian Qian , Theodore Davidson
IPC分类号： C06B21/00 , C06B45/02 , C08J3/20 , C08K7/00 , C10L5/00 , D03D23/00
CPC分类号： C08J3/20 , C06B21/0025 , C06B21/0083 , C06B45/02
摘要： Techniques and processes that combine particulate coating processes with particulate handling steps resulting in the formation of free-flowing particulates for introduction into energetic product vessels to affect an in-situ, net-shape manufactured product. The processes involve selecting suitably sized materials, processing such materials such that they are surface-coated and/or locally “structured” particulates, and pouring, preferably “dry” pouring, these processed materials into an energetic product vessel and infusing the filled vessel with a polymerizable and surface-compatible monomer or oligomer which flows into the unoccupied volume, followed by polymerization of the monomer, which then becomes the binder giving mechanical integrity to the final, net-shape energetic composition.
摘要翻译：将颗粒涂层工艺与颗粒处理步骤相结合的技术和工艺，导致形成自由流动的颗粒，以引入高能产品容器中，以影响原位的网状制造产品。这些方法包括选择适当尺寸的材料，加工这些材料使得它们被表面涂覆和/或局部“结构化”的颗粒，并将这些加工的材料倾倒，优选地“干”地浇注到高能产品容器中并将填充的容器注入流动到未占据体积的可聚合和表面相容的单体或低聚物，然后聚合单体，然后其变成粘合剂，赋予最终的网状能量组合物机械完整性。

4. 发明申请

US20050217572A1 Ultraviolet particle coating systems and processes 审中-公开
标题翻译：紫外线粒子涂层系统和工艺
公开(公告)号：US20050217572A1
公开(公告)日：2005-10-06
申请号：US11094842
申请日：2005-03-30
申请人： Ming-Wan Young , Bainian Qian , Costas Gogos , Rajesh Dave , Linjie Zhu
发明人： Ming-Wan Young , Bainian Qian , Costas Gogos , Rajesh Dave , Linjie Zhu
IPC分类号： B01J2/00 , B05C5/00 , B05D1/00 , B05D1/22 , B05D3/06 , C08J3/28
CPC分类号： C08J3/28 , B01J2/006 , B05D1/005 , B05D1/22 , B05D3/067
摘要： Particle coating processes and systems employ UV curable materials to form tack-free surfaces rapidly. By applying UV curable compositions on well suspended particles a UV particle coating technology enables a scalable process of coating fine particles at desirable coating thicknesses with a wide spectrum of obtainable properties. Processes in accordance with the present invention decouple the particle suspension and film formation steps, enabling ample time to first deliver evenly the coating materials to the particle surfaces, followed by rapid polymerization/curing reaction induced by the UV light to rapidly create tack-free surfaces, thus preventing particles agglomeration while achieving uniform and thin-layer coating.
摘要翻译：颗粒涂层工艺和系统采用紫外光固化材料快速形成无粘结表面。通过将UV可固化组合物应用于良好悬浮的颗粒上，紫外线颗粒涂层技术使得能够以可获得的广谱性能涂覆所需涂层厚度的细颗粒的可伸缩工艺。根据本发明的方法使颗粒悬浮液和成膜步骤解耦，从而有足够的时间首先将涂料均匀地输送到颗粒表面，随后由UV光诱导的快速聚合/固化反应，以快速产生无粘性表面，从而防止颗粒聚集同时实现均匀和薄层涂层。

5. 发明授权

US08252370B1 Continuous high-speed coating of finely ground particulates 有权
标题翻译：连续高速涂覆精细粉碎的颗粒
公开(公告)号：US08252370B1
公开(公告)日：2012-08-28
申请号：US11457501
申请日：2006-07-14
申请人： Ming-Wan Young , Costas George Gogos , Jun Yang , Rajesh Dave , Linje Zhu , Peter Bonnett , William Schepige
发明人： Ming-Wan Young , Costas George Gogos , Jun Yang , Rajesh Dave , Linje Zhu , Peter Bonnett , William Schepige
IPC分类号： B05D1/24
CPC分类号： B01J2/006 , Y10T428/2991 , Y10T428/2998
摘要： A method for the continuous production of finely ground particulates coated with a barrier, or other desirable film wherein the coated particulates exhibit a diameter of less than 10 microns. In an exemplary embodiment, large coated particulates are introduced into a fluid energy, or jet mill, along with smaller, uncoated particulates. As the particulates collide within the mill they are comminuted, and an amount of coating is transferred from the coated particulates to the uncoated ones such that they become sufficiently coated and size-reduced to a desired size. Alternatively, uncoated particulates are milled and coated during their milling. Still alternatively, uncoated particulates are milled and subsequently directed through an atomized mist of coating material wherein the size of the mist droplets are as large, or larger than the directed particulates.
摘要翻译：用于连续生产涂覆有阻挡层的精细研磨的颗粒的方法或其它所需的膜，其中涂覆的微粒表现出小于10微米的直径。在一个示例性实施例中，将大的涂覆颗粒与较小的未涂覆的颗粒一起引入流体能量或喷射式粉碎机。当颗粒在磨机内碰撞时，它们被粉碎，并且一定量的涂层从涂覆的颗粒转移到未涂覆的颗粒，使得它们变得充分地涂覆并且尺寸减小到所需的尺寸。或者，未研磨的颗粒在其研磨期间被研磨和涂覆。或者，未涂覆的颗粒被研磨并随后引导通过涂料的雾化雾，其中雾滴的尺寸大于或大于定向颗粒。

6. 发明授权

US07537803B2 Polymer coating/encapsulation of nanoparticles using a supercritical antisolvent process 有权
标题翻译：使用超临界反溶剂法制备纳米颗粒的聚合物涂层/包封
公开(公告)号：US07537803B2
公开(公告)日：2009-05-26
申请号：US10820091
申请日：2004-04-07
申请人： Yulu Wang , Robert Pfeffer , Rajesh Dave
发明人： Yulu Wang , Robert Pfeffer , Rajesh Dave
IPC分类号： B05D7/00 , C08J7/16 , B01J19/10 , B29B9/08
CPC分类号： A61K9/5153 , A61K9/5031 , A61K9/5089 , A61K9/5192 , B01J2/006 , C08J3/212 , C08K9/08 , C09D7/40 , C09D11/52 , Y02P20/544 , Y10T428/25 , Y10T428/2998
摘要： A process, method and/or system for preparing polymer-coated nanoparticles and/or other ultrafine particles utilizing a supercritical fluid, e.g., supercritical carbon dioxide (SC CO2), as an antisolvent that may be added to a solution of a polymer and an organic solvent in which insoluble nanoparticles or the like are suspended. The coating process occurs when the supercritical fluid (e.g., SC CO2) and the nanoparticle-containing suspension are combined to cause the suspended nanoparticles to precipitate as coated nanoparticles. Processing parameters for optimizing and/or enhancing the efficacy and/or efficiency of the coating process, method and/or system and for controlling the coating and/or agglomeration of coated particles are also described. The process, method and/or system has wide ranging applicability, e.g., for coating and/or encapsulation of pharmaceuticals, cosmetics, food products, chemicals, agrochemicals, pesticides, polymers, coatings, catalysts and the like.
摘要翻译：使用超临界流体（例如超临界二氧化碳（SCCO 2））制备聚合物涂覆的纳米颗粒和/或其它超微粒子的方法，方法和/或系统作为可以加入到聚合物溶液中的抗溶剂其中悬浮有不溶性纳米颗粒等的有机溶剂。当超临界流体（例如SCCO 2）和含纳米颗粒的悬浮液组合以引起悬浮的纳米颗粒作为包覆的纳米颗粒沉淀时，发生涂覆过程。还描述了用于优化和/或增强涂覆工艺，方法和/或系统的功效和/或效率以及用于控制涂覆颗粒的涂覆和/或附聚的加工参数。方法，方法和/或系统具有广泛的适用性，例如用于药物，化妆品，食品，化学品，农业化学品，农药，聚合物，涂料，催化剂等的涂覆和/或包封。

7. 发明申请

US20070108320A1 System and method for nanoparticle and nanoagglomerate fluidization 失效
标题翻译：纳米颗粒和纳米颗粒流化的系统和方法
公开(公告)号：US20070108320A1
公开(公告)日：2007-05-17
申请号：US11605176
申请日：2006-11-28
申请人： Robert Pfeffer , Caroline Nam , Rajesh Dave , Guangliang Liu , Jose Quevedo , Qun Yu , Chao Zhu
发明人： Robert Pfeffer , Caroline Nam , Rajesh Dave , Guangliang Liu , Jose Quevedo , Qun Yu , Chao Zhu
IPC分类号： B02C19/06
CPC分类号： B01F13/0809 , B01F11/0266 , B01F13/0255 , B01J8/1872 , B01J8/40 , B01J8/42 , B01J19/10 , B01J2208/00681 , B82Y15/00
摘要： With the coupling of an external field and aeration (or a flow of another gas), nanoparticles can be smoothly and vigorously fluidized. A magnetic force and/or pre-treatment may be employed with the fluidizing gas and, when coupled with a fluidizing medium, provide excellent means for achieving homogenous nanofluidization. The magnetic force interacts with non-fluidizing magnetic particles and helps to break channels as well as provide enough energy to disrupt the strong interparticle forces, thereby establishing an advantageous agglomerate size distribution. Enhanced fluidization is reflected by improved performance-related attributes. The fluidized nanoparticles may be coated, surface-treated and/or surface-modified in the fluidized state. In addition, the fluidized nanoparticles may participate in a reaction, either as a reactant or a catalyst, while in the fluidized state.
摘要翻译：通过外场和通气（或另一种气体的流动）的耦合，纳米颗粒可以顺利且剧烈流化。可以与流化气体一起使用磁力和/或预处理，并且当与流化介质结合时，提供用于实现均匀纳米流化的优异手段。磁力与非流动性磁性颗粒相互作用，有助于破坏通道，并提供足够的能量来破坏强大的颗粒间力，从而建立有利的聚集体尺寸分布。改进的流量化反映在与性能相关的特性方面。流化的纳米颗粒可以在流化状态下被涂覆，表面处理和/或表面改性。此外，流化的纳米颗粒可以在流化状态下作为反应物或催化剂参与反应。

8. 发明申请

US20070120281A1 Manufacture of fine particles and nano particles and coating thereof 审中-公开
标题翻译：制造细颗粒和纳米颗粒及其涂层
公开(公告)号：US20070120281A1
公开(公告)日：2007-05-31
申请号：US11594411
申请日：2006-11-08
申请人： Boris Khusid , Abhijit Gokhale , Rajesh Dave , Robert Pfeffer
发明人： Boris Khusid , Abhijit Gokhale , Rajesh Dave , Robert Pfeffer
IPC分类号： B29B9/00
CPC分类号： B01J2/04 , B01J2/006 , B01J3/008
摘要： An anti-solvent fluid technique is provided that assists in the formation, production and manufacture of fine particles including micro-sized and nanometer-sized particles for a wide variety of bio-medical and pharmaceutical applications. This technique is particularly effective for the manufacturing of polymers/biopolymers/drugs of micron, submicron or nano size as well as particle coating/encapsulation. Co-solvents are used to dissolve the polymer or mixture of polymers to make a solution. The method facilitates rapid drying of precipitated particles with reduced size and agglomerations. The method includes: (1) providing: an anti-solvent fluid; both organic solvents are soluble in the anti-solvent fluid; a second solvent that is at least partially soluble in or miscible with the first solvent; and a solute that is soluble in the first solvent and is substantially insoluble in the second solvent and the anti-solvent fluid; (2) capillary nozzle(s) are used to inject the solution into anti-solvent; (3) contacting the first solvent, the second solvent and the solute together to form a solution; (4) contacting the solution with the anti-solvent fluid to extract both solvents from the solution and precipitate the solute in the form of particles; and (5) contacting the solution with the anti-solvent fluids to extract both solvents from solution and precipitate the solute(s).
摘要翻译：提供了一种抗溶剂流体技术，其有助于形成，生产和制造包括用于各种生物医学和药物应用的微尺寸和纳米尺寸颗粒的细颗粒。该技术对于制备微米，亚微米或纳米尺寸以及颗粒涂层/包封的聚合物/生物聚合物/药物是特别有效的。共溶剂用于溶解聚合物或聚合物混合物以制成溶液。该方法有助于快速干燥具有减小的尺寸和聚集的沉淀颗粒。该方法包括：（1）提供：反溶剂流体; 两种有机溶剂均溶于反溶剂液体; 至少部分可溶于第一溶剂或与第一溶剂混溶的第二溶剂; 以及可溶于第一溶剂且基本上不溶于第二溶剂和反溶剂流体的溶质; （2）毛细喷嘴用于将溶液注入反溶剂中; （3）将第一溶剂，第二溶剂和溶质接触在一起形成溶液; （4）使溶液与反溶剂流体接触，从溶液中提取两种溶剂，并以颗粒形式沉淀溶质; 和（5）使溶液与反溶剂流体接触以从溶液中萃取两种溶剂并沉淀溶质。

9. 发明授权

US07645327B2 Fractal structured nanoagglomerates as filter media 失效
标题翻译：分形结构纳米粒子作为过滤介质
公开(公告)号：US07645327B2
公开(公告)日：2010-01-12
申请号：US11416034
申请日：2006-05-02
申请人： Robert Pfeffer , Rajesh Dave , Stanislav Dukhin , Jose A. Quevedo , Qun Yu
发明人： Robert Pfeffer , Rajesh Dave , Stanislav Dukhin , Jose A. Quevedo , Qun Yu
IPC分类号： B01D29/02
CPC分类号： B01D46/30 , B01D39/04 , B01D46/003 , B01D2239/0258 , B01D2279/51 , Y10S977/773 , Y10S977/775 , Y10S977/776 , Y10S977/777 , Y10S977/778
摘要： Systems and methods for achieving filtration are provided that utilize agglomerates or granules of nanoparticles. The agglomerates or granules of nanoparticles may be used as and/or incorporated into a HEPA filtration system to remove solid or liquid submicron-sized particles, e.g., MPPS, in an efficient and efficacious manner. The filtration systems and methods are provided that utilize agglomerates or granules in a size range of about 100-500 microns. The agglomerates or granules of nanoparticles exhibit a hierarchical fractal structure. In the case of agglomerates of nanoparticles, porosities of 0.9 or greater are generally employed, and for granules of nanoparticles, porosities that are smaller than 0.9 may be employed. Filter media formed from the agglomerates or granules may be formed from materials such as carbon black and fumed silica, and may be employed in baffled or non-baffled filtration apparatus.
摘要翻译：提供用于实现过滤的系统和方法，其利用纳米颗粒的附聚物或颗粒。纳米颗粒的附聚物或颗粒可以用作和/或并入HEPA过滤系统中以有效和有效的方式除去固体或液体亚微米尺寸的颗粒，例如MPPS。提供了使用约100-500微米尺寸范围内的附聚物或颗粒的过滤系统和方法。纳米颗粒的团聚体或颗粒呈现分层结构。在纳米颗粒附聚物的情况下，通常使用0.9或更大的孔隙率，并且对于纳米颗粒的颗粒，可以使用小于0.9的孔隙率。由附聚物或颗粒形成的过滤介质可以由诸如炭黑和煅制二氧化硅的材料形成，并且可以用于挡板或非挡板过滤装置中。

10. 发明申请

US20090293719A1 FRACTAL STRUCTURED NANOAGGLOMERATES AS FILTER MEDIA 失效
标题翻译：分解结构纳米粒子作为过滤介质
公开(公告)号：US20090293719A1
公开(公告)日：2009-12-03
申请号：US11416034
申请日：2006-05-02
申请人： Robert Pfeffer , Rajesh Dave , Stanislav Dukhin , Jose A. Quevedo , Qun Yu
发明人： Robert Pfeffer , Rajesh Dave , Stanislav Dukhin , Jose A. Quevedo , Qun Yu
IPC分类号： B01D53/02 , B01D46/30 , B01D45/08 , B01D29/58 , B01D50/00
CPC分类号： B01D46/30 , B01D39/04 , B01D46/003 , B01D2239/0258 , B01D2279/51 , Y10S977/773 , Y10S977/775 , Y10S977/776 , Y10S977/777 , Y10S977/778
摘要： Systems and methods for achieving filtration are provided that utilize agglomerates or granules of nanoparticles. The agglomerates or granules of nanoparticles may be used as and/or incorporated into a HEPA filtration system to remove solid or liquid submicron-sized particles, e.g., MPPS, in an efficient and efficacious manner. The filtration systems and methods are provided that utilize agglomerates or granules in a size range of about 100-500 microns. The agglomerates or granules of nanoparticles exhibit a hierarchical fractal structure. In the case of agglomerates of nanoparticles, porosities of 0.9 or greater are generally employed, and for granules of nanoparticles, porosities that are smaller than 0.9 may be employed. Filter media formed from the agglomerates or granules may be formed from materials such as carbon black and fumed silica, and may be employed in baffled or non-baffled filtration apparatus.
摘要翻译：提供用于实现过滤的系统和方法，其利用纳米颗粒的附聚物或颗粒。纳米颗粒的附聚物或颗粒可以用作和/或并入HEPA过滤系统中以有效和有效的方式除去固体或液体亚微米尺寸的颗粒，例如MPPS。提供了使用约100-500微米尺寸范围内的附聚物或颗粒的过滤系统和方法。纳米颗粒的团聚体或颗粒呈现分层结构。在纳米颗粒附聚物的情况下，通常使用0.9或更大的孔隙率，并且对于纳米颗粒的颗粒，可以使用小于0.9的孔隙率。由附聚物或颗粒形成的过滤介质可以由诸如炭黑和煅制二氧化硅的材料形成，并且可以用于挡板或非挡板过滤装置中。

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