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1. 发明授权

US5484458A Triphendioxazine compounds, processes for their preparation and their use as dyestuffs 失效
标题翻译：三苯并二恶嗪化合物，其制备方法及其作为染料的用途
公开(公告)号：US5484458A
公开(公告)日：1996-01-16
申请号：US243111
申请日：1994-05-16
申请人： Werner H. Russ , Horst Tappe , Christian Schumacher
发明人： Werner H. Russ , Horst Tappe , Christian Schumacher
IPC分类号： C07C317/28 , C09B62/44 , C09B62/503 , C09B67/22 , D06P3/24 , D06P3/66 , C09B62/002 , D06P1/38
CPC分类号： C09B62/503 , C07C317/28 , C09B62/4403 , C09B67/0033 , Y10S8/917 , Y10S8/918 , Y10S8/924
摘要： Triphendioxazine compounds corresponding to the formula ##STR1## which are suitable as fiber-reactive dyestuffs for dyeing and printing material, in particular fiber material, containing hydroxy and/or carboxamide groups, such as wool and synthetic polyamide fibers, and especially cellulose fibers, such as cotton, are described. In formula (1), M is hydrogen or an alkali metal and Z is a radical of the formula (2) ##STR2## in which R is hydrogen, sulfo, alkyl having 1 to 4 carbon atoms, alkoxy having 1 to 4 carbon atoms, nitro or cyano, W is alkylene having 3 to 6 carbon atoms and the group --SO.sub.2 --Y is a fiber-reactive group of the vinyl sulfone series.
摘要翻译：对应于式（1）的三苯并二恶嗪化合物适合用作染色和印刷材料的纤维反应性染料，特别是含有羟基和/或羧酰胺基团的纤维材料，例如羊毛和合成聚酰胺纤维，特别是纤维素描述了诸如棉花之类的纤维。在式（1）中，M是氢或碱金属，Z是式（2）的基团，其中R是氢，磺基，具有1至4个碳原子的烷基，具有1至 4个碳原子，硝基或氰基，W是具有3至6个碳原子的亚烷基，基团-SO 2 -Y是乙烯基砜系列的纤维反应性基团。

2. 发明授权

US4857070A 2,4-Diaminophenyl tetrahydrofurfuryl ethers, processes for their preparation and tinting compositions, which contain them for keratinic fibres 失效
标题翻译： 2,4-二氨基苯基四氢糠醚，它们的制备方法和着色组合物，其含有角蛋白纤维
公开(公告)号：US4857070A
公开(公告)日：1989-08-15
申请号：US154495
申请日：1988-02-08
申请人： Winfried Seidel , Horst Tappe
发明人： Winfried Seidel , Horst Tappe
IPC分类号： A61K8/00 , A61K8/49 , A61Q5/10 , C07D307/12 , C09B53/00 , D06P1/32 , D06P3/08
CPC分类号： D06P1/32 , A61K8/4973 , A61Q5/10 , C07D307/12
摘要： The invention relates to new 2,4-diaminophenyl tetrahydrofurfuryl ethers of the general formula VIII and to their salts with inorganic or organic acids ##STR1## in which R.sub.1, R.sub.2, R.sub.3 and R.sub.4, independently of one another, each represent a hydrogen atom, a (C.sub.1 -C.sub.4)alkyl group, hydroxy(C.sub.2 -C.sub.4)alkyl group, dihydroxy(C.sub.3 -C.sub.4)alkyl group, halogeno(C.sub.2 -C.sub.4)alkyl group, amino(C.sub.2 -C.sub.4)alkyl group or an amino(C.sub.2 -C.sub.4)alkyl group which is substituted once or twice by methyl, ethyl or hydroxyethyl radicals on the nitrogen, the carbon chain having a straight or branched arrangement, and it being a proviso that at least one of R.sub.1, R.sub.2, R.sub.3 and R.sub.4 represents a hydrogen atom, to processes for their preparation, and to aqueous tinting compositions for keratin fibres such as fur and human hair, containing at least one coupler and at least one developing component together with customary additives and auxiliaries, the coupler corresponding to the general formula VIII or to the acid salts of these compounds.
摘要翻译：本发明涉及通式VIII的新的2,4-二氨基苯基四氢糠基醚及其与无机或有机酸（VIII）的盐，其中R 1，R 2，R 3和R 4彼此独立地表示氢原子，（C1-C4）烷基，羟基（C2-C4）烷基，二羟基（C3-C4）烷基，卤代（C2-C4）烷基，氨基（C2-C4）烷基或氨基（C 2 -C 4）烷基，其被氮上的甲基，乙基或羟乙基取代一次或两次，所述碳链具有直链或支链排列，条件是R1，R2，R3和 R4代表氢原子，其制备方法，以及含有至少一种偶联剂和至少一种显影组分以及常规添加剂和助剂的角蛋白纤维如毛皮和人发的水性着色组合物，所述成色剂对应于通式VIII或这些化合物的酸式盐。

3. 发明授权

US4567252A Water-insoluble naphthol monoazo dyestuff 失效
标题翻译：水不溶性萘酚单偶氮染料
公开(公告)号：US4567252A
公开(公告)日：1986-01-28
申请号：US492240
申请日：1983-05-06
申请人： Ulrich Buhler , Horst Tappe , Albert Bode , Manfred Hahnke , Kurt Roth
发明人： Ulrich Buhler , Horst Tappe , Albert Bode , Manfred Hahnke , Kurt Roth
IPC分类号： C09B29/01 , C09B29/15 , C09B29/02 , C09B29/34 , D06P3/24 , D06P3/52
CPC分类号： C09B29/0003 , C09B29/103 , Y10S534/02
摘要： Azo dyestuff of the formula ##STR1## wherein X is secondary amino or tertiary amino moiety, useful for dyeing and printing hydrophobic fiber materials to produce a deep orange color having excellent fastness properties and also useful for coloring organic solvents, mineral oil products, waxes, plastics and surface coatings.
摘要翻译：其中X是仲氨基或叔氨基部分的偶氮染料，其可用于染色和印刷疏水纤维材料以产生具有优异坚牢性的深橙色，并且还可用于着色有机溶剂，矿物油产品，蜡，塑料和表面涂层。

4. 发明授权

US4306874A Process for printing synthetic, hydrophobic fiber material in accordance with the principle of transfer printing 失效
标题翻译：印刷合成疏水纤维材料的方法按照转印原理
公开(公告)号：US4306874A
公开(公告)日：1981-12-22
申请号：US174732
申请日：1980-08-01
申请人： Horst Tappe , Claus Schuster
发明人： Horst Tappe , Claus Schuster
IPC分类号： C09B29/10 , C09B29/42 , D06P1/02 , D06P5/28 , D06P5/13 , D06P3/82
CPC分类号： D06P5/006 , C09B29/363 , Y10S8/918 , Y10S8/922
摘要： A sublimable monoazo dyestuff of the formula ##STR1## wherein X is alkyl of 1-4 carbon atoms is used as the dyestuff in the process for printing synthetic, hydrophobic materials, treated cellulose materials or materials containing both by transfer printing using formulations containing said sublimable monoazo dyestuff.
摘要翻译：在印刷合成，疏水材料，经处理的纤维素材料或含有两者的材料的过程中，将具有1-4个碳原子的烷基的升华性单偶氮染料用作染料，其中使用含有所述可升华的制剂单偶氮染料

5. 发明授权

US4265629A Process for the production of resist effects on polyester/cellulose mixed fiber textiles 失效
标题翻译：生产聚酯/纤维素混纺纤维织物的抗皱效果的方法
公开(公告)号：US4265629A
公开(公告)日：1981-05-05
申请号：US105204
申请日：1979-12-19
申请人： Joachim Ribka , Horst Tappe , Kurt Roth , Hans-Jurgen Weyer
发明人： Joachim Ribka , Horst Tappe , Kurt Roth , Hans-Jurgen Weyer
IPC分类号： D06P5/12 , D06P5/15
CPC分类号： D06P5/15 , D06P5/12
摘要： In the process for production of resist effects on textile materials of mixed fibers of polyester and cellulose comprising impregnating the materials with a dye liquor containing disperse dyestuffs and reactive dyestuffs which react with the resisting agents, drying or partially drying the padded materials and subsequently printing a resist paste on the material, and heat-treating the materials the improvement comprises the dischargeable disperse dyestuffs being of a class of dyestuffs of which an exemplary species is ##STR1## one of the tautomeric forms of a class of dyestuffs of which an exemplary species is ##STR2## or disperse dyestuffs which are free from groups conferring solubility in water and which contain at least two carboxylic acid ester moieties.
摘要翻译：在对聚酯和纤维素的混合纤维的纺织材料的抗蚀剂效果的生产过程中，包括用含有分散染料的染液和与抗蚀剂反应的活性染料浸渍材料，干燥或部分干燥填充材料并随后印刷在材料上抵抗糊料，并且对材料进行热处理，改进包括可排放的分散染料是一类染料，其示例性物质是一类染料的互变异构体之一，其示例性物质是或分散不含赋予在水中溶解度且含有至少两个羧酸酯部分的基团的染料。

6. 发明授权

US4157446A 3-Formyl-pyridines and process for making them 失效
标题翻译： 3-甲酰基吡啶类及其制备方法
公开(公告)号：US4157446A
公开(公告)日：1979-06-05
申请号：US819756
申请日：1977-07-29
申请人： Horst Tappe
发明人： Horst Tappe
IPC分类号： C07D213/69 , C07D213/71 , C07D213/76
CPC分类号： C07D213/69 , C07D213/71
摘要： A .beta.,.beta.,.beta.-trihalo-.alpha.-hydroxyethyl (e.g. --CHOH--CCl.sub.3) group is introduced into a 2,6-dihydroxy pyridine. The 3-formyl-4-methyl-2,6-dihydroxy pyridine produced by splitting off haloform from the trihalohydroxyethyl product, is a desirable intermediate for the making of dyes and other products, and the alkali metal or alkaline earth metal salts of the formyl compound are more stable forms of this intermediate.
摘要翻译：将β，β，β-三卤-α-羟乙基（例如-CHOH-CCl 3）基团引入2,6-二羟基吡啶中。通过从三卤羟乙基产物中分离卤代衍生的3-甲酰基-4-甲基-2,6-二羟基吡啶是制备染料和其它产物的理想中间体，以及甲酰基的碱金属或碱土金属盐化合物是该中间体的更稳定的形式。

7. 再颁专利

USRE33908E Mixtures of blue mono-azo disperse dyestuffs and their use for dyeing polyester 失效
公开(公告)号：USRE33908E
公开(公告)日：1992-05-05
申请号：US658720
申请日：1991-02-19
申请人： Horst Tappe , Hubert Kruse , Reinhard Kuhn , Albert Bode , Margareta Boos
发明人： Horst Tappe , Hubert Kruse , Reinhard Kuhn , Albert Bode , Margareta Boos
IPC分类号： C09B29/01 , C09B29/085 , C09B67/22 , D06P1/18
CPC分类号： C09B67/0051 , C09B29/0003 , Y10S8/921 , Y10S8/922 , Y10S8/924
摘要： Synthetic fiber materials are effectively colored by dyeing or printing with a dyestuff mixture containing at least two separate dyestuffs (I) and (II) in a weight ratio of (I):(II) of from (20 to 99):(80 to 1) wherein:(I) is at least one dyestuff of the formula ##STR1## and (II) is at least one dyestuff of the formula ##STR2## in which X and Y are the same or different and each is independently chloro and bromo:R.sup.1 and R.sup.2 are the same or different and each independently denotes hydrogen, alkoxy having 1 to 4 carbon atoms, alkenyl having 3 or 4 carbon atoms, cyclohexyl, benzyl, chlorobenzyl, bromobenzyl, nitrobenzyl, cyanobenzyl, alkylbenzyl having 1 to 4 carbon atoms in the alkyl moiety, alkoxybenzyl having 1 to 4 alkoxy carbon atoms, alkyl having 1 to 11 carbon atoms, alkyl having 1 to 11 carbon atoms interrupted by 1 to 3 oxygen atoms or substituted alkyl having 1 to 11 carbon atoms wherein the substituent is one selected from the group consisting of chloro, bromo, cyano, phenyl, phenoxy, hydroxy, (C.sub.1 -to-C.sub.4 -alkyl)-carbonyloxy, (C.sub.1 -to-C.sub.4 -alkoxy)-carbonyl, phenylcarbonyloxy, (C.sub.3 -to-C.sub.5 -alkenyloxy)-carbonyloxy, (C.sub.1 -to-C.sub.4 -alkoxy)-carbonyloxy, phenoxycarbonyloxy, tetrahydrofurfuryl, (C.sub.1 -to-C.sub.4 -alkyl)-tetrahydrofurfuryl, tetrahydropyronyl and (C.sub.1 -to-C.sub.4 -alkyl)-tetrahydropyronyl;R.sup.3 and R.sup.4 are the same or different and each is independently methyl, ethyl, n-propyl or i-propyl;R.sup.5 and R.sup.6 are the same or different and each is independently one of the definitions of R.sup.1 and R.sup.2 excepting hydrogen.

8. 发明授权

US4963661A Water soluble naphthylazopyrazolone dyestuffs having fiber-reactive groups of the vinylsulfone series 失效
标题翻译：具有乙烯基砜系列纤维反应性基团的水溶性萘基吡唑啉酮染料
公开(公告)号：US4963661A
公开(公告)日：1990-10-16
申请号：US198136
申请日：1988-05-24
申请人： Horst Tappe , Dieter Oehme , Ludwig Schlafer , Werner H. Russ
发明人： Horst Tappe , Dieter Oehme , Ludwig Schlafer , Werner H. Russ
IPC分类号： D06P1/384 , C09B62/51
CPC分类号： C09B62/51
摘要： Water-soluble monoazo compounds according to the general formula (1) below having valuable fiber-reactive dyestuff properties which dye carboxamido- and/or hydroxy-containing materials, in particular cellulose fibers, in fast yellow to orange hues. ##STR1## in which the symbols denote: M is hydrogen or an alkali metal,R.sup.1 is hydrogen, methyl, ethyl, methoxy, ethoxy, chlorine, bromine, carboxy or sulfo,R.sup.2 is hydrogen, methyl, ethyl, methoxy, ethoxy, chlorine, or bromine,R is carboxy or lower carbalkoxy,n is the number zero or 1,X and Y independently of each other are each .beta.-thiosulfatoethyl or .beta.-sulfatoethyl or vinyl, however, in the case of X and/or Y being equal to vinyl the index n must be 1.
摘要翻译：根据下述通式（1）的水溶性单偶氮化合物具有有价值的纤维反应性染料性质，它以快速的黄色至橙色的色调染色甲酰氨基和/或羟基的材料，特别是纤维素纤维。其中符号表示：M为氢或碱金属，R1为氢，甲基，乙基，甲氧基，乙氧基，氯，溴，羧基或磺基，R2为氢，甲基，乙基，甲氧基，乙氧基，氯或溴，R是羧基或低级烷氧羰基，n是数字0或1，X和Y彼此独立地各自是β-硫代硫代乙基或β-磺基乙基或乙烯基，然而，在X和/ 或Y等于乙烯基，索引n必须为1。

9. 发明授权

US4678476A Mixtures of blue mono-azo disperse dyestuffs and their use for dyeing polyester 失效
标题翻译：蓝色单偶氮分散染料的混合物及其用于染色聚酯的用途
公开(公告)号：US4678476A
公开(公告)日：1987-07-07
申请号：US911746
申请日：1986-09-26
申请人： Horst Tappe , Hubert Kruse , Reinhard Kuhn , Albert Bode , Margareta Boos
发明人： Horst Tappe , Hubert Kruse , Reinhard Kuhn , Albert Bode , Margareta Boos
IPC分类号： C09B29/01 , C09B29/085 , C09B67/22 , D06P1/18 , C09B29/00 , D06P1/04
CPC分类号： C09B67/0051 , C09B29/0003 , Y10S8/921 , Y10S8/922 , Y10S8/924
摘要： Synthetic fiber materials are effectively colored by dyeing or printing with a dyestuff mixture containing at least two separate dyestuffs (I) and (II) in a weight ratio of (I):(II) of from (20 to 99):(80 to 1) wherein:(I) is at least one dyestuff of the formula ##STR1## and (II) is at least one dyestuff of the formula ##STR2## in which X and Y are the same or different and each is independently chloro and bromo:R.sup.1 and R.sup.2 are the same or different and each independently denotes hydrogen, alkoxy having 1 to 4 carbon atoms, alkenyl having 3 or 4 carbon atoms, cyclohexyl, benzyl, chlorobenzyl, bromobenzyl, nitrobenzyl, cyanobenzyl, alkylbenzyl having 1 to 4 carbon atoms in the alkyl moiety, alkoxybenzyl having 1 to 4 alkoxy carbon atoms, alkyl having 1 to 11 carbon atoms, alkyl having 1 to 11 carbon atoms interrupted by 1 to 3 oxygen atoms or substituted alkyl having 1 to 11 carbon atoms wherein the substituent is one selected from the group consisting of chloro, bromo, cyano, phenyl, phenoxy, hydroxy, (C.sub.1 -to-C.sub.4 -alkyl)-carbonyloxy, (C.sub.1 -to-C.sub.4 -alkoxy)-carbonyl, phenylcarbonyloxy, (C.sub.3 -to-C.sub.5 -alkenyloxy)-carbonyloxy, (C.sub.1 -to-C.sub.4 -alkoxy)-carbonyloxy, phenoxycarbonyloxy, tetrahydrofurfuryl, (C.sub.1 -to-C.sub.4 -alkyl)-tetrahydrofurfuryl, tetrahydrophyronyl and (C.sub.1 -to-C.sub.4 -alkyl)-tetrahydropyronyl;R.sup.3 and R.sup.4 are the same or different and each is independently methyl, ethyl, n-propyl or i-propyl;R.sup.5 and R.sup.6 are the same or different and each is independently one of the definitions of R.sup.1 and R.sup.2 excepting hydrogen.
摘要翻译：合成纤维材料通过用含有至少两种分开的染料（I）和（II）的染料混合物以（20〜99）:( 80〜（80〜 1）其中：（I）是至少一种式IMA的染料，（II）是至少一种式“IMAGE”的染料，其中X和Y相同或不同，并且各自独立地是氯和溴：R1和R2相同或不同，各自独立地表示氢，具有1-4个碳原子的烷氧基，具有3或4个碳原子的链烯基，环己基，苄基，氯苄基，溴苄基，硝基苄基，氰基苄基，具有1-4个碳原子的烷基苄基在烷基部分中，具有1-4个烷氧基碳原子的烷氧基苄基，具有1至11个碳原子的烷基，具有1至3个碳原子的1至11个碳原子的烷基或被取代的具有1至11个碳原子的烷基，其中取代基是1 选自氯，溴，氰基，苯基，杂环基羟基，（C 1 -C 4 - 烷基） - 羰基氧基，（C 1 -C 4 - 烷氧基） - 羰基，苯基羰氧基，（C 3 -C 5 - 烯氧基） - 羰基氧基，（C 1 -C 4 - ） - 羰基氧基，苯氧基羰基氧基，四氢糠基，（C 1 -C 4 - 烷基） - 四氢糠基，四氢化芴基和（C 1 -C 4烷基） - 四氢吡喃基; R 3和R 4相同或不同，各自独立地为甲基，乙基，正丙基或异丙基; R 5和R 6相同或不同，并且各自独立地是除氢之外的R 1和R 2的定义之一。

10. 发明授权

US4552953A Water-insoluble monoazo dyestuffs, their preparation and their use 失效
标题翻译：水不溶性单偶氮染料，其制备及其用途
公开(公告)号：US4552953A
公开(公告)日：1985-11-12
申请号：US450191
申请日：1982-12-16
申请人： Ulrich Buhler , Klaus Kuhlein , Horst Tappe , Maria Kallay , Uwe Kosubek , Rudolf Lowenfeld
发明人： Ulrich Buhler , Klaus Kuhlein , Horst Tappe , Maria Kallay , Uwe Kosubek , Rudolf Lowenfeld
IPC分类号： C09B29/00 , C09B29/01 , C09B29/15 , C09B69/00
CPC分类号： C09B29/103 , C09B29/0003 , C09B69/00
摘要： Monoazo dyestuffs, free of carboxylic acid moieties or sulphonic acid moieties, of the formula ##STR1## wherein A and A' independently of one another are linear or branched alkylene having 2 to 6 carbon atoms;R is hydrogen, alkyl having 1 to 4 carbon atoms, cycloalkyl having 5 or 6 carbon atoms, alkenyl having 3 to 5 carbon atoms, phenyl, benzyl, phenethyl, alkylcarbonyl having 1 to 4 atoms or benzoyl;m is a number from 1 to 5 and n is a number from 0 to 1.
摘要翻译：没有羧酸部分或磺酸部分的单阴离子染料，其具有下式：其中A和A'彼此独立地为具有2至6个碳原子的直链或支链亚烷基; R为氢，具有1至4个碳原子的烷基，具有5或6个碳原子的环烷基，具有3至5个碳原子的烯基，苯基，苄基，苯乙基，1至4个原子的烷基羰基或苯甲酰基; m为1〜5的数，n为0〜1的数。

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