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1. 发明授权

US4265629A Process for the production of resist effects on polyester/cellulose mixed fiber textiles 失效
标题翻译：生产聚酯/纤维素混纺纤维织物的抗皱效果的方法
公开(公告)号：US4265629A
公开(公告)日：1981-05-05
申请号：US105204
申请日：1979-12-19
申请人： Joachim Ribka , Horst Tappe , Kurt Roth , Hans-Jurgen Weyer
发明人： Joachim Ribka , Horst Tappe , Kurt Roth , Hans-Jurgen Weyer
IPC分类号： D06P5/12 , D06P5/15
CPC分类号： D06P5/15 , D06P5/12
摘要： In the process for production of resist effects on textile materials of mixed fibers of polyester and cellulose comprising impregnating the materials with a dye liquor containing disperse dyestuffs and reactive dyestuffs which react with the resisting agents, drying or partially drying the padded materials and subsequently printing a resist paste on the material, and heat-treating the materials the improvement comprises the dischargeable disperse dyestuffs being of a class of dyestuffs of which an exemplary species is ##STR1## one of the tautomeric forms of a class of dyestuffs of which an exemplary species is ##STR2## or disperse dyestuffs which are free from groups conferring solubility in water and which contain at least two carboxylic acid ester moieties.
摘要翻译：在对聚酯和纤维素的混合纤维的纺织材料的抗蚀剂效果的生产过程中，包括用含有分散染料的染液和与抗蚀剂反应的活性染料浸渍材料，干燥或部分干燥填充材料并随后印刷在材料上抵抗糊料，并且对材料进行热处理，改进包括可排放的分散染料是一类染料，其示例性物质是一类染料的互变异构体之一，其示例性物质是或分散不含赋予在水中溶解度且含有至少两个羧酸酯部分的基团的染料。

2. 发明授权

US4252530A Process for dyeing and printing synthetic hydrophobic fiber material 失效
标题翻译：染色和印刷合成疏水纤维材料的工艺
公开(公告)号：US4252530A
公开(公告)日：1981-02-24
申请号：US66432
申请日：1979-08-14
申请人： Joachim Ribka , Horst Tappe , Kurt Roth , Hans-Jurgen Weyer
发明人： Joachim Ribka , Horst Tappe , Kurt Roth , Hans-Jurgen Weyer
IPC分类号： C09B29/042 , C09B29/00 , C09B29/08 , D06P5/12 , D06P5/13 , D06P5/15
CPC分类号： D06P5/151 , C09B29/0085 , C09B29/0809 , D06P5/12
摘要： White patterns on synthetic fiber textiles or patterns of a different color on a colored background are produced by dyeing the material with a dyestuff dischargeable to white, drying the material, printing the material with a discharge resist paste and heating the treated material to 100.degree.-230.degree. C. wherein the discharge agent is a base which produces a pH of at least 8 in a 5% strength aqueous solution.
摘要翻译：在彩色背景上的合成纤维纺织品或不同颜色的图案上的白色图案通过用可排出白色的染料染色材料来制造，干燥材料，用放电抗蚀剂浆料印刷材料并将处理过的材料加热至100℃ - 230℃，其中排出剂是在5％强度的水溶液中产生至少8的pH的碱。

3. 发明授权

US4349348A Process for printing synthetic, hydrophobic fiber material 失效
标题翻译：印刷合成疏水纤维材料的方法
公开(公告)号：US4349348A
公开(公告)日：1982-09-14
申请号：US264715
申请日：1981-05-18
申请人： Horst Tappe , Horst Kindler , Kurt Roth , Hans-Jurgen Weyer
发明人： Horst Tappe , Horst Kindler , Kurt Roth , Hans-Jurgen Weyer
IPC分类号： C09B29/40 , D06P5/12 , D06P5/13 , D06P5/15
CPC分类号： D06P5/12 , C09B29/3608
摘要： Improved textile materials are produced having white or variously colored designs on a colored substrate on textile materials containing hydrophobic, synthetic fibers by impregnating the materials with dye liquors containing dyeing and padding auxiliaries as well as dyestuffs dischargeable to white, drying or incipiently drying the impregnated materials and then printing a desired pattern onto the materials with a discharge reserve paste containing a discharging agent, and subsequently subjecting the materials to a heat treatment at temperatures from 100.degree. to 230.degree. C., the improvement comprises the dyestuffs dischargeable to white being dyestuffs of the formula ##STR1## wherein n is a number from 1 to 9; and said discharging agent being a base which produces a pH value of at least 8 in a 5% strength aqueous solution.
摘要翻译：通过用包含染色和填充助剂的染液浸渍材料以及可排放成白色的染料，干燥或初始干燥浸渍的材料，在含有疏水性合成纤维的纺织材料上的着色基材上制造改进的纺织品材料然后用含有放电剂的放电储备膏将所需的图案印刷在材料上，随后在100℃至230℃的温度下对该材料进行热处理，改进之处在于可以将可排出白色的染料作为染料式其中n为1至9的数; 并且所述排出剂是在5％强度的水溶液中产生至少8的pH值的碱。

4. 发明授权

US4505856A Azo dyestuff dischargeable to white 失效
标题翻译：偶氮染料可放电至白色
公开(公告)号：US4505856A
公开(公告)日：1985-03-19
申请号：US503513
申请日：1983-06-10
申请人： Ulrich Buhler , Joachim Ribka , Horst Tappe , Kurt Roth
发明人： Ulrich Buhler , Joachim Ribka , Horst Tappe , Kurt Roth
IPC分类号： C09B29/00 , C09B29/08 , C09B43/124 , D06P5/12 , D06P5/15 , C09B29/033 , C09B29/039 , C09B29/085 , C09B29/09
CPC分类号： D06P5/12 , C09B29/00 , C09B29/0807 , C09B43/1247 , D06P5/151
摘要： Azo dyestuff free from groups imparting solubility in water are used in the process for the production of white or variously colored designs on a colored substrate on textile material wherein the dyestuff is dischargeable to white and is of the formulaD--N.dbd.N--K--NHSO.sub.2 Rwhereinwherein D is 6-nitrobenzthiazol-2-yl, 5-nitrobenzisothiazol-3-yl, a substituted phenyl, a substituted thiazole or a substituted thiophene moiety;K is a 1,4-phenylene, 1,4-naphthylene, 2,5-thiazolylene or 2,5-thienylene; andR is alkyl, substituted alkyl, alkenyl, substituted alkenyl, phenyl or substituted phenyl.
摘要翻译：用于在纺织材料上着色的基材上生产白色或各种着色图案的方法中使用不含赋予水溶性的基团的偶氮染料，其中染料可以排放到白色并具有式DN = NK-NHSO 2 R，其中D 是6-硝基苯并噻唑-2-基，5-硝基苯并异噻唑-3-基，取代的苯基，取代的噻唑或取代的噻吩部分; K是1,4-亚苯基，1,4-亚萘基，2,5-噻唑基或2,5-亚噻吩基; R是烷基，取代的烷基，烯基，取代的烯基，苯基或取代的苯基。

5. 发明授权

US4406661A Process for dyeing and printing synthetic, hydrophobic fibre material with dischargeable azo disperse dye 失效
标题翻译：染色和印刷合成疏水纤维材料与可放电偶氮分散染料的方法
公开(公告)号：US4406661A
公开(公告)日：1983-09-27
申请号：US386916
申请日：1982-06-10
申请人： Ulrich Buhler , Joachim Ribka , Horst Tappe , Kurt Roth
发明人： Ulrich Buhler , Joachim Ribka , Horst Tappe , Kurt Roth
IPC分类号： C09B29/00 , C09B29/08 , C09B43/124 , D06P5/12 , D06P5/15 , C09B43/12
CPC分类号： C09B43/1247 , C09B29/00 , C09B29/0807 , D06P5/12 , D06P5/151 , Y10S8/922
摘要： Azo dyestuffs free from groups imparting solubility in water are used in the process for the production of white or variously colored designs on a colored substrate on textile materials containing hydrophobic, synthetic fibers by impregnating the materials with dye liquors containing dyeing auxiliaries and padding auxiliaries as well as dyestuffs which are dischargeable to white, drying or incipiently drying the impregnated materials, printing the materials with an alkaline discharge reserve paste which contains a discharging agent, and subsequently subjecting the materials to a heat treatment at temperatures from 100.degree. to 230.degree. C., wherein said discharging agent is a base which produces a pH value of at least 8 in a 5% strength aqueous solution and the dyestuffs which are dischargeable to white are of the formulaD--N.dbd.N--K--NHSO.sub.2 RwhereinD is 6-nitrobenzthiazol-2-yl, 5-nitrobenzisothiazol-3-yl, a substituted phenyl, a substituted thiazole or a substituted thiophene moiety;K is a coupling component of the 1,4-phenylene, 1,4-naphthylene, 2,5-thiazolyl or 2,5-thienyl series; andR is alkyl, substituted alkyl, alkenyl, substituted alkenyl, phenyl or substituted phenyl.
摘要翻译：使用不含赋予溶解性的基团的偶氮染料用于在含有疏水性合成纤维的纺织材料上的有色基材上生产白色或各种着色图案的方法，通过用含有染色助剂和填充助剂的染液浸渍材料作为可以排出白色的染料，干燥或初始干燥浸渍的材料，用含有放电剂的碱性放电储备膏印刷材料，随后在100℃至230℃的温度下进行热处理。其中所述排出剂是在5％强度水溶液中产生至少8的pH值的碱，并且可排出至白色的染料具有式DN = NK-NHSO 2 R，其中D为6-硝基苯并噻唑-2-基，取代的苯基，取代的噻唑或取代的噻吩部分; K是1,4-亚苯基，1,4-亚萘基，2,5-噻唑基或2,5-噻吩基系的偶联组分; R是烷基，取代的烷基，烯基，取代的烯基，苯基或取代的苯基。

6. 发明授权

US4567252A Water-insoluble naphthol monoazo dyestuff 失效
标题翻译：水不溶性萘酚单偶氮染料
公开(公告)号：US4567252A
公开(公告)日：1986-01-28
申请号：US492240
申请日：1983-05-06
申请人： Ulrich Buhler , Horst Tappe , Albert Bode , Manfred Hahnke , Kurt Roth
发明人： Ulrich Buhler , Horst Tappe , Albert Bode , Manfred Hahnke , Kurt Roth
IPC分类号： C09B29/01 , C09B29/15 , C09B29/02 , C09B29/34 , D06P3/24 , D06P3/52
CPC分类号： C09B29/0003 , C09B29/103 , Y10S534/02
摘要： Azo dyestuff of the formula ##STR1## wherein X is secondary amino or tertiary amino moiety, useful for dyeing and printing hydrophobic fiber materials to produce a deep orange color having excellent fastness properties and also useful for coloring organic solvents, mineral oil products, waxes, plastics and surface coatings.
摘要翻译：其中X是仲氨基或叔氨基部分的偶氮染料，其可用于染色和印刷疏水纤维材料以产生具有优异坚牢性的深橙色，并且还可用于着色有机溶剂，矿物油产品，蜡，塑料和表面涂层。

7. 发明授权

US4416665A Water-insoluble azo dyestuff, for discharge printing 失效
标题翻译：水不溶性偶氮染料，用于放电印刷
公开(公告)号：US4416665A
公开(公告)日：1983-11-22
申请号：US303852
申请日：1981-09-21
申请人： Horst Tappe , Kurt Roth
发明人： Horst Tappe , Kurt Roth
IPC分类号： C09B29/00 , C09B29/08 , C09B29/04 , D06P5/17
CPC分类号： C09B29/0085 , C09B29/0816 , Y10S8/922
摘要： Water-insoluble azo dyestuff of the formula ##STR1## its manufacture and its use as the dyestuff in the dyeing and printing of hydrophobic fiber materials.
摘要翻译：水溶性偶氮染料，其配方为“IMAGE”，其制造及其用作染色和印染疏水性纤维材料的染料。

8. 发明授权

US4431585A Water-insoluble azo dyestuffs, processes for their manufacture and their use for dyeing and printing synthetic hydrophobic fiber material 失效
标题翻译：水不溶性偶氮染料，其制造方法及其用于染色和印刷合成疏水纤维材料的用途
公开(公告)号：US4431585A
公开(公告)日：1984-02-14
申请号：US237628
申请日：1981-02-24
申请人： Horst Tappe , Ulrich Buhler , Kurt Roth , Hans-J. Weyer , Uwe Kosubek
发明人： Horst Tappe , Ulrich Buhler , Kurt Roth , Hans-J. Weyer , Uwe Kosubek
IPC分类号： C09B29/08 , C09B31/043 , C09B43/40 , C09B43/42 , C09B29/06 , C09B29/00
CPC分类号： C09B43/405 , C09B29/0813 , C09B31/043 , C09B43/40 , C09B43/42
摘要： Water-insoluble azo dyestuffs suitable for dyeing and printing synthetic hydrophobic fiber materials are produced by azo coupling and have the formula ##STR1## wherein D is free from ionic moieties and is an unsubstituted or substituted phenyl, thiazole, isothiazole, benzthiazole, thiadiazole, benzisothiazole or thiophene moiety;A is alkylene having 2 to 6 carbon atoms which is unsubstituted or substituted by --OH;B is hydrogen, alkyl having 1 to 4 carbon atoms, hydroxyalkyl having 2 to 4 carbon atoms, alkoxyalkyl having 1 to 4 carbon atoms in the alkoxy moiety and a total of 3 to 8 carbon atoms, alkanoyloxyalkyl having 2 to 6 carbon atoms in the alkanoyl moiety and a total of 3 to 8 carbon atoms, hydroxypolyoxyalkylene having 4 to 12 carbon atoms, alkoxypolyoxyalkylene having 1 to 4 carbon atoms in the alkoxy moiety and a total of 5 to 16 carbon atoms, alkanoyloxypolyoxyalkylene having 2 to 5 carbon atoms in the alkanoyl moiety and a total of 5 to 16 carbon atoms, alkanoyl having 2 to 6 carbon atoms or benzoyl;R.sup.1 is hydrogen, methyl or chlorine;R.sup.2 is hydrogen, halogen, alkyl having 1 to 4 carbon atoms or alkoxy having 1 to 4 carbon atoms;and R.sup.3 is hydrogen or alkoxy having 1 to 8 carbon atoms.
摘要翻译：适用于染色和印刷合成疏水性纤维材料的水不溶性偶氮染料是通过偶氮偶合产生的，并具有式“IMAGE”，其中D不含离子部分，是未取代或取代的苯基，噻唑，异噻唑，苯并噻唑，噻二唑，苯并异噻唑或噻吩部分; A是未被取代或被-OH取代的具有2至6个碳原子的亚烷基; B是氢，具有1至4个碳原子的烷基，具有2至4个碳原子的羟基烷基，烷氧基部分中具有1至4个碳原子的烷氧基烷基和总共3至8个碳原子，在该化合物中具有2至6个碳原子的烷酰氧基烷基烷酰基部分和总共3至8个碳原子，具有4至12个碳原子的羟基聚氧化烯，烷氧基部分中具有1至4个碳原子的烷氧基聚氧化烯和总共5至16个碳原子，在2至5个碳原子上具有2至5个碳原子的烷酰氧基聚氧化烯烷酰基部分和总共5至16个碳原子，具有2至6个碳原子的烷酰基或苯甲酰基; R1是氢，甲基或氯; R2是氢，卤素，具有1至4个碳原子的烷基或具有1至4个碳原子的烷氧基; 并且R 3是氢或具有1至8个碳原子的烷氧基。

9. 发明授权

US4398913A Process for producing discharge reserve prints on textile materials 失效
标题翻译：在纺织材料上生产放电预留印花的工艺
公开(公告)号：US4398913A
公开(公告)日：1983-08-16
申请号：US304099
申请日：1981-09-21
申请人： Ulrich Buhler , Joachim Ribka , Kurt Roth , Theo Stahl
发明人： Ulrich Buhler , Joachim Ribka , Kurt Roth , Theo Stahl
IPC分类号： D06P5/12 , D06P5/13 , D06P5/17
CPC分类号： D06P5/12 , D06P5/17 , Y10S534/01 , Y10S8/922
摘要： In the process for production of discharge reserve prints on textile material comprised of water-repellent fibers or water repellent fibers mixed with cellulose fibers, wherein a disperse dyestuff which is dischargeable to white is applied in the form of a dye liquor or printing paste to the textile material after which said material is dried or incipiently dried, and a discharge reserve printing paste is printed on the material in the desired pattern, and the thus treated material is subsequently subjected to a heat treatment at temperatures of 100.degree. to 230.degree. C., the improvement comprises said disperse dyestuff which is dischargeable to white is a dyestuff of the formula ##STR1## as more fully defined herein and wherein said discharge reserve printing paste contains, as the discharging agent, a base which produces a pH value of at least 8 in a 5% strength aqueous solution.
摘要翻译：在与由纤维素纤维混合的疏水性纤维或防水纤维构成的纺织材料上制造出料备料的方法中，将可排出白色的分散染料以染料液或印刷浆料的形式施用于纺织材料，之后将所述材料干燥或初始干燥，并将排出储备印刷浆料以期望的图案印刷在材料上，然后将这样处理的材料在100℃至230℃的温度下进行热处理。改进之处在于，所述分散染料可放电至白色为本文更完整定义的式“IMAGE”的染料，其中所述放电储备印刷浆料含有至少产生至少pH值的碱 8在5％强度的水溶液中。

10. 发明授权

US4386935A Process for producing discharge reserve prints on textile materials with amino-azo-benzene dyes 失效
标题翻译：用氨基偶氮苯染料在纺织材料上生产放料储存印花的方法
公开(公告)号：US4386935A
公开(公告)日：1983-06-07
申请号：US305998
申请日：1981-09-28
申请人： Ulrich Buhler , Klaus Kuhlein , Theo Stahl , Horst Tappe , Kurt Roth
发明人： Ulrich Buhler , Klaus Kuhlein , Theo Stahl , Horst Tappe , Kurt Roth
IPC分类号： D06P5/13 , D06P5/12 , D06P5/17 , C09B29/08
CPC分类号： D06P5/17 , D06P5/12
摘要： An improved process for producing discharge reserve prints on textile materials comprising water-repellent fibers or mixed water-repellent and cellulose fibers wherein a disperse dyestuff which is dischargeable to white is applied to the textile material in the form of a dye liquor or dye printing paste, at least partially drying the textile material, applying a discharge reserve printing paste to the material by printing on the material in the desired pattern and subsequently heating the printed material at temperatures from 100.degree. to 230.degree. C., with the improvement comprising (a) the discharge reserve printing paste containing, as the discharging agent, an alkaline material which produces a pH value of at least 8 in 5% strength aqueous solution and (b) the disperse dyestuff which is dischargeable to white is a disperse dyestuff of the formula ##STR1## as more fully defined herein.
摘要翻译：一种用于在纺织材料上生产排放储备印刷品的改进方法，其包括拒水纤维或混合疏水和纤维素纤维，其中将可排出白色的分散染料以染料液或染料印刷浆料的形式施加到织物材料至少部分地干燥纺织材料，通过在所需图案的材料上印刷并随后在100-230℃的温度下加热印刷材料，将放电储备印刷浆料施加到材料上，改进包括（a ）排放储备印刷浆料，其含有在5重量％水溶液中产生至少8的pH值的碱性物质作为排出剂，和（b）可分散到白色的分散染料是式如本文中更全面地定义。

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