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    • 62. 发明授权
    • Sputtering methods for depositing stress tunable tantalum and tantalum
nitride films
    • 用于沉积应力可调钽和氮化钽膜的溅射方法
    • US6139699A
    • 2000-10-31
    • US863451
    • 1997-05-27
    • Tony ChiangPeijun DingBarry L. Chin
    • Tony ChiangPeijun DingBarry L. Chin
    • C23C14/00C23C14/06C23C14/14C23C14/16C23C14/34C23C14/35C23C14/58H01L21/285H01L21/768H01L23/532
    • C23C14/345C23C14/0036C23C14/0641C23C14/16C23C14/3492C23C14/358C23C14/5833H01L21/2855H01L21/76838H01L21/76841H01L21/76843H01L21/76862H01L21/76864H01L23/53233H01L23/53238H01L2924/0002
    • The present disclosure pertains to our discovery that residual stress residing in a tantalum film or tantalum nitride film can be controlled (tuned) by controlling particular process variables during film deposition. By tuning individual film stresses within a film stack, it is possible to balance stresses within the stack. Process variables of particular interest include: power to the sputtering target; process chamber pressure (i.e., the concentration of various gases and ions present in the chamber); substrate DC offset bias voltage (typically an increase in the AC applied substrate bias power); power to an ionization source (typically a coil); and temperature of the substrate upon which the film is deposited. The process chamber pressure and the substrate offset bias most significantly affect the film tensile and compressive stress components, respectively. The most advantageous tuning of a sputtered film is achieved using high density plasma sputter deposition, which provides for particular control over the ion bombardment of the depositing film surface. When the tantalum or tantalum nitride film is deposited using high density plasma sputtering, power to the ionization source can be varied for stress tuning of the film. We have been able to reduce the residual stress in tantalum or tantalum nitride films deposited using high density plasma sputtering to between about 6.times.10.sup.+9 dynes/cm.sup.2 and about -6.times.10.sup.+9 dynes/cm.sup.2 using techniques described herein. The tantalum and tantalum nitride films can also be tuned following deposition using ion bombardment of the film surface and annealing of the deposited film.
    • 本公开涉及我们的发现,通过在膜沉积期间控制特定的工艺变量,可以控制(调整)驻留在钽膜或氮化钽膜中的残余应力。 通过调整薄膜叠层内的各个薄膜应力,可以平衡叠层内的应力。 特别感兴趣的过程变量包括:溅射靶的功率; 处理室压力(即存在于室中的各种气体和离子的浓度); 衬底DC偏移偏置电压(通常为施加衬底偏置功率的AC增加); 电源(通常为线圈); 以及沉积膜的基板的温度。 处理室压力和基板偏移偏压分别最显着地影响膜的拉伸和压应力分量。 使用高密度等离子体溅射沉积来实现溅射膜的最有利的调谐,其提供对沉积膜表面的离子轰击的特定控制。 当使用高密度等离子体溅射沉积钽或氮化钽膜时,电离源的功率可以改变以用于膜的应力调谐。 使用本文所述的技术,我们已经能够将使用高密度等离子体溅射沉积的钽或氮化钽膜中的残余应力减小到约6×10 9 + 9达因/ cm 2和约-6×10 9达因/ cm 2之间。 也可以在使用离子轰击膜表面和沉积膜的退火进行沉积之后调整钽和氮化钽膜。
    • 67. 发明授权
    • Stackable multi-port gas nozzles
    • 可堆叠多口气体喷嘴
    • US08968473B2
    • 2015-03-03
    • US12880941
    • 2010-09-13
    • Steve PoppeYan RozenzonPeijun Ding
    • Steve PoppeYan RozenzonPeijun Ding
    • C23C16/455C23C16/458C23C16/44
    • C23C16/45576C23C16/4412C23C16/45521C23C16/4587
    • One embodiment provides a reactor for material deposition. The reactor includes a chamber and at least one gas nozzle. The chamber includes a pair of susceptors, each having a front side and a back side. The front side mounts a number of substrates. The susceptors are positioned vertically so that the front sides of the susceptors face each other, and the vertical edges of the susceptors are in contact with each other, thereby forming a substantially enclosed narrow channel between the substrates mounted on different susceptors. The gas nozzle includes a gas-inlet component situated in the center and a detachable gas-outlet component stacked around the gas-inlet component. The gas-inlet component includes at least one opening coupled to the chamber, and is configured to inject precursor gases into the chamber. The detachable gas-outlet component includes at least one opening coupled to the chamber, and is configured to output exhaust gases from the chamber.
    • 一个实施方案提供了用于材料沉积的反应器。 反应器包括室和至少一个气体喷嘴。 该室包括一对基座,每个基座具有前侧和后侧。 前面安装了许多基板。 基座垂直定位,使得基座的前侧彼此面对,并且基座的垂直边缘彼此接触,从而在安装在不同的基座上的基板之间形成基本封闭的窄通道。 气体喷嘴包括位于中心的气体入口部件和在气体入口部件周围堆叠的可拆卸气体出口部件。 气体入口部件包括至少一个连接到腔室的开口,并且被构造成将前体气体注入到腔室中。 可拆卸的气体出口部件包括至少一个连接到该腔室的开口,并且构造成输出来自腔室的废气。
    • 69. 发明申请
    • STACKABLE MULTI-PORT GAS NOZZLES
    • 可堆叠多口气体喷嘴
    • US20110067632A1
    • 2011-03-24
    • US12880941
    • 2010-09-13
    • Steve PoppeYan RozenzonPeijun Ding
    • Steve PoppeYan RozenzonPeijun Ding
    • C23C16/455C23C16/00C23C16/458
    • C23C16/45576C23C16/4412C23C16/45521C23C16/4587
    • One embodiment provides a reactor for material deposition. The reactor includes a chamber and at least one gas nozzle. The chamber includes a pair of susceptors, each having a front side and a back side. The front side mounts a number of substrates. The susceptors are positioned vertically so that the front sides of the susceptors face each other, and the vertical edges of the susceptors are in contact with each other, thereby forming a substantially enclosed narrow channel between the substrates mounted on different susceptors. The gas nozzle includes a gas-inlet component situated in the center and a detachable gas-outlet component stacked around the gas-inlet component. The gas-inlet component includes at least one opening coupled to the chamber, and is configured to inject precursor gases into the chamber. The detachable gas-outlet component includes at least one opening coupled to the chamber, and is configured to output exhaust gases from the chamber.
    • 一个实施方案提供了用于材料沉积的反应器。 反应器包括室和至少一个气体喷嘴。 该室包括一对基座,每个基座具有前侧和后侧。 前面安装了许多基板。 基座垂直定位,使得基座的前侧彼此面对,并且基座的垂直边缘彼此接触,从而在安装在不同的基座上的基板之间形成基本封闭的窄通道。 气体喷嘴包括位于中心的气体入口部件和在气体入口部件周围堆叠的可拆卸气体出口部件。 气体入口部件包括耦合到腔室的至少一个开口,并且构造成将前体气体注入到腔室中。 可拆卸的气体出口部件包括至少一个连接到该腔室的开口,并且构造成输出来自腔室的废气。