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    • 1. 发明专利
    • Method for producing porous glass, and method for producing optical member
    • 用于生产多孔玻璃的方法和用于生产光学构件的方法
    • JP2012193101A
    • 2012-10-11
    • JP2012014366
    • 2012-01-26
    • Canon Incキヤノン株式会社
    • KOKETSU NAOYUKICHO SOIKOTANI YOSHINORISUGIYAMA SUSUMUTAKASHIMA KENJI
    • C03C3/089C03C11/00G02B1/00
    • C03C11/005C03B32/00
    • PROBLEM TO BE SOLVED: To provide a method for producing porous glass capable of controlling a pore size and a porosity by performing phase separation treatment by a low-temperature heat treatment.SOLUTION: This method for producing porous glass includes: a step for forming phase-separated glass by generating phase separation by heating at a temperature of ≥300°C to ≤500°C for ≥3 to ≤50 hours, base material glass in which a SiOconcentration is ≥50 to ≤70 wt.%, a BOconcentration is ≥15 to ≤40 wt.%, a LiO concentration is ≥1.0 to ≤8.0 wt.%, a NaO concentration is ≥2.0 to ≤8.0 wt.%, a KO concentration is ≥0.3 to ≤5.0 wt.%, the total of concentrations of LiO, NaO and KO is ≥3.5 to ≤15 wt.%, and the KO concentration has a ratio of ≥0.10 and ≤0.30 to the total of the concentrations of LiO, NaO and KO; and a step for forming porous glass by etching the phase-separated glass.
    • 解决的问题:提供一种通过进行低温热处理的相分离处理来制造能够控制孔径和孔隙率的多孔玻璃的方法。 &lt; P&gt;解决方案:多孔玻璃的制造方法包括:通过在≥300℃〜500℃的温度下加热而产生相分离≥3〜≤50小时的相分离玻璃的工序,基材 SiO 2 浓度的玻璃为≥50〜≤70重量%,B 2 3 浓度≥15〜≤40重量%,Li 2 O浓度≥1.0〜≤8.0重量%,Na 2 O浓度≥2.0〜≤8.0重量%,K 2 O浓度≥0.3〜≤5.0重量% Li 2 O,Na 2 O和K 2 >O≥3.5〜≤15重量%,K 2 O浓度与Li 2 O,Na 2 O和K 2 < 以及通过蚀刻相分离玻璃来形成多孔玻璃的步骤。 版权所有(C)2013,JPO&INPIT
    • 6. 发明专利
    • Method of manufacturing porous glass and method of manufacturing imaging apparatus
    • 制造多孔玻璃的方法和制造成像装置的方法
    • JP2012131695A
    • 2012-07-12
    • JP2011253073
    • 2011-11-18
    • Canon Incキヤノン株式会社
    • TAKASHIMA KENJICHO SOIKOTANI YOSHINORISUGIYAMA SUSUMUKOKETSU NAOYUKI
    • C03C15/00C03B32/00G02B1/11G02B1/115
    • C03C11/005C03B32/00C03C15/00C03C21/002C03C21/005
    • PROBLEM TO BE SOLVED: To provide a method of manufacturing a porous glass in which the porosity decreases as a function of the distance from the surface in the direction of depth.SOLUTION: A method of manufacturing a porous glass includes: a step of bringing one or more than one ion species selected from silver ion, potassium ion and lithium ion into contact with a matrix glass containing borosilicate glass as main ingredient and heating the matrix glass to form a glass body having an ion concentration distribution with a concentration of the one or more than one ion species decreasing as a function of a distance from a surface in a direction of depth; a step of heating and phase-separating the glass body to form a phase-separated glass; and a step of etching the phase-separated glass to form a porous glass having a porosity decreasing as the function of the distance from the surface in the direction of depth.
    • 要解决的问题:提供一种多孔玻璃的制造方法,其中孔隙率随深度方向与表面的距离而减小。 解决方案:一种制造多孔玻璃的方法包括:将选自银离子,钾离子和锂离子中的一种或多种离子种类与含有硼硅酸盐玻璃的基质玻璃作为主要成分接触,并加热 基质玻璃以形成具有离子浓度分布的玻璃体,所述离子浓度分布与一个或多于一个离子种类的浓度作为距离深度方向上的表面的距离的函数减小; 加热和相分离玻璃体以形成相分离玻璃的步骤; 以及蚀刻相分离玻璃以形成孔隙率随着深度方向与表面的距离的函数而减小的步骤。 版权所有(C)2012,JPO&INPIT
    • 7. 发明专利
    • Method of producing phosphor, method of producing face plate, and method of manufacturing image display apparatus
    • 生产磷光体的方法,生产面板的方法和制造图像显示装置的方法
    • JP2012067167A
    • 2012-04-05
    • JP2010212222
    • 2010-09-22
    • Canon Incキヤノン株式会社
    • KOKETSU NAOYUKISARUTA HISASHIROSASAKURI DAISUKESOMA MAKOTO
    • C09K11/08C09K11/59
    • PROBLEM TO BE SOLVED: To reliably prevent phosphor particles 5 from aggregating when producing a phosphor in a heating process where crystallinity of precursor particles 1 of the phosphor is improved.SOLUTION: A method of producing a phosphor includes: dispersing the precursor particles 1 of the phosphor in an organic resin 3 to produce a precursor-dispersed paste 2; improving the crystallinity of the precursor particles 1 to produce the phosphor particles 5 in the presence of carbon 4 made by carbonizing the organic resin 3 present in the precursor-dispersed paste 2, thereby obtaining a mixture of the phosphor particles 5 and carbon 4; and thereafter subjecting the mixture to heating processing at temperature lower than the temperature at which the phosphor particles 5 are aggregated, thus removing the carbon 4.
    • 要解决的问题:在提高荧光体的前体颗粒1的结晶度的加热过程中,在制造荧光体时,可靠地防止荧光体颗粒5聚集。 解决方案:一种制造荧光体的方法包括:将荧光体的前体颗粒1分散在有机树脂3中以制备前体分散糊2; 提高前体粒子1的结晶度,在碳前体分散膏2中存在的有机树脂3碳化4的存在下制造荧光体粒子5,得到荧光体粒子5和碳4的混合物; 然后在比荧光体颗粒5聚集的温度低的温度下对混合物进行加热处理,从而除去碳4.版权所有(C)2012,JPO&INPIT