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    • 8. 发明授权
    • Simple method for detecting temperature distributions in single crystals
and method for manufacturing silicon single crystals by employing the
simple method
    • 采用简单方法检测单晶温度分布的简单方法及单晶硅制造方法
    • US6042646A
    • 2000-03-28
    • US15515
    • 1998-01-29
    • Fumitaka IshikawaToshiaki SaishojiKozo Nakamura
    • Fumitaka IshikawaToshiaki SaishojiKozo Nakamura
    • C30B15/00C30B15/14C30B15/20
    • C30B29/06C30B15/14Y10T117/1004Y10T117/1008
    • A single crystal is pulled to a length at which the beginning of the body of the single crystal is assumed sufficiently to have been cooled down to a temperature below 1000.degree. C.; then the single crystal being pulled is detached from the molten silicon by pulling it at a speed high enough to cut it out from the molten silicon. Then oxygen precipitation heat-treatment is performed on the single crystal to locate the portion of AOP. AOP arises at the boundary of grown-in defects being formed zone while the single crystal passes through 1100.degree. C., and the position is at about 1100.degree. C. immediately before, detaching the single crystal out from the molten silicon. Therefore, the position at temperature 1100.degree. C. in the single crystal immediately before detaching the single crystal out from the molten silicon are known, then the temperature distributions of the single crystal immediately before detaching it out from the molten silicon can be decided easily. If the speed at which the temperature range near 1100.degree. C. is passed through is controlled, then the occurrence of the defects while growing the single crystal can be controlled.
    • 将单晶拉至一定长度,在该长度下,假定单晶体的开始充分地冷却至低于1000℃的温度; 然后通过以足够高的速度将熔融硅从熔融硅中分离出来,将其从熔融硅中切出。 然后在单晶上进行氧沉淀热处理以定位AOP的部分。 在单晶通过1100℃时,在形成区域的生长缺陷的边界处产生AOP,并且立即在约1100℃的位置处将单晶从熔融硅中分离出来。 因此,在将单晶从熔融硅中分离出来之前,在单晶中的1100℃的位置是已知的,因此可以容易地决定将其从熔融硅中分离出来之前的单晶的温度分布。 如果通过1100℃附近的温度的速度被控制,则可以控制生长单晶时的缺陷的发生。