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1. 发明申请

WO2008118960A3 RADIATION PROTECTION USING CARBON NANOTUBE DERIVATIVES 审中-公开
标题翻译：使用碳纳米管衍生物进行辐射防护
公开(公告)号：WO2008118960A3
公开(公告)日：2009-05-07
申请号：PCT/US2008058268
申请日：2008-03-26
申请人： UNIV RICE WILLIAM M , TOUR JAMES M , LU MENG , LUCENTE-SCHULTZ REBECCA , LEONARD ASHLEY , DOYLE CONDELL DEWAYNE , KOSYNKIN DMITRY V , PRICE BRANDI KATHERINE , CONYERS JODIE L , MOORE VALERIE C , CASSCELLS S WARD , MYERS JEFFREY NICHOLAS , MASON KATHY ANN , MILAS LUKA
发明人： TOUR JAMES M , LU MENG , LUCENTE-SCHULTZ REBECCA , LEONARD ASHLEY , DOYLE CONDELL DEWAYNE , KOSYNKIN DMITRY V , PRICE BRANDI KATHERINE , CONYERS JODIE L , MOORE VALERIE C , CASSCELLS S WARD , MYERS JEFFREY NICHOLAS , MASON KATHY ANN , MILAS LUKA
IPC分类号： A61K9/00
CPC分类号： A61K9/0092 , A61K8/19 , A61K47/60 , A61K47/6925 , A61K2800/413 , A61Q17/04 , B82Y5/00 , B82Y30/00 , B82Y40/00 , C01B32/15 , C01B2202/02 , C01B2202/04 , C01B2202/06
摘要： A method of reducing side effects of damage in a human subject exposed to radiation includes administering to the human subject carbon nanotubes in a pharmaceutically acceptable carrier after or prior to exposure to radiation. A composition for reducing radical damage includes a carbon nanotube which is functionalized (1) for substantial water solubility and (2) with a radical trapping agent appended to the carbon nanotube forming a radical scavenger- carbon nanotube conjugate.
摘要翻译：在暴露于辐射的人类受试者中减少损伤的副作用的方法包括在暴露于辐射之后或暴露于辐射之前向人受试者在药学上可接受的载体中施用碳纳米管。用于还原自由基损伤的组合物包括官能化的碳纳米管（1），其具有显着的水溶性，和（2）与形成自由基清除碳纳米管缀合物的碳纳米管附着的自由基捕获剂。

2. 发明申请

WO2009070380A3 WATER-SOLUBLE CARBON NANOTUBE COMPOSITIONS FOR DRUG DELIVERY AND MEDICAL APPLICATIONS 审中-公开
标题翻译：水溶性碳纳米管组合物用于药物递送和医疗应用
公开(公告)号：WO2009070380A3
公开(公告)日：2009-10-29
申请号：PCT/US2008078776
申请日：2008-10-03
申请人： UNIV RICE WILLIAM M , TOUR JAMES M , LUCENTE-SCHULTZ REBECCA , LEONARD ASHLEY , KOSYNKIN DMITRY V , PRICE BRANDI KATHERINE , HUDSON JARED L , CONYERS JODIE L , MOORE VALERIE C , CASSCELLS S WARD , MYERS JEFFREY N , MILAS ZVONIMIR L , MASON KATHY A , MILAS LUKA
发明人： TOUR JAMES M , LUCENTE-SCHULTZ REBECCA , LEONARD ASHLEY , KOSYNKIN DMITRY V , PRICE BRANDI KATHERINE , HUDSON JARED L , CONYERS JODIE L , MOORE VALERIE C , CASSCELLS S WARD , MYERS JEFFREY N , MILAS ZVONIMIR L , MASON KATHY A , MILAS LUKA
IPC分类号： A61K9/00
CPC分类号： B82Y5/00 , A61K47/60 , A61K47/6925 , A61K47/6929
摘要： Compositions comprising a plurality of functionalized carbon nanotubes and at least one type of payload molecule are provided herein. The compositions are soluble in water and PBS in some embodiments. In certain embodiments, the payload molecules are insoluble in water. Methods are described for making the compositions and administering the compositions. An extended release formulation for paclitaxel utilizing functionalized carbon nanotubes is also described.
摘要翻译：本文提供了包含多个官能化碳纳米管和至少一种类型的有效负载分子的组合物。在一些实施方案中，组合物可溶于水和PBS。在某些实施例中，有效负载分子不溶于水。描述了制备组合物和施用组合物的方法。还描述了利用官能化碳纳米管的紫杉醇的缓释制剂。

3. 发明申请

WO2011016889A3 HIGHLY OXIDIZED GRAPHENE OXIDE AND METHODS FOR PRODUCTION THEREOF 审中-公开
标题翻译：高度氧化的氧化石墨及其生产方法
公开(公告)号：WO2011016889A3
公开(公告)日：2011-04-21
申请号：PCT/US2010034905
申请日：2010-05-14
申请人： UNIV RICE WILLIAM M , TOUR JAMES M , KOSYNKIN DMITRY V
发明人： TOUR JAMES M , KOSYNKIN DMITRY V
IPC分类号： C01B31/00
CPC分类号： C01B31/0476 , B82Y30/00 , B82Y40/00 , C01B32/192 , C01B32/23 , C09K8/032
摘要： A highly oxidized form of graphene oxide and methods for production thereof are described in various embodiments of the present disclosure. In general, the methods include mixing a graphite source with a solution containing at least one oxidant and at least one protecting agent and then oxidizing the graphite source with the at least one oxidant in the presence of the at least one protecting agent to form the graphene oxide. Graphene oxide synthesized by the presently described methods is of a high structural quality that is more oxidized and maintains a higher proportion of aromatic rings and aromatic domains than does graphene oxide prepared in the absence of at least one protecting agent. Methods for reduction of graphene oxide into chemically converted graphene are also disclosed herein. The chemically converted graphene of the present disclosure is significantly more electrically conductive than is chemically converted graphene prepared from other sources of graphene oxide.
摘要翻译：在本公开的各种实施例中描述了氧化石墨烯的高度氧化形式及其生产方法。通常，所述方法包括将石墨源与含有至少一种氧化剂和至少一种保护剂的溶液混合，然后在至少一种保护剂存在下用至少一种氧化剂氧化石墨源以形成石墨烯氧化物。通过目前描述的方法合成的氧化石墨烯具有较高的结构质量，其比没有至少一种保护剂时制备的石墨烯氧化物更多地被氧化并保持较高比例的芳族环和芳族域。本文还公开了将氧化石墨烯还原成化学转化的石墨烯的方法。本公开内容的化学转化的石墨烯与由其他石墨烯氧化物源制备的化学转化的石墨烯相比导电性明显更高。

4. 发明申请

WO2009089391A3 GRAPHENE COMPOSITONS AND DRILLING FLUIDS DERIVED THEREFROM 审中-公开
标题翻译：石墨复合材料和由此衍生的钻井液
公开(公告)号：WO2009089391A3
公开(公告)日：2009-10-29
申请号：PCT/US2009030498
申请日：2009-01-08
申请人： TOUR JAMES M , SCHMIDT HOWARD K , LOMEDA JAY R , KOSYNKIN DMITRY V , DOYLE CONDELL D , UNIV RICE WILLIAM M
发明人： TOUR JAMES M , SCHMIDT HOWARD K , LOMEDA JAY R , KOSYNKIN DMITRY V , DOYLE CONDELL D
IPC分类号： C09K8/03 , C01B31/00 , C01B31/04 , C09K8/035 , C09K8/62
CPC分类号： C09K8/032 , B82Y30/00 , B82Y40/00 , C01B32/192 , C01B32/194 , C01B32/23 , C01B2204/04 , C01B2204/28 , C09K8/035 , C09K8/62 , Y10S977/734 , Y10S977/737 , Y10S977/738
摘要： Drilling fluids comprising graphenes and nanoplatelet additives and methods for production thereof are disclosed. Graphene includes graphite oxide, graphene oxide, chemically-converted graphene, and functionalized chemically-converted graphene. Derivatized graphenes and methods for production thereof are disclosed. The derivatized graphenes are prepared from a chemically-converted graphene through derivatization with a plurality of functional groups. Derivatization can be accomplished, for example, by reaction of a chemically-converted graphene with a diazonium species. Methods for preparation of graphite oxide are also disclosed.
摘要翻译：公开了包含石墨烯和纳米片添加剂的钻井液及其生产方法。石墨烯包括氧化石墨，氧化石墨烯，化学转化的石墨烯和官能化的化学转化的石墨烯。衍生化的石墨烯及其生产方法被公开。衍生的石墨烯由化学转化的石墨烯通过用多个官能团衍生化来制备。衍生化可以通过例如化学转化的石墨烯与重氮化合物的反应来完成。还公开了用于制备氧化石墨的方法。

5. 发明申请

WO2012094045A3 LAYER-BY-LAYER REMOVAL OF GRAPHENE 审中-公开
标题翻译：逐层去除石墨
公开(公告)号：WO2012094045A3
公开(公告)日：2014-04-03
申请号：PCT/US2011055747
申请日：2011-10-11
申请人： UNIV RICE WILLIAM M , TOUR JAMES M , DIMIEV AYRAT M , KOSYNKIN DMITRY V
发明人： TOUR JAMES M , DIMIEV AYRAT M , KOSYNKIN DMITRY V
IPC分类号： B32B9/00
CPC分类号： C01B31/0484 , B82Y30/00 , B82Y40/00 , C01B32/182 , C01B32/19 , C01B32/192 , C01B32/194 , H01L21/30604 , H01L21/3085
摘要： The present invention provides methods of selectively removing one or more graphene layers from a graphene material by: (1) applying a metal to a surface of the graphene material; and (2) applying a hydrogen containing solution to the surface of the graphene material that is associated with the metal. The hydrogen containing solution dissolves the metal along with one or more layers of graphene associated with the metal, thereby removing the layer(s) of graphene from the graphene material. In some embodiments, the hydrogen containing solution is an acidic solution, such as hydrochloric acid. In some embodiments, the metal is zinc. In some embodiments, the methods of the present invention are utilized to selectively remove one or more layers of graphene from one or more targeted sites on the surface of a graphene material.
摘要翻译：本发明提供了通过以下步骤从石墨烯材料中选择性地去除一个或多个石墨烯层的方法：（1）将金属施加到石墨烯材料的表面; 和（2）将含氢溶液施加到与金属相关联的石墨烯材料的表面。含氢溶液与一个或多个与金属相关的石墨烯层一起溶解金属，从而从石墨烯材料去除石墨烯层。在一些实施方案中，含氢溶液是酸性溶液，例如盐酸。在一些实施方案中，金属是锌。在一些实施方案中，本发明的方法用于从石墨烯材料表面上的一个或多个目标位点选择性地除去一层或多层石墨烯。

6. 发明申请

WO2005085132A2 AMPLIFICATION OF CARBON NANOTUBES VIA SEEDED-GROWTH METHODS 审中-公开
标题翻译：碳纳米管通过种子生长方法的放大
公开(公告)号：WO2005085132A2
公开(公告)日：2005-09-15
申请号：PCT/US2004034002
申请日：2004-10-14
申请人： UNIV RICE WILLIAM M , SMALLEY RICHARD E , HAUGE ROBERT H , BARRON ANDREW R , TOUR JAMES M , SCHMIDT HOWARD K , BILLUPS W EDWARD , DYKE CHRISTOPHER A , MOORE VALERIE C , WHITSITT ELIZABETH , ANDERSON ROBIN A , COLORADO RAMON JR , STEWART MICHAEL , OGRIN DOUGLAS C
发明人： SMALLEY RICHARD E , HAUGE ROBERT H , BARRON ANDREW R , TOUR JAMES M , SCHMIDT HOWARD K , BILLUPS W EDWARD , DYKE CHRISTOPHER A , MOORE VALERIE C , WHITSITT ELIZABETH , ANDERSON ROBIN A , COLORADO RAMON JR , STEWART MICHAEL , OGRIN DOUGLAS C
IPC分类号： B01J23/881 , B01J27/22 , C01B3/00 , C01B31/00 , C01B31/02
CPC分类号： B82Y40/00 , B01J23/881 , B01J27/22 , B82Y30/00 , C01B3/0021 , C01B32/162 , C01B32/172 , C01B32/176 , C01B2202/02 , C01B2202/04 , C01B2202/06 , C01B2202/36 , Y02E60/325
摘要： The present invention is directed towards methods (processes) of providing large quantities of carbon nanotubes (CNTs) of defined diameter and chirality (i.e., precise populations). In such processes, CNT seeds of a pre-selected diameter and chirality are grown to many (e.g., hundreds) times their original length. This is optionally followed by cycling some of the newly grown material back as seed material for regrowth. Thus, the present invention provides for the large-scale production of precise populations of CNTs, the precise composition of such populations capable of being optimized for a particular application (e.g., hydrogen storage). The present invention is also directed to complexes of CNTs and transition metal catalyst precurors, such complexes typically being formed en route to forming CNT seeds.
摘要翻译：本发明涉及提供大量具有规定直径和手性（即精确群体）的碳纳米管（CNT）的方法（方法）。在这种方法中，预先选择的直径和手性的CNT种子生长到其原始长度的许多（例如，数百）倍。随后可以将一些新生成的材料循环回种子材料再生。因此，本发明提供了大规模生产精确的碳纳米管群体，能够针对特定应用（例如，氢存储）优化的这些群体的精确组成。本发明还涉及CNT和过渡金属催化剂前体的复合物，这些络合物通常在形成CNT晶种途中形成。

7. 发明申请

WO2005030858A3 POLYMERIZATION INITIATED AT THE SIDEWALLS OF CARBON NANOTUBES 审中-公开
标题翻译：碳纳米管的开发聚合
公开(公告)号：WO2005030858A3
公开(公告)日：2005-06-23
申请号：PCT/US2004019769
申请日：2004-06-21
申请人： UNIV RICE WILLIAM M , UNIV HOUSTON , TOUR JAMES M , HUDSON JARED L , KRISHNAMOORTI RAMANAN , YURELKI KORAY , MITCHELL CYNTHIA A
发明人： TOUR JAMES M , HUDSON JARED L , KRISHNAMOORTI RAMANAN , YURELKI KORAY , MITCHELL CYNTHIA A
IPC分类号： C01B31/02 , C08F292/00 , C08K3/04 , C08K7/06 , C08K7/24
CPC分类号： C08F4/484 , B82Y30/00 , B82Y40/00 , C01B32/174 , C01B2202/02 , C08F2/00 , C08F112/08 , C08F292/00 , C08K3/041 , C08K9/04 , C08L67/04
摘要： The present invention is directed to aryl halide (such as aryl bromide) functionalized carbon nanotubes can be utilized in anionic polymerization processes to form polymer-carbon nanotube materials with improved dispersion ability in polymer matrices. In this process the aryl halide is reacted with an alkyllithium species or is reacted with a metal to replace the aryl-bromine bond with an aryl-lithium or aryl-metal bond, respectively. It has further been discovered that other functionalized carbon nanotubes, after deprotonation with a deprotonation agent, can similarly be utilized in anionic polymerization processes to form polymer-carbon nanotube materials. Additionally or alternatively, a ring opening polymerization process can be performed. The resultant materials can be used by themselves due to their enhanced strength and reinforcement ability when compared to their unbound polymer analogs. Additionally, these materials can also be blended with pre-formed polymers to establish compatibility and enhanced dispersion of nanotubes in otherwise hard to disperse matrices resulting in significantly improved material properties. The resultant polymer-carbon nanotube materials can also be used in drug delivery processes due to their improved dispersion ability and biodegradability, and can also be used for scaffolding to promote cellular growth of tissue.
摘要翻译：本发明涉及芳基卤化物（例如芳基溴化物）官能化碳纳米管可以用于阴离子聚合方法以形成具有改进的聚合物基质分散能力的聚合物 - 碳纳米管材料。在该方法中，芳基卤化物与烷基锂物质反应，或与金属反应，分别用芳基 - 锂或芳基 - 金属键代替芳基 - 溴键。还已经发现，其它官能化碳纳米管在去质子化脱质子化之后，可以类似地用于阴离子聚合方法中以形成聚合物 - 碳纳米管材料。另外或者可选地，可以进行开环聚合方法。所得材料由于与未结合的聚合物类似物相比具有增强的强度和增强能力，可以自己使用。另外，这些材料也可以与预先形成的聚合物混合以建立纳米管在其它难分散的基质中的相容性和增强的分散，导致显着改善的材料性质。所得聚合物 - 碳纳米管材料由于其分散能力和生物降解性的改善而可用于药物递送过程中，并且也可用于支架以促进组织的细胞生长。

8. 发明申请

WO2004068497A3 SELF-ASSEMBLY OF MOLECULES AND NANOTUBES AND/OR NANOWIRES IN NANOCELL COMPUTING DEVICES, AND METHODS FOR PROGRAMMING SAME 审中-公开
标题翻译： NANOCELL计算设备中的分子和纳米体系和/或纳米单体的自组装及其编程方法
公开(公告)号：WO2004068497A3
公开(公告)日：2004-12-29
申请号：PCT/US2004002266
申请日：2004-01-28
申请人： UNIV RICE WILLIAM M , TOUR JAMES M , CHENG LONG , FRANZON PAUL D , NACKASHI DAVID
发明人： TOUR JAMES M , CHENG LONG , FRANZON PAUL D , NACKASHI DAVID
IPC分类号： G11C13/02 , H01L27/28 , H01L51/00 , H01L51/30 , G11C11/00 , G11C27/00 , H01L29/00 , H01L35/40
CPC分类号： G11C13/025 , B82Y10/00 , G11C13/0014 , H01L27/28 , H01L51/0048 , H01L51/005 , H01L51/0052 , H01L51/0595
摘要： An assembly of a NanoCell comprising a disordered array of metallic islands interlinked with molecules between metallic input/output leads and with disordered arrays of molecules and Au islands is disclosed. The NanoCell may function both as a memory device that is programmable post-fabrication. The assembled NanoCells exhibit reproducible switching behavior and at least two types of memory effects at room temperature. The switch-type memory is characteristic of a destructive read while the conductivity-type memory features a nondestructive read. Both types of s memory effects are stable for more than a week at room temperature and bit level ratios (0:1) of the conductivity-type memory have been observed to be as high as 10 :1 and reaching 10 :1 upon ozone treatment which likely destroys extraneous leakage pathways. The invention demonstrates the efficacy of a disordered nano-scale array for high-yielding switching and memory while mitigating the arduous task of nano-scale patterning.
摘要翻译：公开了包含与金属输入/输出引线之间的分子互连并且具有无序的分子阵列和Au岛的金属岛的无序阵列的纳米晶体组件。 NanoCell可以兼作可编程后期制作的存储器件。组装的NanoCells在室温下表现出可重现的切换行为和至少两种记忆效应。开关型存储器是具有破坏性读取的特征，而导电型存储器具有非破坏性读取。两种类型的记忆效应在室温下稳定超过一周，并且观察到导电型存储器的位电平比（0：1）高达10 4：1并达到10 <6 > 1：臭氧处理可能会破坏外部泄漏通道。本发明证明了无序纳米尺度阵列在高产量切换和记忆方面的功效，同时减轻了纳米尺度图案的艰巨任务。

9. 发明申请

WO2008054836A2 SHORT, FUNCTIONALIZED, SOLUBLE CARBON NANOTUBES, METHODS OF MAKING SAME, AND POLYMER COMPOSITES MADE THEREFROM 审中-公开
标题翻译：短功能化，可溶性碳纳米管，其制备方法及其制备的聚合物复合材料
公开(公告)号：WO2008054836A2
公开(公告)日：2008-05-08
申请号：PCT/US2007062570
申请日：2007-02-22
申请人： UNIV RICE WILLIAM M , HWANG WEN-FANG , CHEN ZHEYI , TOUR JAMES M
发明人： HWANG WEN-FANG , CHEN ZHEYI , TOUR JAMES M
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/174 , C01B32/176 , C01B2202/02 , C01B2202/28
摘要： In some embodiments, the present invention relates to new processes to simultaneously shorten and functionalize raw or purified carbon nanotubes to improve their dispersity and processibility, and the short functionalized nanotubes that may be made by the processes. This present invention also relates to new compositions of matter using short functionalized carbon nanotubes with thermoset, thermoplastic polymers, high temperature polymers, and other materials; the processes for making such composite materials; and the products of said processes.
摘要翻译：在一些实施方案中，本发明涉及同时缩短和官能化原始或纯化的碳纳米管以提高其分散性和可加工性的新方法，以及可通过该方法制备的短官能化纳米管。本发明还涉及使用具有热固性，热塑性聚合物，高温聚合物和其它材料的短官能化碳纳米管的物质的新组合物; 制造这种复合材料的方法; 和所述方法的产品。

10. 发明申请

WO2005114708A3 CARBON NANOTUBE-SILICON COMPOSITE STRUCTURES AND METHODS FOR MAKING SAME 审中-公开
标题翻译：碳纳米管 - 硅复合结构及其制备方法
公开(公告)号：WO2005114708A3
公开(公告)日：2006-07-20
申请号：PCT/US2005016102
申请日：2005-05-06
申请人： UNIV RICE WILLIAM M , TOUR JAMES M , DYKE CHRISTOPHER A , MAYA FRANCISCO , STEWART MICHAEL , CHEN BO , FLATT AUSTEN K
发明人： TOUR JAMES M , DYKE CHRISTOPHER A , MAYA FRANCISCO , STEWART MICHAEL , CHEN BO , FLATT AUSTEN K
IPC分类号： H01L51/30 , C01B31/02 , H01L21/00
CPC分类号： B82Y30/00 , B82Y10/00 , H01L51/0048 , Y10S977/847 , Y10S977/892
摘要： The present invention is directed toward methods of attaching or grafting carbon nanotubes (CNTs) to silicon , wherein such attaching or grafting occurs via functional groups on either or both of the CNTs and silicon surface. The present invention is also directed to the novel compositions produced by such methods. In some embodiments, the present invention is directed to afford the covalent attachment of individualized (unroped) SWNTs to Si surfaces.
摘要翻译：本发明涉及将碳纳米管（CNT）附着或接枝到硅上的方法，其中通过碳纳米管和硅表面中的任一个或两者上的官能团进行这种附着或接枝。本发明还涉及通过这些方法制备的新型组合物。在一些实施方案中，本发明旨在提供个体化（未经处理的）SWNT与Si表面的共价连接。

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