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1. 发明申请

WO2005082518A2 SWELL CONTROL IN SLURRY LOOP REACTOR 审中-公开
标题翻译：在浆料循环反应器中的膨胀控制
公开(公告)号：WO2005082518A2
公开(公告)日：2005-09-09
申请号：PCT/EP2005/050519
申请日：2005-02-08
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , FOUARGE, Louis , LEWALLE, André , VAN DER AUWERA, Marc , VAN DEN BRANDE, Frans
发明人： FOUARGE, Louis , LEWALLE, André , VAN DER AUWERA, Marc , VAN DEN BRANDE, Frans
IPC分类号： B01J19/00
CPC分类号： B01J19/1837 , B01J19/002 , B01J2219/00094 , B01J2219/002 , B01J2219/00216 , B01J2219/00229 , B01J2219/00254 , C08F10/00 , C08F2/00
摘要： The present invention discloses a method for controlling the onset and development of swelling in a slurry loop reactor by progressively diluting the reactor, the amount of dilution being driven by the amplitude of the fluctuations measured on some plant measurement.
摘要翻译：本发明公开了一种通过逐渐稀释反应器来控制浆液环流反应器中溶胀的发生和发展的方法，稀释量由在某些设备测量中测得的波动幅度驱动

2. 发明申请

WO2005080439A2 SURFACE FINISH OF REACTOR 审中-公开
标题翻译：反应器的表面光洁度
公开(公告)号：WO2005080439A2
公开(公告)日：2005-09-01
申请号：PCT/EP2005/050520
申请日：2005-02-08
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , FOUARGE, Louis , VAN DER AUWERA, Marc
发明人： FOUARGE, Louis , VAN DER AUWERA, Marc
IPC分类号： C08F2/00
CPC分类号： C08F10/00 , C08F110/02 , C08F2/002
摘要： This invention discloses the use in the production of a polyolefin of a slurry loop reactor wherein all internal parts in contact with the slurry are polished first by a mechanical process to a level of at most 70 RMS roughness value and are subsequently polished by a chemical or electrochemical process, to a final level of at most 40 RMS roughness value.
摘要翻译：本发明公开了在淤浆环路反应器的聚烯烃的生产中的用途，其中与淤浆接触的所有内部部件首先通过机械工艺抛光至最高70 RMS RMS粗糙度值并随后通过化学或电化学过程抛光至最高40 RMS RMS值。

3. 发明申请

WO2012013804A1 PUMP FOR LOOP REACTOR 审中-公开
标题翻译：泵反循环泵
公开(公告)号：WO2012013804A1
公开(公告)日：2012-02-02
申请号：PCT/EP2011/063146
申请日：2011-07-29
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , TIMMERMANS, Frank , OOMS, Wouter , DEWACHTER, Daan , FOUARGE, Louis
发明人： TIMMERMANS, Frank , OOMS, Wouter , DEWACHTER, Daan , FOUARGE, Louis
IPC分类号： B01J19/18 , C08F2/01
CPC分类号： B01J19/1875 , B01J19/1837 , C08F10/02 , C08F110/02 , F04D3/00 , F04D29/181 , C08F2/14 , C08F2/01 , C08F2500/05 , C08F2500/24
摘要： The present invention relates the use of a pump in a loop reactor for the production of polyethylene, as well as a reactor comprising such pump and methods for producing polyolefin by means of such reactor. The pump according to the invention is characterized in that it is an axial flow impeller circulation pump, wherein the impeller comprises 6 blades and wherein the pump is fixed on a spring supported frame. Use of the pump according to the present invention allows for preparation of homogeneous polyethylene products that meet high quality standards from the complicated ethylene polymerization mixtures while at the same time being produced with low energy consumption.
摘要翻译：本发明涉及在用于生产聚乙烯的环管式反应器中的泵的使用，以及包括这种泵的反应器和通过这种反应器生产聚烯烃的方法。根据本发明的泵的特征在于它是轴流式叶轮循环泵，其中叶轮包括6个叶片，并且其中泵固定在弹簧支撑的框架上。根据本发明的泵的使用允许制备符合来自复杂乙烯聚合混合物的高质量标准的同质聚乙烯产品，同时以低能量消耗生产。

4. 发明申请

WO2005082980A2 ADDITIVISING POLYMER POWDERS 审中-公开
标题翻译：添加聚合物粉末
公开(公告)号：WO2005082980A2
公开(公告)日：2005-09-09
申请号：PCT/EP2005/050561
申请日：2005-02-09
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , FOUARGE, Louis , D'HOOGHE, Leo , SILLIS, Marjan
发明人： FOUARGE, Louis , D'HOOGHE, Leo , SILLIS, Marjan
IPC分类号： C08J3/20
CPC分类号： C08J3/2053
摘要： The invention provides an apparatus for introducing additives onto a polymer powder. It also provides a method for introducing an additive into a polyolefin powder, which method comprises the following steps: (a) adding the additive in a solvent to form a solution; and (b) introducing the solution to the polymer powder at a temperature of 60°C or more, wherein, the solution is introduced to the polymer powder by spraying via a heated spraying means.
摘要翻译：本发明提供了一种将添加剂引入聚合物粉末的装置。它还提供了一种将添加剂引入聚烯烃粉末中的方法，该方法包括以下步骤：（a）将添加剂加入溶剂中形成溶液; 和（b）在60℃以上的温度下将溶液引入到聚合物粉末中，其中，通过经过加热的喷涂方法喷雾将溶液引入聚合物粉末中。

5. 发明申请

WO2007096380A1 METHOD FOR TRANSFORMING A LOOP REACTOR 审中-公开
标题翻译：环流反应器的改造方法
公开(公告)号：WO2007096380A1
公开(公告)日：2007-08-30
申请号：PCT/EP2007/051659
申请日：2007-02-21
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , FOUARGE, Louis , DUCHESNE, Eric
发明人： FOUARGE, Louis , DUCHESNE, Eric
IPC分类号： B01J19/18 , B01J8/22 , C08F10/02 , C08F2/14 , C08F2/01
CPC分类号： C08F2/01 , B01J8/007 , B01J19/1818 , B01J19/1837 , B01J2208/00176 , B01J2208/00619 , B01J2219/00024 , B01J2219/00031 , B01J2219/00033 , B01J2219/0004 , B01J2219/00094 , B01J2219/00184 , B01J2219/00254 , C08F10/02 , C08F110/02 , C08F210/16 , Y10T29/49716 , C08F2/14 , C08F210/14 , C08F2/001
摘要： The present invention discloses a method for transforming a single reactor line into a double reactor line wherein the existing single reactor line is equipped with a flash tank for separating the solid polymer product from the flash vapour and wherein the vapour is sent to a system of at least two separating columns allowing the separation of its constituents into monomer, diluent and comonomer.
摘要翻译：本发明公开了一种用于将单个反应器管线转化为双重反应器管线的方法，其中现有的单个反应器管线装备有用于将固体聚合物产物与闪蒸蒸气分离的闪蒸罐，并且其中蒸气被送至系统最少两个分离柱允许其组分分离成单体，稀释剂和共聚单体。

6. 发明申请

WO2005077522A1 METHOD AND APPARATUS FOR PREPARING AND SUPPLYING CATALYST SLURRY TO A POLYMERISATION REACTOR. 审中-公开
标题翻译：制备和提供催化剂浆料到聚合反应器的方法和装置。
公开(公告)号：WO2005077522A1
公开(公告)日：2005-08-25
申请号：PCT/EP2005/050625
申请日：2005-02-14
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , FOUARGE, Louis
发明人： FOUARGE, Louis
IPC分类号： B01J19/00
CPC分类号： B01J8/0035 , B01J8/003 , B01J8/007 , B01J8/226 , B01J2208/00212 , B01J2208/00557 , B01J2208/00619 , B01J2208/00752 , C08F10/02 , C08F110/02 , Y10S526/919 , Y10T137/8593 , C08F2/01 , C08F2500/05
摘要： The present invention relates to an apparatus for preparing and supplying catalyst to an ethylene slurry loop polymerisation reactor and to an apparatus for controlling the injection of catalyst slurry in a polymerization reactor wherein polyethylene is prepared. The present invention a Iso relates to a method for optimising catalyst supply to a polymerisation reactor. The diluted catalyst is transferred to the reactor (1) using a membrane pump (5) controllable in function of the concentration of a reactant in said reactor (1).
摘要翻译：本发明涉及一种用于制备和供应催化剂到乙烯浆料回路聚合反应器的装置，以及用于控制在聚合反应器中注入催化剂浆料的装置，其中制备聚乙烯。本发明的Iso涉及一种优化催化剂供应到聚合反应器的方法。使用可在所述反应器（1）中反应物浓度可控的膜泵（5）将稀释的催化剂转移到反应器（1）中。

7. 发明申请

WO2012013802A1 PRESSURE CONTROL OF THE CATALYST MIXING VESSEL 审中-公开
标题翻译：催化混合容器的压力控制
公开(公告)号：WO2012013802A1
公开(公告)日：2012-02-02
申请号：PCT/EP2011/063143
申请日：2011-07-29
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , BRUSSELLE, Alain , DEWACHTER, Daan , FOUARGE, Louis
发明人： BRUSSELLE, Alain , DEWACHTER, Daan , FOUARGE, Louis
IPC分类号： C08F10/02 , C08F2/01 , C08F2/14
CPC分类号： G05D16/02 , B01J8/0035 , B01J8/20 , B01J2219/00162 , C08F4/76 , C08F10/02 , C08F2/14 , C08F2/01
摘要： The present invention relates to a process for preparing catalyst slurry in a catalyst slurry preparation system and supplying catalyst slurry to an ethylene polymerization loop reactor wherein an accurate control of the pressure within said catalyst slurry preparation system is provided. More particularly, the present invention provides a method for preparing a catalyst slurry and supplying said catalyst slurry to an ethylene polymerization loop reactor, said catalyst slurry comprising solid catalyst and a liquid hydrocarbon diluent, wherein said method comprises the steps of: (a) feeding concentrated catalyst slurry to a mixing vessel by means of a feeding device; (b) diluting said concentrated catalyst slurry in a suitable amount of said diluent in a mixing vessel thereby obtaining a diluted catalyst slurry having a concentration suitable for use in an ethylene polymerization reaction; wherein said mixing vessel is provided with at least one pressure regulating unit connected therewith and wherein said pressure regulating unit comprises a pulsation dampener; and (c) transferring said diluted catalyst slurry from said mixing vessel to said ethylene polymerization loop reactor; characterized in that the method comprises the step of maintaining said mixing vessel essentially free of a gaseous phase by regulating the pressure in said mixing vessel using said at least one pressure regulating unit comprising the pulsation dampener.
摘要翻译：本发明涉及一种在催化剂浆料制备系统中制备催化剂浆料并将催化剂浆料供应到乙烯聚合反应器中的方法，其中提供了所述催化剂浆料制备系统内的压力的精确控制。更具体地说，本发明提供了一种制备催化剂浆料并将所述催化剂浆料供应到乙烯聚合反应器的方法，所述催化剂浆料包括固体催化剂和液体烃稀释剂，其中所述方法包括以下步骤：（a）浓缩的催化剂浆料通过进料装置进入混合容器; （b）将所述浓缩催化剂浆液在合适量的稀释剂中稀释在混合容器中，由此获得具有适合用于乙烯聚合反应的浓度的稀释催化剂浆料; 其中所述混合容器设置有与其连接的至少一个压力调节单元，并且其中所述压力调节单元包括脉动阻尼器; 和（c）将所述稀释的催化剂浆料从所述混合容器转移到所述乙烯聚合反应器中; 其特征在于，所述方法包括通过使用包括脉动阻尼器的所述至少一个压力调节单元来调节所述混合容器中的压力来维持所述混合容器基本上不含气相的步骤。

8. 发明申请

WO2012013797A1 USE OF A CATALYST SLURRY PREPARATION SYSTEM 审中-公开
标题翻译：使用催化剂浆液制备系统
公开(公告)号：WO2012013797A1
公开(公告)日：2012-02-02
申请号：PCT/EP2011/063136
申请日：2011-07-29
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , BRUSSELLE, Alain , FOUARGE, Louis
发明人： BRUSSELLE, Alain , FOUARGE, Louis
IPC分类号： C08F2/00 , B01J8/00
CPC分类号： C08F10/02 , B01F7/00633 , B01F7/1675 , B01F7/22 , B01F13/0827 , B01F13/0836 , B01F13/0845 , B01J8/002 , B01J8/0035 , C08F4/00 , C08F4/65912 , C08F4/65927 , C08F10/00 , C08F4/65916
摘要： The present invention relates to the use of a catalyst preparation system for the preparation of a diluted catalyst slurry. In particular, the invention relates to a catalyst preparation system comprising a mixing vessel for mixing a particulate catalyst and a liquid hydrocarbon diluent. According to the invention, diluted catalyst slurry is prepared in a mixing vessel comprising a rotatable axial impeller system comprising at least two double-bladed hubs. The invention also relates to a process for preparing diluted catalyst slurry for use in the preparation of a particulate polyethylene product in a loop reactor with the catalyst preparation system as described herein.
摘要翻译：本发明涉及催化剂制备系统用于制备稀释催化剂浆料的用途。特别地，本发明涉及一种催化剂制备系统，其包括用于混合颗粒催化剂和液体烃稀释剂的混合容器。根据本发明，稀释的催化剂浆料在混合容器中制备，该混合容器包括可旋转的轴流式叶轮系统，其包括至少两个双叶片轮毂。本发明还涉及一种用于制备稀释的催化剂浆料的方法，所述稀释的催化剂浆料用于在具有如本文所述的催化剂制备系统的环管反应器中制备颗粒状聚乙烯产品。

9. 发明申请

WO2007096381A1 TRANSFER PIPE BETWEEN LOOP REACTORS 审中-公开
标题翻译：环流反应器之间的转移管
公开(公告)号：WO2007096381A1
公开(公告)日：2007-08-30
申请号：PCT/EP2007/051660
申请日：2007-02-21
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , FOUARGE, Louis
发明人： FOUARGE, Louis
IPC分类号： B01J19/18 , C08F10/00 , B01J8/00 , B01J4/00
CPC分类号： B01J4/008 , B01J19/1837 , B01J2219/0004 , B01J2219/00166 , B01J2219/00184 , B01J2219/00254
摘要： The present invention discloses a transfer system between the first and second reactors in a double loop reactor that is equipped to reduce clogging in the transfer lines by providing a regulation mechanism arranged to insure equivalent flushing in each transfer line.
摘要翻译：本发明公开了一种双回路反应器中的第一和第二反应器之间的转移系统，该双回路反应器装备有通过设置用于确保每个输送管线中的等效冲洗的调节机构来减少输送管线中的堵塞。

10. 发明申请

WO2005080443A3 SLURRY LOOP REACTORS 审中-公开
公开(公告)号：WO2005080443A3
公开(公告)日：2005-09-01
申请号：PCT/EP2005/050531
申请日：2005-02-08
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , FOUARGE, Louis , VAN CAMP, Carl
发明人： FOUARGE, Louis , VAN CAMP, Carl
IPC分类号： C08F2/14
摘要： An apparatus defined as a set of loop reactors suitable for the polymerization process of a monomer, preferably ethylene and optionally an olefin comonomer, comprising for each of said reactors: a plurality of interconnected pipes P defining a flow path for a polymer slurry, said slurry consisting essentially of ethylene, optionally a comonomer, a polymerization catalyst, liquid diluent and solid olefin polymer particles, means for feeding monomer, optionally a co-monomer, diluent and optionally hydrogen in the reactor, means for feeding a polymerization catalyst in the reactor, a pump suitable for maintaining the polymer slurry in circulation in such reactor, one or more settling legs connected to the pipes P of such reactor for settling of polymer slurry, one or more control valves connected to the outlet of such settling legs, and one or more flash lines for discharging settled polymer slurry out of the reactor characterized in that each of said loop reactors comprises a three-or-more-way valve defining three-or-more ends, one end A being positioned at the outlet of said one or more control valves. A method to switch from series to parallel configuration a set of loop reactors. The use of the apparatus to switch polymerization reactors from parallel to series configuration and vice-versa.

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