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1. 发明申请

WO2012119954A1 PROCESS FOR PREPARING POLYETHYLENE BLEND COMPRISING METALLOCENE PRODUCED RESINS AND ZIEGLER-NATTA PRODUCED RESINS 审中-公开
标题翻译：用于制备包含金属生产树脂和齐格勒 - 生产树脂的聚乙烯混合物的方法
公开(公告)号：WO2012119954A1
公开(公告)日：2012-09-13
申请号：PCT/EP2012/053658
申请日：2012-03-02
申请人： TOTAL RESEARCH & TECHNOLOGY FELUY , DEWACHTER, Daan , DAMME, Eric
发明人： DEWACHTER, Daan , DAMME, Eric
IPC分类号： C08L23/06
CPC分类号： C08L23/06 , C08F110/02 , C08L23/04 , C08L23/0815 , C08L2205/02 , C08L2205/025 , C08L2314/02 , C08L2314/06 , C08L2666/06 , C08F2500/12 , C08F2500/24
摘要： The invention relates to a process for preparing a homogeneous polyethylene product, said process comprising the steps of: (a) producing a first polyethylene resin in the presence of a metallocene catalyst in a reactor, said first polyethylene resin having a density of from 0.940 to 0.970 g/cm 3 , with the density being determined with the ASTM D-1505 standardized test at a temperature of 23°C and wherein the first polyethylene resin has Low Molecular Weight (LMW) with a Ml2 of between 2 and 250 g/10 min, with the Melt Index Ml 2 being measured by the procedure of ASTM D-1238 using a temperature of 190°C and a load of 2.16 kg; (b) separately producing a second polyethylene resin in the presence of a Ziegler- Natta catalyst in a reactor, wherein the second polyethylene resin has High Molecular Weight (HMW) with a Ml 2 of between 0.01 and 15 g/10 min; and (c) physically blending together said first and said second polyethylene resin to produce the polyethylene product.
摘要翻译：本发明涉及一种制备均匀聚乙烯产品的方法，所述方法包括以下步骤：（a）在茂金属催化剂存在下在反应器中制备第一聚乙烯树脂，所述第一聚乙烯树脂的密度为0.940至 0.970g / cm 3，其密度通过ASTM D-1505标准化试验在23℃的温度下测定，其中第一聚乙烯树脂具有2M2 / 250g / 10min之间的低分子量（LMW）熔体指数M12通过ASTM D-1238的程序使用190℃的温度和2.16kg的负荷来测量; （b）在齐格勒 - 纳塔催化剂存在下，在反应器中分别生产第二聚乙烯树脂，其中所述第二聚乙烯树脂具有高分子量（HMW），M 21为0.01至15g / 10min; 和（c）将所述第一和第二聚乙烯树脂物理混合在一起以制备聚乙烯产品。

2. 发明申请

WO2012013795A1 METHOD FOR METERING A CATALYST SLURRY 审中-公开
标题翻译：测量催化剂浆料的方法
公开(公告)号：WO2012013795A1
公开(公告)日：2012-02-02
申请号：PCT/EP2011/063133
申请日：2011-07-29
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , DEWACHTER, Daan , BEKAERT, Daniel
发明人： DEWACHTER, Daan , BEKAERT, Daniel
IPC分类号： F16K25/00 , F16K27/00 , B01J8/00
CPC分类号： B01J8/001 , B01J8/0015 , B01J2204/002 , B01J2208/00752 , F17D3/00 , Y10T137/0318
摘要： The invention relates to a catalyst metering device with a valve formed of an iron-based alloy steel hardened to a Rockwell hardness C of at least 60. The device can be used for metering of a catalyst for an ethylene polymerization reaction. The invention further relates to ethylene polymerization wherein the catalyst is metered in a catalyst metering device with a iron-based alloy steel hardened valve, as well as to a ethylene polymerization reactor comprising such a catalyst metering device.
摘要翻译：本发明涉及一种具有由硬化至洛氏硬度C至少为60的铁基合金钢形成的阀的催化剂计量装置。该装置可用于计量用于乙烯聚合反应的催化剂。本发明还涉及乙烯聚合，其中催化剂在具有铁基合金钢硬化阀的催化剂计量装置中以及包含这种催化剂计量装置的乙烯聚合反应器中计量。

3. 发明申请

WO2007076996A1 DYNAMIC PRESSURE CONTROL IN DOUBLE LOOP REACTOR 审中-公开
标题翻译：双环反应器动态压力控制
公开(公告)号：WO2007076996A1
公开(公告)日：2007-07-12
申请号：PCT/EP2006/012534
申请日：2006-12-27
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY PATENT DEPARTMENT , DEWACHTER, Daan , FOUARGE, Louis , BRUSSELLE, Alain
发明人： DEWACHTER, Daan , FOUARGE, Louis , BRUSSELLE, Alain
IPC分类号： B01J19/18 , B01J8/00 , C08F10/00
CPC分类号： C08F2/001 , B01J8/007 , B01J19/1837 , B01J19/1881 , B01J2219/00033 , B01J2219/0004 , B01J2219/00094 , B01J2219/00166 , C08F10/00 , C08F110/02 , C08F110/06 , C08F2/01
摘要： The present invention discloses a slurry loop reactor comprising at least two loop reactors connected in series and wherein the line connecting the two loops is subject to a dynamic pressure difference.
摘要翻译：本发明公开了一种包含至少两个串联连接的回路反应器的浆液回路反应器，其中连接两个回路的管线经受动压差。

4. 发明申请

WO2013110322A1 METHOD FOR PROCESSING POLYETHYLENE 审中-公开
标题翻译：加工聚乙烯的方法
公开(公告)号：WO2013110322A1
公开(公告)日：2013-08-01
申请号：PCT/EP2012/051043
申请日：2012-01-24
申请人： TOTAL RESEARCH & TECHNOLOGY FELUY , STEVENS, Peter , FANT, Franky , DEWACHTER, Daan , BRUSSELLE, Alain
发明人： STEVENS, Peter , FANT, Franky , DEWACHTER, Daan , BRUSSELLE, Alain
IPC分类号： C08F10/00 , C08F2/02 , B01J19/18
CPC分类号： C08J3/203 , B29B9/06 , B29C47/0004 , B29C47/0011 , B29C47/0066 , C08J3/00 , C08J2323/06 , C08J2323/16 , C08J2423/06
摘要： Method for consecutively batch processing at least two different polyethylene grades in pellet form in a pellet handling unit, comprising the steps of consecutively batch processing at least two different polyethylene grades in pellet form in a pellet handling unit, wherein the ratio of the melt flow index (MI) of a first polyethylene in pellet form (MI f ) to the MI of a later processed polyethylene in pellet form (MI l ) is smaller than 0.30, and comprising the step of processing an intermediate polyethylene grade in pellet form, wherein the amount of intermediate polyethylene grade processed is at most 1/100 th of the handling capacity of the pellet handling unit, and wherein said intermediate polyethylene grade has the same MI than said later processed polyethylene in pellet form.
摘要翻译：在丸粒处理单元中连续批处理至少两种不同聚乙烯粒度聚乙烯等级的方法，包括以下步骤：在颗粒处理单元中连续批处理至少两种颗粒形式的不同聚乙烯等级，其中熔体流动指数颗粒形式（MIf）的后处理聚乙烯的MI的颗粒形式（MIf）的第一聚乙烯的MI（MI）小于0.30，包括以颗粒形式加工中间聚乙烯等级的步骤中间聚乙烯等级加工量最多为颗粒处理单元的处理能力的1/100，其中所述中间聚乙烯等级具有与所述稍后加工的聚乙烯颗粒相同的MI。

5. 发明申请

WO2012013804A1 PUMP FOR LOOP REACTOR 审中-公开
标题翻译：泵反循环泵
公开(公告)号：WO2012013804A1
公开(公告)日：2012-02-02
申请号：PCT/EP2011/063146
申请日：2011-07-29
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , TIMMERMANS, Frank , OOMS, Wouter , DEWACHTER, Daan , FOUARGE, Louis
发明人： TIMMERMANS, Frank , OOMS, Wouter , DEWACHTER, Daan , FOUARGE, Louis
IPC分类号： B01J19/18 , C08F2/01
CPC分类号： B01J19/1875 , B01J19/1837 , C08F10/02 , C08F110/02 , F04D3/00 , F04D29/181 , C08F2/14 , C08F2/01 , C08F2500/05 , C08F2500/24
摘要： The present invention relates the use of a pump in a loop reactor for the production of polyethylene, as well as a reactor comprising such pump and methods for producing polyolefin by means of such reactor. The pump according to the invention is characterized in that it is an axial flow impeller circulation pump, wherein the impeller comprises 6 blades and wherein the pump is fixed on a spring supported frame. Use of the pump according to the present invention allows for preparation of homogeneous polyethylene products that meet high quality standards from the complicated ethylene polymerization mixtures while at the same time being produced with low energy consumption.
摘要翻译：本发明涉及在用于生产聚乙烯的环管式反应器中的泵的使用，以及包括这种泵的反应器和通过这种反应器生产聚烯烃的方法。根据本发明的泵的特征在于它是轴流式叶轮循环泵，其中叶轮包括6个叶片，并且其中泵固定在弹簧支撑的框架上。根据本发明的泵的使用允许制备符合来自复杂乙烯聚合混合物的高质量标准的同质聚乙烯产品，同时以低能量消耗生产。

6. 发明申请

WO2012013800A1 PROCESS FOR SUPPLYING CATALYST TO A POLYMERIZATION REACTOR 审中-公开
标题翻译：向聚合反应器供应催化剂的方法
公开(公告)号：WO2012013800A1
公开(公告)日：2012-02-02
申请号：PCT/EP2011/063140
申请日：2011-07-29
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , DEWACHTER, Daan , BRUSSELLE, Alain
发明人： DEWACHTER, Daan , BRUSSELLE, Alain
IPC分类号： B01J8/00 , C08F2/00
CPC分类号： F03B17/00 , B01J8/002 , B01J2208/00752 , C08F4/65916 , C08F10/00 , C08F210/16 , Y10S417/90 , Y10S526/919 , Y10T137/0318 , C08F2/14 , C08F2/01 , C08F210/14
摘要： The present invention relates to a method for feeding metallocene catalyst slurry to an olefin polymerization loop reactor (1) using a positive displacement device (5) comprising a first chamber (5-6) and a second chamber (5-3) each chamber having an outlet and each chamber comprising a ball arranged between the walls of said chamber, wherein said chambers are connected to each other by a pump chamber (5-2) operably connected to a pump, wherein the difference between the diameter of said ball and the diameter of said chamber is comprised between 5 to 200 times the average particle size (d50) of said catalyst.
摘要翻译：本发明涉及使用包括第一室（5-6）和第二室（5-3）的正位移装置（5）将茂金属催化剂浆料供给到烯烃聚合反应器（1）的方法，每个室具有出口和每个室包括布置在所述室的壁之间的球，其中所述室通过可操作地连接到泵的泵室（5-2）彼此连接，其中所述球的直径与所述室的直径为所述催化剂的平均粒度（d50）的5至200倍。

7. 发明申请

WO2012013794A1 PROCESS FOR PREPARING POLYOLEFINS 审中-公开
标题翻译：制备聚烯烃的方法
公开(公告)号：WO2012013794A1
公开(公告)日：2012-02-02
申请号：PCT/EP2011/063132
申请日：2011-07-29
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , SIRAUX, Daniel , VANTOMME, Aurélien , DAMME, Eric , DEWACHTER, Daan
发明人： SIRAUX, Daniel , VANTOMME, Aurélien , DAMME, Eric , DEWACHTER, Daan
IPC分类号： C08F10/00 , C08F2/02 , B01J19/18
CPC分类号： C08F2/01 , B01J4/001 , B01J8/007 , B01J19/1818 , B01J19/1837 , C08F210/16 , C08F2/005 , C08F2/14 , C08F210/14
摘要： The present invention relates to a process of preparing a polyolefin in a loop reactor by introducing anti-fouling agent through a sleeve provided around at least part of the shaft of the pump. Also, the invention relates to the use of anti-fouling agent to prevent or reduce fouling by feeding the anti-fouling agent against the impeller of the pump upon introduction to the loop reactor.
摘要翻译：本发明涉及一种在环管式反应器中制备聚烯烃的方法，该方法是通过在泵的至少一部分周围设置的套筒引入防污剂。此外，本发明涉及通过在引入环流反应器时将防污垢剂施加到泵的叶轮上来防止或减少结垢的用途。

8. 发明申请

WO2007076996A8 DYNAMIC PRESSURE CONTROL IN DOUBLE LOOP REACTOR 审中-公开
标题翻译：双环反应器动态压力控制
公开(公告)号：WO2007076996A8
公开(公告)日：2008-07-10
申请号：PCT/EP2006012534
申请日：2006-12-27
申请人： TOTAL PETROCHEMICALS RES FELUY , DEWACHTER DAAN , FOUARGE LOUIS , BRUSSELLE ALAIN
发明人： DEWACHTER DAAN , FOUARGE LOUIS , BRUSSELLE ALAIN
IPC分类号： B01J19/18 , B01J8/00 , C08F10/00
CPC分类号： C08F2/001 , B01J8/007 , B01J19/1837 , B01J19/1881 , B01J2219/00033 , B01J2219/0004 , B01J2219/00094 , B01J2219/00166 , C08F10/00 , C08F110/02 , C08F110/06 , C08F2/01
摘要： The present invention discloses a slurry loop reactor comprising at least two loop reactors connected in series and wherein the line connecting the two loops is subject to a dynamic pressure difference.
摘要翻译：本发明公开了一种包含至少两个串联连接的回路反应器的浆液回路反应器，其中连接两个回路的管线经受动压差。

9. 发明申请

WO2007113308A1 PROCESS FOR IMPROVING THE POLYMERIZATION OF ETHYLENE AND ONE OR MORE OPTIONAL CO-MONOMER(S) IN A POLYMERIZATION LOOP REACTOR 审中-公开
标题翻译：在聚合反应器中改善乙烯和一种或多种可选的共聚单体聚合的方法
公开(公告)号：WO2007113308A1
公开(公告)日：2007-10-11
申请号：PCT/EP2007/053272
申请日：2007-04-03
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , DEWACHTER, Daan
发明人： DEWACHTER, Daan
IPC分类号： C08F10/02 , C08F2/14 , B01J19/24
CPC分类号： B01J8/08 , B01J8/007 , B01J19/18 , B01J2219/00094 , B01J2219/00164 , C08F10/02 , C08F110/02 , C08F210/16 , C08F2/001 , C08F2/14 , C08F210/14
摘要： The present invention relates to a process for improving the polymerization of ethylene and one or more optional co-monomer(s) in a polymerization loop reactor characterized in that said process comprises the step of controlling the hydrogen/monomer ratio along the path of the reactor by multiple, spatially separated, feeding of hydrogen along the path of the loop reactor. In particular, the invention provides a process for controlling, and preferably narrowing, the molecular weight distribution of the produced polymer particles. In another aspect, the invention relates to a polymerization loop reactor suitable for the polymerization process of ethylene and an optional olefin co-monomer, wherein the molecular weight distribution of the produced ethylene polymer can be controlled.
摘要翻译：本发明涉及在聚合反应器反应器中改进乙烯和一种或多种任选的共聚单体聚合的方法，其特征在于所述方法包括沿着反应器的路径控制氢/单体比例的步骤通过多个空间分离，沿着环管反应器的路径供给氢。特别地，本发明提供了一种控制所产生的聚合物颗粒的分子量分布并优选变窄的方法。另一方面，本发明涉及适用于乙烯和任选的烯烃共聚单体的聚合方法的聚合反应器反应器，其中可以控制所生产的乙烯聚合物的分子量分布。

10. 发明申请

WO2012119953A1 PROCESS FOR PREPARING ZIEGLER-NATTA PRODUCED POLYETHYLENE BLENDS 审中-公开
标题翻译：制备ZIEGLER-NATTA生产的聚乙烯混合物的方法
公开(公告)号：WO2012119953A1
公开(公告)日：2012-09-13
申请号：PCT/EP2012/053654
申请日：2012-03-02
申请人： TOTAL RESEARCH & TECHNOLOGY FELUY , DEWACHTER, Daan , DAMME, Eric
发明人： DEWACHTER, Daan , DAMME, Eric
IPC分类号： C08L23/06 , C08L23/08 , C08F10/02
CPC分类号： C08L23/06 , C08L23/0815 , C08L2205/025 , C08L2207/062 , C08L2308/00 , C08L2314/02 , C08L2666/06
摘要： The invention relates to a process for preparing a multimodal polyethylene product, said product comprising at least two different polyethylene resins, the process comprising the steps of: (a) producing a first HMW polyethylene resin in the presence of a Ziegler-Natta catalyst in a reactor, wherein the High Load Melt Index (HLMI) of said first polyethylene resin is between 0.01 and 5 g/10 min, with the High Load Melt Index (HLMI) being measured by the procedure of ASTM D-1238 using a temperature of 190°C and a load of 21.6 kg; (b) separately producing a second LMW polyethylene resin in the presence of a Ziegler-Natta catalyst in a reactor, wherein the Melt Index (Ml2) of said second polyethylene resin is between 1 and 150 g/10 min, with the Melt Index Ml2 being measured by the procedure of ASTM D-1238 using a temperature of 190°C and a load of 2.16 kg; and (c) physically blending together said first and said second polyethylene resin to produce a multimodal polyethylene product, wherein the Ziegler-Natta catalyst used for the production of said first polyethylene resin has an average particle size (D50) of at most 15 μηι, with the D50 being measured by laser diffraction analysis on a Malvern type analyzer, and wherein step (c) is performed in device for continuously melting and blending said first and second polyethylene resin.
摘要翻译：本发明涉及一种制备多峰聚乙烯产品的方法，所述产品包含至少两种不同的聚乙烯树脂，该方法包括以下步骤：（a）在齐格勒 - 纳塔催化剂存在下，在第一种HMW聚乙烯树脂反应器，其中所述第一聚乙烯树脂的高负荷熔体指数（HLMI）为0.01至5g / 10min，其中通过ASTM D-1238的程序使用190℃的温度测量高负荷熔体指数（HLMI） °C，负荷21.6 kg; （b）在齐格勒 - 纳塔催化剂存在下在反应器中分别生产第二LMW聚乙烯树脂，其中所述第二聚乙烯树脂的熔体指数（M12）为1-150g / 10min，熔体指数M12 通过ASTM D-1238的程序使用190℃的温度和2.16kg的负荷来测量; 和（c）将所述第一和第二聚乙烯树脂物理混合在一起以制备多峰聚乙烯产品，其中用于生产所述第一聚乙烯树脂的齐格勒 - 纳塔催化剂的平均粒径（D50）至多为15微米 α，通过在Malvern型分析仪上的激光衍射分析来测量D50，并且其中步骤（c）在用于连续熔融和共混所述第一和第二聚乙烯树脂的装置中进行。

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