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1. 发明申请

WO2007113206A1 PROCESS TO KILL A CATALYZED OLEFIN POLYMERIZATION 审中-公开
标题翻译：杀死催化烯烃聚合的方法
公开(公告)号：WO2007113206A1
公开(公告)日：2007-10-11
申请号：PCT/EP2007/053026
申请日：2007-03-29
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , MISERQUE, Olivier , BRUSSELLE, Alain , WARICHET, Vincent
发明人： MISERQUE, Olivier , BRUSSELLE, Alain , WARICHET, Vincent
IPC分类号： C08F10/00 , C08F10/02 , C08F4/00 , C08F2/00
CPC分类号： C08F10/00 , C08F2/42
摘要： Process to kill a continuous catalyzed olefin liquid phase polymerization in which the catalyst is a Ziegler-Natta or a metallocene catalyst, wherein, a predetermined amount of killing agent is injected into the reactor during at least twice the cycle time of the reactor.
摘要翻译：杀死其中催化剂是齐格勒 - 纳塔或茂金属催化剂的连续催化烯烃液相聚合的方法，其中在反应器的循环时间的至少两倍内将预定量的杀伤剂注入反应器。

2. 发明申请

WO2007076996A1 DYNAMIC PRESSURE CONTROL IN DOUBLE LOOP REACTOR 审中-公开
标题翻译：双环反应器动态压力控制
公开(公告)号：WO2007076996A1
公开(公告)日：2007-07-12
申请号：PCT/EP2006/012534
申请日：2006-12-27
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY PATENT DEPARTMENT , DEWACHTER, Daan , FOUARGE, Louis , BRUSSELLE, Alain
发明人： DEWACHTER, Daan , FOUARGE, Louis , BRUSSELLE, Alain
IPC分类号： B01J19/18 , B01J8/00 , C08F10/00
CPC分类号： C08F2/001 , B01J8/007 , B01J19/1837 , B01J19/1881 , B01J2219/00033 , B01J2219/0004 , B01J2219/00094 , B01J2219/00166 , C08F10/00 , C08F110/02 , C08F110/06 , C08F2/01
摘要： The present invention discloses a slurry loop reactor comprising at least two loop reactors connected in series and wherein the line connecting the two loops is subject to a dynamic pressure difference.
摘要翻译：本发明公开了一种包含至少两个串联连接的回路反应器的浆液回路反应器，其中连接两个回路的管线经受动压差。

3. 发明申请

WO2012013807A1 METHOD FOR PRODUCING POLYETHYLENE 审中-公开
标题翻译：生产聚乙烯的方法
公开(公告)号：WO2012013807A1
公开(公告)日：2012-02-02
申请号：PCT/EP2011/063151
申请日：2011-07-29
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , STEVENS, Peter , FANT, Franky , DEWACHTER, Daan , BRUSSELLE, Alain
发明人： STEVENS, Peter , FANT, Franky , DEWACHTER, Daan , BRUSSELLE, Alain
IPC分类号： C08F10/00 , C08F2/02 , B01J19/18
CPC分类号： C08F2/01 , B01J8/226 , B01J19/1837 , B01J2219/00006 , C08F210/16 , C08F2410/03 , C08F2/14 , C08F210/14 , C08F2500/24 , C08F2500/05 , C08F2500/12
摘要： The present invention relates to a method for consecutively producing at least two different polyethylene resins in one slurry loop reactor, comprising producing a first polyethylene resin in the presence of a Ziegler-Natta and/or a Chromium catalyst, and consecutively producing a second polyethylene resin in the presence of a metallocene catalyst, characterized in that the ratio of the melt flow index of the first produced polyethylene resin to the melt flow index of the second produced polyethylene resin is at least 0.3.
摘要翻译：本发明涉及在一个浆料环流反应器中连续生产至少两种不同的聚乙烯树脂的方法，包括在齐格勒 - 纳塔和/或铬催化剂存在下制备第一种聚乙烯树脂，并连续地生产第二种聚乙烯树脂在金属茂催化剂的存在下，其特征在于，第一制得的聚乙烯树脂的熔体流动指数与第二次生产的聚乙烯树脂的熔体流动指数的比率至少为0.3。

4. 发明申请

WO2007113213A1 SLURRY POLYMERISATION PROCESS OF ETHYLENE IN THE PRESENCE OF LOW AMOUNT OF SCAVENGER. 审中-公开
标题翻译：乙烯的低聚合过程在少量SCAVENGER的存在下。
公开(公告)号：WO2007113213A1
公开(公告)日：2007-10-11
申请号：PCT/EP2007/053044
申请日：2007-03-29
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , MISERQUE, Olivier , SLAWINSKI, Martine , SIRAUX, Daniel , BRUSSELLE, Alain
发明人： MISERQUE, Olivier , SLAWINSKI, Martine , SIRAUX, Daniel , BRUSSELLE, Alain
IPC分类号： C08F2/14 , C08F4/659 , C08F10/00 , C08F2/00
CPC分类号： C08F210/16 , C08F4/65912 , C08F4/65927 , C08F10/00 , C08F110/02 , C08F4/65916 , C08F2/001 , C08F2500/12 , C08F210/14
摘要： The invention discloses a metallocene catalysed slurry polymerisation process of ethylene in the presence of a low concentration of scavenger. This allows improving the anti-sheeting of the reactor during the polymerisation process.
摘要翻译：本发明公开了一种茂金属催化的在低浓度清除剂存在下乙烯的淤浆聚合方法。这允许在聚合过程中改善反应器的抗张力。

5. 发明申请

WO2012013802A1 PRESSURE CONTROL OF THE CATALYST MIXING VESSEL 审中-公开
标题翻译：催化混合容器的压力控制
公开(公告)号：WO2012013802A1
公开(公告)日：2012-02-02
申请号：PCT/EP2011/063143
申请日：2011-07-29
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , BRUSSELLE, Alain , DEWACHTER, Daan , FOUARGE, Louis
发明人： BRUSSELLE, Alain , DEWACHTER, Daan , FOUARGE, Louis
IPC分类号： C08F10/02 , C08F2/01 , C08F2/14
CPC分类号： G05D16/02 , B01J8/0035 , B01J8/20 , B01J2219/00162 , C08F4/76 , C08F10/02 , C08F2/14 , C08F2/01
摘要： The present invention relates to a process for preparing catalyst slurry in a catalyst slurry preparation system and supplying catalyst slurry to an ethylene polymerization loop reactor wherein an accurate control of the pressure within said catalyst slurry preparation system is provided. More particularly, the present invention provides a method for preparing a catalyst slurry and supplying said catalyst slurry to an ethylene polymerization loop reactor, said catalyst slurry comprising solid catalyst and a liquid hydrocarbon diluent, wherein said method comprises the steps of: (a) feeding concentrated catalyst slurry to a mixing vessel by means of a feeding device; (b) diluting said concentrated catalyst slurry in a suitable amount of said diluent in a mixing vessel thereby obtaining a diluted catalyst slurry having a concentration suitable for use in an ethylene polymerization reaction; wherein said mixing vessel is provided with at least one pressure regulating unit connected therewith and wherein said pressure regulating unit comprises a pulsation dampener; and (c) transferring said diluted catalyst slurry from said mixing vessel to said ethylene polymerization loop reactor; characterized in that the method comprises the step of maintaining said mixing vessel essentially free of a gaseous phase by regulating the pressure in said mixing vessel using said at least one pressure regulating unit comprising the pulsation dampener.
摘要翻译：本发明涉及一种在催化剂浆料制备系统中制备催化剂浆料并将催化剂浆料供应到乙烯聚合反应器中的方法，其中提供了所述催化剂浆料制备系统内的压力的精确控制。更具体地说，本发明提供了一种制备催化剂浆料并将所述催化剂浆料供应到乙烯聚合反应器的方法，所述催化剂浆料包括固体催化剂和液体烃稀释剂，其中所述方法包括以下步骤：（a）浓缩的催化剂浆料通过进料装置进入混合容器; （b）将所述浓缩催化剂浆液在合适量的稀释剂中稀释在混合容器中，由此获得具有适合用于乙烯聚合反应的浓度的稀释催化剂浆料; 其中所述混合容器设置有与其连接的至少一个压力调节单元，并且其中所述压力调节单元包括脉动阻尼器; 和（c）将所述稀释的催化剂浆料从所述混合容器转移到所述乙烯聚合反应器中; 其特征在于，所述方法包括通过使用包括脉动阻尼器的所述至少一个压力调节单元来调节所述混合容器中的压力来维持所述混合容器基本上不含气相的步骤。

6. 发明申请

WO2012013797A1 USE OF A CATALYST SLURRY PREPARATION SYSTEM 审中-公开
标题翻译：使用催化剂浆液制备系统
公开(公告)号：WO2012013797A1
公开(公告)日：2012-02-02
申请号：PCT/EP2011/063136
申请日：2011-07-29
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , BRUSSELLE, Alain , FOUARGE, Louis
发明人： BRUSSELLE, Alain , FOUARGE, Louis
IPC分类号： C08F2/00 , B01J8/00
CPC分类号： C08F10/02 , B01F7/00633 , B01F7/1675 , B01F7/22 , B01F13/0827 , B01F13/0836 , B01F13/0845 , B01J8/002 , B01J8/0035 , C08F4/00 , C08F4/65912 , C08F4/65927 , C08F10/00 , C08F4/65916
摘要： The present invention relates to the use of a catalyst preparation system for the preparation of a diluted catalyst slurry. In particular, the invention relates to a catalyst preparation system comprising a mixing vessel for mixing a particulate catalyst and a liquid hydrocarbon diluent. According to the invention, diluted catalyst slurry is prepared in a mixing vessel comprising a rotatable axial impeller system comprising at least two double-bladed hubs. The invention also relates to a process for preparing diluted catalyst slurry for use in the preparation of a particulate polyethylene product in a loop reactor with the catalyst preparation system as described herein.
摘要翻译：本发明涉及催化剂制备系统用于制备稀释催化剂浆料的用途。特别地，本发明涉及一种催化剂制备系统，其包括用于混合颗粒催化剂和液体烃稀释剂的混合容器。根据本发明，稀释的催化剂浆料在混合容器中制备，该混合容器包括可旋转的轴流式叶轮系统，其包括至少两个双叶片轮毂。本发明还涉及一种用于制备稀释的催化剂浆料的方法，所述稀释的催化剂浆料用于在具有如本文所述的催化剂制备系统的环管反应器中制备颗粒状聚乙烯产品。

7. 发明申请

WO2013110322A1 METHOD FOR PROCESSING POLYETHYLENE 审中-公开
标题翻译：加工聚乙烯的方法
公开(公告)号：WO2013110322A1
公开(公告)日：2013-08-01
申请号：PCT/EP2012/051043
申请日：2012-01-24
申请人： TOTAL RESEARCH & TECHNOLOGY FELUY , STEVENS, Peter , FANT, Franky , DEWACHTER, Daan , BRUSSELLE, Alain
发明人： STEVENS, Peter , FANT, Franky , DEWACHTER, Daan , BRUSSELLE, Alain
IPC分类号： C08F10/00 , C08F2/02 , B01J19/18
CPC分类号： C08J3/203 , B29B9/06 , B29C47/0004 , B29C47/0011 , B29C47/0066 , C08J3/00 , C08J2323/06 , C08J2323/16 , C08J2423/06
摘要： Method for consecutively batch processing at least two different polyethylene grades in pellet form in a pellet handling unit, comprising the steps of consecutively batch processing at least two different polyethylene grades in pellet form in a pellet handling unit, wherein the ratio of the melt flow index (MI) of a first polyethylene in pellet form (MI f ) to the MI of a later processed polyethylene in pellet form (MI l ) is smaller than 0.30, and comprising the step of processing an intermediate polyethylene grade in pellet form, wherein the amount of intermediate polyethylene grade processed is at most 1/100 th of the handling capacity of the pellet handling unit, and wherein said intermediate polyethylene grade has the same MI than said later processed polyethylene in pellet form.
摘要翻译：在丸粒处理单元中连续批处理至少两种不同聚乙烯粒度聚乙烯等级的方法，包括以下步骤：在颗粒处理单元中连续批处理至少两种颗粒形式的不同聚乙烯等级，其中熔体流动指数颗粒形式（MIf）的后处理聚乙烯的MI的颗粒形式（MIf）的第一聚乙烯的MI（MI）小于0.30，包括以颗粒形式加工中间聚乙烯等级的步骤中间聚乙烯等级加工量最多为颗粒处理单元的处理能力的1/100，其中所述中间聚乙烯等级具有与所述稍后加工的聚乙烯颗粒相同的MI。

8. 发明申请

WO2012013800A1 PROCESS FOR SUPPLYING CATALYST TO A POLYMERIZATION REACTOR 审中-公开
标题翻译：向聚合反应器供应催化剂的方法
公开(公告)号：WO2012013800A1
公开(公告)日：2012-02-02
申请号：PCT/EP2011/063140
申请日：2011-07-29
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , DEWACHTER, Daan , BRUSSELLE, Alain
发明人： DEWACHTER, Daan , BRUSSELLE, Alain
IPC分类号： B01J8/00 , C08F2/00
CPC分类号： F03B17/00 , B01J8/002 , B01J2208/00752 , C08F4/65916 , C08F10/00 , C08F210/16 , Y10S417/90 , Y10S526/919 , Y10T137/0318 , C08F2/14 , C08F2/01 , C08F210/14
摘要： The present invention relates to a method for feeding metallocene catalyst slurry to an olefin polymerization loop reactor (1) using a positive displacement device (5) comprising a first chamber (5-6) and a second chamber (5-3) each chamber having an outlet and each chamber comprising a ball arranged between the walls of said chamber, wherein said chambers are connected to each other by a pump chamber (5-2) operably connected to a pump, wherein the difference between the diameter of said ball and the diameter of said chamber is comprised between 5 to 200 times the average particle size (d50) of said catalyst.
摘要翻译：本发明涉及使用包括第一室（5-6）和第二室（5-3）的正位移装置（5）将茂金属催化剂浆料供给到烯烃聚合反应器（1）的方法，每个室具有出口和每个室包括布置在所述室的壁之间的球，其中所述室通过可操作地连接到泵的泵室（5-2）彼此连接，其中所述球的直径与所述室的直径为所述催化剂的平均粒度（d50）的5至200倍。

9. 发明申请

WO2007076996A8 DYNAMIC PRESSURE CONTROL IN DOUBLE LOOP REACTOR 审中-公开
标题翻译：双环反应器动态压力控制
公开(公告)号：WO2007076996A8
公开(公告)日：2008-07-10
申请号：PCT/EP2006012534
申请日：2006-12-27
申请人： TOTAL PETROCHEMICALS RES FELUY , DEWACHTER DAAN , FOUARGE LOUIS , BRUSSELLE ALAIN
发明人： DEWACHTER DAAN , FOUARGE LOUIS , BRUSSELLE ALAIN
IPC分类号： B01J19/18 , B01J8/00 , C08F10/00
CPC分类号： C08F2/001 , B01J8/007 , B01J19/1837 , B01J19/1881 , B01J2219/00033 , B01J2219/0004 , B01J2219/00094 , B01J2219/00166 , C08F10/00 , C08F110/02 , C08F110/06 , C08F2/01
摘要： The present invention discloses a slurry loop reactor comprising at least two loop reactors connected in series and wherein the line connecting the two loops is subject to a dynamic pressure difference.
摘要翻译：本发明公开了一种包含至少两个串联连接的回路反应器的浆液回路反应器，其中连接两个回路的管线经受动压差。

10. 发明申请

WO2012013803A1 METHOD FOR HANDLING METALLOCENE CATALYSTS 审中-公开
标题翻译：处理金属催化剂的方法
公开(公告)号：WO2012013803A1
公开(公告)日：2012-02-02
申请号：PCT/EP2011/063145
申请日：2011-07-29
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , BRUSSELLE, Alain , DEWACHTER, Daan , DE KOSTER, Michiel
发明人： BRUSSELLE, Alain , DEWACHTER, Daan , DE KOSTER, Michiel
IPC分类号： B65D88/12 , B65D88/54 , C08F2/00
CPC分类号： C08F210/16 , B65D88/30 , B65D88/66 , B65D90/623 , C08F2/01 , C08F2/14 , C08F210/06
摘要： The present invention relates to a method for handling a solid composition comprising a metallocene catalyst,comprising the step of: transporting said composition in a closed and oxygen-free transportation container provided with a bottom discharge opening. The container is advantageous for storing a metallocene catalyst, particularly in a dry form. Preferably, the bottom discharge opening of the method of the invention is provided with a ball valve. The container of the invention allows for safe transportation and handling of hazardous catalyst materials.
摘要翻译：本发明涉及一种处理包含金属茂催化剂的固体组合物的方法，包括以下步骤：将所述组合物输送到设有底部排出口的封闭且无氧的运输容器中。该容器有利于储存茂金属催化剂，特别是干燥形式。优选地，本发明的方法的底部排出口设置有球阀。本发明的容器允许危险催化剂材料的安全运输和处理。

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