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    • 5. 发明申请
    • CONTROLLED PREPARATION OF NANOPARTICLE MATERIALS
    • 控制制备纳米材料
    • WO2007049052A2
    • 2007-05-03
    • PCT/GB2006004003
    • 2006-10-27
    • NANOCO TECHNOLOGIES LTDPICKETT NIGEL
    • PICKETT NIGEL
    • C01B17/20C01B19/00H01L29/12
    • C01B19/007B82Y10/00B82Y30/00C01B17/20C01B19/002C01P2002/72C01P2002/84C01P2004/64C01P2004/80C01P2004/84C30B7/00C30B7/005H01L29/127Y10T428/2982Y10T428/2991Y10T428/2993Y10T428/2995Y10T428/2996
    • A method of producing nanoparticles comprising effecting conversion of a nanoparticle precursor composition to the material of the nanoparticles, said precursor composition comprising a first precursor species containing a first ion to be incorporated into the growing nanoparticles and a second precursor species containing a second ion to be incorporated into the growing nanoparticles, said conversion being effected in the presence of a molecular cluster compound under conditions permitting seeding and growth of the nanoparticles, wherein the method comprises dispersing the molecular cluster compound and an initial portion of the nanoparticle precursor composition which is less than the total amount of the nanoparticle precursor composition to be used to produce said nanoparticles in a suitable dispersing medium at a first temperature; increasing the temperature of the dispersing medium containing the cluster compound and precursor composition to a second temperature which is sufficient to initiate seeding and growth of the nanoparticles on the molecular clusters of said molecular cluster compound; and adding one or more further portions of the nanoparticle precursor composition to the dispersing medium containing the growing nanoparticles, wherein the temperature of the dispersing medium containing the growing nanoparticles is increased before, during and/or after the addition of the or each further portion of the nanoparticle precursor composition.
    • 一种制备纳米颗粒的方法,其包括使纳米颗粒前体组合物转化为纳米颗粒的材料,所述前体组合物包含含有待结合到生长纳米颗粒中的第一离子的第一前体物质和含有第二离子的第二前体物质 掺入生长的纳米颗粒中,所述转化在允许纳米颗粒的接种和生长的条件下在分子簇化合物的存在下进行,其中所述方法包括将分子簇化合物和初始部分的纳米颗粒前体组合物分散在小于 用于在合适的分散介质中在第一温度下制备所述纳米颗粒的纳米颗粒前体组合物的总量; 将含有簇化合物和前体组合物的分散介质的温度升高到足以引发纳米颗粒在所述分子簇化合物的分子簇上的接种和生长的第二温度; 以及将纳米颗粒前体组合物的一个或多个其它部分加入到含有生长的纳米颗粒的分散介质中,其中含有生长的纳米颗粒的分散介质的温度在加入之前,期间和/或之后增加 纳米颗粒前体组合物。