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1. 发明申请

WO2008002888A3 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
公开(公告)号：WO2008002888A3
公开(公告)日：2008-01-03
申请号：PCT/US2007/072070
申请日：2007-06-26
申请人： GENERAL ELECTRIC COMPANY , CHAN, Kwok, Pong , CROLL, Joshua, McClellan , GANESAN, Balakrishnan , HAGBERG, Erik , HARRIGAN, Marcus , KHOURI, Farid, Fouad , KISHAN, Gurram , MATHUR, Ritesh , MAXAM, John, Lester , MULLEN, Tara, J. , ODLE, Roy, Ray , RANGANATHAN, Sathish, Kumar , SUFFIELD, Rachel, Marie , WANG, Wenhui , WHITE, James, Mitchell
发明人： CHAN, Kwok, Pong , CROLL, Joshua, McClellan , GANESAN, Balakrishnan , HAGBERG, Erik , HARRIGAN, Marcus , KHOURI, Farid, Fouad , KISHAN, Gurram , MATHUR, Ritesh , MAXAM, John, Lester , MULLEN, Tara, J. , ODLE, Roy, Ray , RANGANATHAN, Sathish, Kumar , SUFFIELD, Rachel, Marie , WANG, Wenhui , WHITE, James, Mitchell
IPC分类号： C08K3/34 , C08K5/50 , C08K9/04 , C08L79/08
摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides a polymer-organoclay composite composition comprising (a) a polymeric resin; and (b) an organoclay composition comprising alternating inorganic silicate layers and organic layers, said organic layers comprising a quaternary phosphonium cation having structure X wherein Ar 1 , Ar 2 , and Ar 3 are independently C 2 -C 50 aromatic radicals; Ar 4 is a bond or a C 2 -C 50 aromatic radical; "a" is a number from 1 to about 200; "c" is a number from 0 to 3; R 1 is independently at each occurrence a halogen atom, a C 1 -C 20 aliphatic radical, a C 5 -C 20 cycloaliphatic radical, or a C 2 -C 20 aromatic radical; and R 2 is a halogen atom, a C 1 -C 20 aliphatic radical, a C 5 -C 20 cycloaliphatic radical, a C 2 -C 50 aromatic radical, or a polymer chain.

2. 发明申请

WO2008002890A2 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
标题翻译：聚合物复合材料的组合物和方法
公开(公告)号：WO2008002890A2
公开(公告)日：2008-01-03
申请号：PCT/US2007/072072
申请日：2007-06-26
申请人： GENERAL ELECTRIC COMPANY , CHAN, Kwok, Pong , CROLL, Joshua, McClellan , HAGBERG, Erik , MAXAM, John, Lester , MULLEN, Tara, J. , ODLE, Roy, Ray , SUFFIELD, Rachel, Marie , WHITE, James, Mitchell , YAMAGUCHI, Norimitsu
发明人： CHAN, Kwok, Pong , CROLL, Joshua, McClellan , HAGBERG, Erik , MAXAM, John, Lester , MULLEN, Tara, J. , ODLE, Roy, Ray , SUFFIELD, Rachel, Marie , WHITE, James, Mitchell , YAMAGUCHI, Norimitsu
CPC分类号： C08J5/18 , C08J3/201 , C08J5/10 , C08J2379/08 , C08K3/346 , C08K5/18 , C08K5/19 , C08K5/3432 , C08K5/50 , C08K9/04
摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides a method of making a polymer-organoclay composite composition, said method comprising melt mixing a quaternary organoclay composition comprising alternating inorganic silicate layers and organic layers, said organic layers comprising a quaternary organic cation with a polyetherimide composition; said melt mixing being carried out at a temperature in a range between about 300°C and about 450°C to provide a polymer-organoclay composite composition, said polymer-organoclay composite composition being characterized by a percent exfoliation of at least 10 percent.
摘要翻译：本发明涉及可用于制备有机粘土组合物，聚合物 - 有机粘土复合材料组合物和制备聚合物纳米复合材料的方法的有机盐组合物。在一个实施方案中，本发明提供了制备聚合物 - 有机粘土复合材料组合物的方法，所述方法包括熔融混合包含交替的无机硅酸盐层和有机层的季有机粘土组合物，所述有机层包含季铵有机阳离子与聚醚酰亚胺组合物; 所述熔体混合在约300℃至约450℃之间的温度下进行，以提供聚合物 - 有机粘土复合材料组合物，所述聚合物 - 有机粘土复合组合物的特征在于至少10％的剥离百分比。

3. 发明申请

WO2008002891A3 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
公开(公告)号：WO2008002891A3
公开(公告)日：2008-01-03
申请号：PCT/US2007/072073
申请日：2007-06-26
申请人： GENERAL ELECTRIC COMPANY , CAO, Feng , CHAN, Kwok, Pong , HAGBERG, Erik , KHOURI, Farid, Fouad , MULLEN, Tara, J. , ODLE, Roy, Ray , WHITE, James, Mitchell , YAMAGUCHI, Norimitsu
发明人： CAO, Feng , CHAN, Kwok, Pong , HAGBERG, Erik , KHOURI, Farid, Fouad , MULLEN, Tara, J. , ODLE, Roy, Ray , WHITE, James, Mitchell , YAMAGUCHI, Norimitsu
IPC分类号： C08F2/44 , C08K9/04 , C08K3/34 , C08K5/50 , C08L79/08 , C08K5/17
摘要： In one embodiment, the present invention provides a method of making a polymer- organoclay composite composition comprising (a) contacting under condensation polymerization conditions a first monomer, a second monomer, a solvent, and an organoclay composition, said organoclay composition comprising alternating inorganic silicate layers and organic layers, to provide a first polymerization reaction mixture, wherein one of said first monomer and second monomers is a diamine and the the other is an dianhydride; (b) carrying out a stoichiometry verification step on the first polymerization reaction mixture; (c) optionally adding additional reactant (monomer 1, monomer 2, or chainstopper) to the first polymerization reaction mixture to provide a second polymerization reaction mixture; and (d) removing solvent from the first polymerization reaction mixture or the second polymerization reaction mixture to provide a first polymer-organoclay composite composition comprising a polymer component and an organoclay component wherein the organoclay component is at least 10% exfoliated.

4. 发明申请

WO2008002880A2 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
标题翻译：聚合物复合材料的组合物和方法
公开(公告)号：WO2008002880A2
公开(公告)日：2008-01-03
申请号：PCT/US2007/072036
申请日：2007-06-25
申请人： GENERAL ELECTRIC COMPANY , CHAN, Kwok, Pong , MAXAM, John, Lester , ODLE, Roy, Ray , MULLEN, Tara, J. , WHITE, James, Mitchell , HAGBERG, Erik
发明人： CHAN, Kwok, Pong , MAXAM, John, Lester , ODLE, Roy, Ray , MULLEN, Tara, J. , WHITE, James, Mitchell , HAGBERG, Erik
IPC分类号： C08K9/04 , C08K3/34 , C08K5/50 , C08L71/00 , C08L79/08 , C08L81/06
CPC分类号： C08F2/44 , C01P2002/72 , C01P2004/04 , C08K9/04 , C08L79/08 , C09C1/42
摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides a polymer-organoclay composite composition comprising (a) a polymeric resin; and (b) an organoclay composition comprising alternating inorganic silicate layers and organic layers, said organic layers comprising a quaternary phosphonium cation having structure (XXXIII) wherein Ar 12 , Ar 13 , Ar 14 and Ar 15 are independently C 2 -C 50 aromatic radicals; and Ar 16 is a C 2 -C 200 aromatic radical, or a polymer chain comprising at least one aromatic group.
摘要翻译：本发明涉及可用于制备有机粘土组合物，聚合物 - 有机粘土复合组合物和用于制备聚合物纳米复合材料的方法的有机盐组合物。在一个实施方案中，本发明提供了一种聚合物 - 有机粘土复合组合物，其包含（a）聚合物树脂; 和（b）包含交替的无机硅酸盐层和有机层的有机粘土组合物，所述有机层包含具有结构（XXXIII）的季鏻阳离子，其中Ar 12，Ar 13， Ar 14和Ar 15独立地为C 2 -C 50芳族基团; 并且Ar 16是C 2 -C 20芳族基团或包含至少一个芳族基团的聚合物链。

5. 发明申请

WO2008002870A2 METHODS OF PREPARING POLYMER-ORGANOCLAY COMPOSITES AND ARTICLES DERIVED THEREFROM 审中-公开
标题翻译：制备聚合物 - 有机粘合剂复合材料的方法和由此衍生的制品
公开(公告)号：WO2008002870A2
公开(公告)日：2008-01-03
申请号：PCT/US2007/072019
申请日：2007-06-25
申请人： GENERAL ELECTRIC COMPANY , CHAN, Kwok, Pong , ODLE, Roy, Ray , HALL, David, Bruce , MAXAM, John, Lester , STELLA, Albert, Santo , GENOVESE, Sarah, Elizabeth , MULLEN, Tara, J. , WHITE, James, Mitchell , HAGBERG, Erik
发明人： CHAN, Kwok, Pong , ODLE, Roy, Ray , HALL, David, Bruce , MAXAM, John, Lester , STELLA, Albert, Santo , GENOVESE, Sarah, Elizabeth , MULLEN, Tara, J. , WHITE, James, Mitchell , HAGBERG, Erik
IPC分类号： C08F2/44 , C08K9/04 , C08L79/08 , C08K3/34 , C08K5/19 , C08K5/3432 , C08K5/50
CPC分类号： C08F2/44
摘要： A method for preparing a polymer-organoclay composite composition comprises combining a solvent and an unexfoliated organoclay to provide a first mixture, wherein the unexfoliated organoclay comprises alternating inorganic silicate layers and organic layers, and has an initial spacing between the silicate layers; exposing the first mixture to an energized condition of a sufficient intensity and duration to increase the initial spacing of the inorganic silicate layers, to provide a second mixture; contacting the second mixture with a polymer composition so that the polymer composition fills at least one region located between at least one pair of silicate layers, wherein the polymer composition is at least partially soluble in the solvent; and removing at least a portion of the solvent from the second mixture, wherein the inorganic silicate layers remain separated by the polymer after removal of the solvent.
摘要翻译：用于制备聚合物 - 有机粘土复合组合物的方法包括将溶剂和未剥落的有机粘土组合以提供第一混合物，其中未剥落的有机粘土包含交替的无机硅酸盐层和有机层，并且具有初始间距在硅酸盐层之间; 使第一混合物暴露于足够强度和持续时间的激励条件以增加无机硅酸盐层的初始间距，以提供第二混合物; 使第二混合物与聚合物组合物接触，使得聚合物组合物填充位于至少一对硅酸盐层之间的至少一个区域，其中聚合物组合物至少部分可溶于溶剂中; 和从第二混合物中除去至少一部分溶剂，其中在除去溶剂后，无机硅酸盐层仍然被聚合物分开。

6. 发明申请

WO2008002889A2 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
标题翻译：聚合物复合材料的组合物和方法
公开(公告)号：WO2008002889A2
公开(公告)日：2008-01-03
申请号：PCT/US2007/072071
申请日：2007-06-26
申请人： GENERAL ELECTRIC COMPANY , CHAN, Kwok, Pong , HAGBERG, Erik , MULLEN, Tara, J. , ODLE, Roy, Ray , WHITE, James, Mitchell , YAMAGUCHI, Norimitsu
发明人： CHAN, Kwok, Pong , HAGBERG, Erik , MULLEN, Tara, J. , ODLE, Roy, Ray , WHITE, James, Mitchell , YAMAGUCHI, Norimitsu
CPC分类号： C08J3/201 , B82Y30/00 , C01B33/44 , C08J5/005 , C08K3/346 , C08K5/50 , C08K9/04
摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides a method of making a polymer-organoclay composite composition, said method comprising melt mixing a quaternary organoclay composition comprising alternating inorganic silicate layers and organic layers, said organic layers comprising a quaternary organic cation with a polymeric resin comprising at least one polymer selected from the group consisting of polyamides, polyesters, polyarylene sulfides, polyarylene ethers, polyether sulfones, polyether ketones, polyether ether ketones, polyphenylenes, and polyphenylenes said polymeric resin being substantially free of polyetherimides; said melt mixing being carried out at a temperature in a range between about 300 °C and about 450 °C to provide a polymer-organoclay composite composition, said polymer-organoclay composite composition being characterized by a percent exfoliation of at least 10 percent.
摘要翻译：本发明涉及可用于制备有机粘土组合物，聚合物 - 有机粘土复合组合物和用于制备聚合物纳米复合材料的方法的有机盐组合物。在一个实施方案中，本发明提供了制备聚合物 - 有机粘土复合组合物的方法，所述方法包括熔融混合包含交替的无机硅酸盐层和有机层的季有机粘土组合物，所述有机层包含季有机阳离子和聚合物树脂，至少一种选自聚酰胺，聚酯，聚亚芳基硫醚，聚亚芳基醚，聚醚砜，聚醚酮，聚醚醚酮，聚亚苯基和聚亚苯基的聚合物，所述聚合物树脂基本上不含聚醚酰亚胺; 所述熔融混合在约300℃至约450℃的温度范围内进行以提供聚合物 - 有机粘土复合组合物，所述聚合物 - 有机粘土复合组合物的特征在于百分比剥落至少10％

7. 发明申请

WO2008002866A2 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
标题翻译：聚合物复合材料的组合物和方法
公开(公告)号：WO2008002866A2
公开(公告)日：2008-01-03
申请号：PCT/US2007/072013
申请日：2007-06-25
申请人： GENERAL ELECTRIC COMPANY , CHAN, Kwok, Pong , ODLE, Roy, Ray , MULLEN, Tara, J. , WHITE, James, Mitchell , HAGBERG, Erik
发明人： CHAN, Kwok, Pong , ODLE, Roy, Ray , MULLEN, Tara, J. , WHITE, James, Mitchell , HAGBERG, Erik
IPC分类号： C08K9/04 , C08K3/34 , C08K5/50
CPC分类号： C08K9/04 , C08K5/50
摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides an organoclay composition comprising alternating inorganic silicate layers and organic layers, said organic layers comprising a quaternary phosphonium cation having structure (Formula XXXIII), wherein Ar 12 , Ar 13 , Ar 14 and Ar 15 are independently C 2 -C 50 aromatic radicals; and Ar 16 is a C 2 -C 200 aromatic radical, or a polymer chain comprising at least one aromatic group.
摘要翻译：本发明涉及可用于制备有机粘土组合物，聚合物 - 有机粘土复合组合物和用于制备聚合物纳米复合材料的方法的有机盐组合物。在一个实施方案中，本发明提供了一种包含交替的无机硅酸盐层和有机层的有机粘土组合物，所述有机层包含具有结构（式XXXIII）的季鏻阳离子，其中Ar 12，Ar ^{13，Ar 14和Ar 15独立地为C 2 -C 50芳族基团; 并且Ar 16是C 2 -C 20芳族基团或包含至少一个芳族基团的聚合物链。}

8. 发明申请

WO2008039577A2 POLYIMIDE SOLVENT CAST FILMS HAVING LOW COEFFICIENT OF THERMAL EXPANSION AND METHOD OF MANUFACTURE THEREOF 审中-公开
标题翻译：具有低膨胀系数的聚酰亚胺溶剂型薄膜及其制造方法
公开(公告)号：WO2008039577A2
公开(公告)日：2008-04-03
申请号：PCT/US2007/071205
申请日：2007-06-14
申请人： GENERAL ELECTRIC COMPANY , CHAN, Kwok, Pong , HAGBERG, Erik , MULLEN, Tara, J. , ODLE, Roy, Ray
发明人： CHAN, Kwok, Pong , HAGBERG, Erik , MULLEN, Tara, J. , ODLE, Roy, Ray
IPC分类号： C08K3/08 , C08K13/02 , C08K5/134 , C23C18/54 , H05K9/00 , B44C5/04 , B32B27/32 , B32B5/18
CPC分类号： H05K1/0346 , B82Y30/00 , C08G73/1007 , C08J5/005 , C08J5/18 , C08J2379/08 , H05K1/0373 , H05K2201/0154 , H05K2201/0209 , H05K2201/0257 , H05K2201/068
摘要： A solvent cast film comprises a polyimide comprising structural units derived from polymerization of a dianhydride component comprising a dianhydride selected from the group consisting of 3,4'-oxydiphthalic dianhydride, 3,3'-oxydiphthalic dianhydride, 4,4'-oxydiphthalic dianhydride, and combinations thereof, with a diamine component wherein the polyimide has a glass transition temperature of at least 190°C; wherein the film has a coefficient of thermal expansion of less than 60 ppm/°C, a thickness from 0.1 to 250 micrometers, and less than 5% residual solvent by weight; wherein the polyimide has less than 15 molar % of structural units derived from a member selected from the group consisting of biphenyltetracarboxylic acid, a dianhydride of biphenyltetracarboxylic acid, an ester of biphenyltetracarboxylic acid, and a combination thereof.
摘要翻译：溶剂流延膜包括聚酰亚胺，其包含衍生自二酐组分的聚合的结构单元，所述二酐组分包含二酐，其选自3,4'-氧二邻苯二甲酸二酐，3,3'-氧联二邻苯二甲酸二酐，4,4'-氧联二邻苯二甲酸二酐，和其组合与二胺组分，其中聚酰亚胺的玻璃化转变温度至少为190℃; 其中所述膜具有小于60ppm /℃的热膨胀系数，0.1至250微米的厚度和小于5重量％的残留溶剂; 其中所述聚酰亚胺具有少于15摩尔％的衍生自选自联苯四羧酸，联苯四羧酸的二酐，联苯四羧酸的酯及其组合的成员的结构单元。

9. 发明申请

WO2008060712A2 ARTICLES COMPRISING A POLYIMIDE SOLVENT CAST FILM HAVING A LOW COEFFICIENT OF THERMAL EXPANSION AND METHOD OF MANUFACTURE THEREOF 审中-公开
标题翻译：包含具有低热膨胀系数的聚酰亚胺溶剂铸膜的制品及其制造方法
公开(公告)号：WO2008060712A2
公开(公告)日：2008-05-22
申请号：PCT/US2007/071217
申请日：2007-06-14
申请人： GENERAL ELECTRIC COMPANY , CHAN, Kwok, Pong , HAGBERG, Erik , MULLEN, Tara, J. , ODLE, Roy, Ray
发明人： CHAN, Kwok, Pong , HAGBERG, Erik , MULLEN, Tara, J. , ODLE, Roy, Ray
CPC分类号： H05K1/0346 , B29B17/0042 , B29B17/0404 , B29K2079/08 , B29L2007/008 , B32B15/08 , C08G73/1007 , C08J5/18 , C08J2379/08 , C08L79/08 , H05K1/0373 , H05K2201/0154 , H05K2201/0209 , H05K2201/0257 , H05K2201/068 , Y02W30/62 , Y02W30/625 , Y10T428/12569 , Y10T428/25 , Y10T428/2938 , Y10T428/31678 , Y10T428/31681 , Y10T428/31721 , Y10T428/31765
摘要： A solvent cast film comprises a polyimide comprising structural units derived from polymerization of a dianhydride component comprising a dianhydride selected from the group consisting of 3,4'-oxydiphthalic dianhydride, 3,3'-oxydiphthalic dianhydride, 4,4'-oxydiphthalic dianhydride, and combinations thereof, with a diamine component comprising 4,4'-diaminodiphenylsulfone; wherein the polyimide has a glass transition temperature from 190°C to 400°C; and wherein the film has a coefficient of thermal expansion of less than 60 ppm/°C, a thickness from 0.1 to 250 micrometers, endless than 5% residual solvent by weight.
摘要翻译：溶剂流延膜包括聚酰亚胺，其包含衍生自二酐组分的聚合的结构单元，所述二酐组分包含二酐，其选自3,4'-氧二邻苯二甲酸二酐，3,3'-氧联二邻苯二甲酸二酐，4,4'-氧联二邻苯二甲酸二酐，和其组合与二胺组分包含4,4'-二氨基二苯砜; 其中所述聚酰亚胺的玻璃化转变温度为190℃至400℃; 并且其中所述膜具有小于60ppm /℃的热膨胀系数，0.1至250微米的厚度，不超过5重量％的残留溶剂。

10. 发明申请

WO2008060710A2 ARTICLES COMPRISING A POLYIMIDE SOLVENT CAST FILM HAVING A LOW COEFFICIENT OF THERMAL EXPANSION AND METHOD OF MANUFACTURE THEREOF 审中-公开
标题翻译：包含具有低热膨胀系数的聚酰亚胺溶剂铸膜的制品及其制造方法
公开(公告)号：WO2008060710A2
公开(公告)日：2008-05-22
申请号：PCT/US2007/071203
申请日：2007-06-14
申请人： GENERAL ELECTRIC COMPANY , CHAN, Kwok, Pong , HAGBERG, Erik , MULLEN, Tara, J. , ODLE, Roy, Ray
发明人： CHAN, Kwok, Pong , HAGBERG, Erik , MULLEN, Tara, J. , ODLE, Roy, Ray
CPC分类号： H05K1/0346 , B32B15/08 , C08G73/1007 , C08J5/18 , C08J2379/08 , C08K3/346 , C08L79/08 , H05K2201/0154 , H05K2201/068 , Y10T428/12569 , Y10T428/2938 , Y10T428/31765
摘要： An article comprises a solvent cast film comprising a polyetherimide comprising structural units derived from a dianhydride component selected from the group consisting of 3,4'-oxydiphthalic anhydride, 3,3'-oxydiphthalic anhydride, 4,4'- oxydiphthalic anhydride, and combinations thereof, and a diamine component. The polyetherimide has a glass transition temperature that is at least 1900C. The film has a coefficient of thermal expansion of less than 60 ppm/°C, a thickness from 0.1 to 250 micrometers, and less than 5% residual solvent by weight. The film has less than 15 molar % of a member selected from the group consisting of biphenyltetracarboxylic acid, dianhydrides of biphenyltetracarboxylic acid, esters of biphenyltetracarboxylic acid, and combinations thereof.
摘要翻译：一种制品包括含有聚醚酰亚胺的溶剂流延薄膜，该聚醚酰亚胺包含衍生自二酐组分的结构单元，所述二酐组分选自3,4'-氧联二邻苯二甲酸酐，3,3'-氧联二邻苯二甲酸酐，4,4'-氧联二邻苯二甲酸酐和组合和二胺组分。聚醚酰亚胺的玻璃化转变温度至少为190℃。该膜具有小于60ppm /℃的热膨胀系数，0.1至250微米的厚度和小于5重量％的残留溶剂。该膜具有少于15摩尔％的选自联苯四羧酸，联苯四羧酸的二酐，联苯四羧酸的酯及其组合的成员。

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