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1. 发明申请

WO2008002870A2 METHODS OF PREPARING POLYMER-ORGANOCLAY COMPOSITES AND ARTICLES DERIVED THEREFROM 审中-公开
标题翻译：制备聚合物 - 有机粘合剂复合材料的方法和由此衍生的制品
公开(公告)号：WO2008002870A2
公开(公告)日：2008-01-03
申请号：PCT/US2007/072019
申请日：2007-06-25
申请人： GENERAL ELECTRIC COMPANY , CHAN, Kwok, Pong , ODLE, Roy, Ray , HALL, David, Bruce , MAXAM, John, Lester , STELLA, Albert, Santo , GENOVESE, Sarah, Elizabeth , MULLEN, Tara, J. , WHITE, James, Mitchell , HAGBERG, Erik
发明人： CHAN, Kwok, Pong , ODLE, Roy, Ray , HALL, David, Bruce , MAXAM, John, Lester , STELLA, Albert, Santo , GENOVESE, Sarah, Elizabeth , MULLEN, Tara, J. , WHITE, James, Mitchell , HAGBERG, Erik
IPC分类号： C08F2/44 , C08K9/04 , C08L79/08 , C08K3/34 , C08K5/19 , C08K5/3432 , C08K5/50
CPC分类号： C08F2/44
摘要： A method for preparing a polymer-organoclay composite composition comprises combining a solvent and an unexfoliated organoclay to provide a first mixture, wherein the unexfoliated organoclay comprises alternating inorganic silicate layers and organic layers, and has an initial spacing between the silicate layers; exposing the first mixture to an energized condition of a sufficient intensity and duration to increase the initial spacing of the inorganic silicate layers, to provide a second mixture; contacting the second mixture with a polymer composition so that the polymer composition fills at least one region located between at least one pair of silicate layers, wherein the polymer composition is at least partially soluble in the solvent; and removing at least a portion of the solvent from the second mixture, wherein the inorganic silicate layers remain separated by the polymer after removal of the solvent.
摘要翻译：用于制备聚合物 - 有机粘土复合组合物的方法包括将溶剂和未剥落的有机粘土组合以提供第一混合物，其中未剥落的有机粘土包含交替的无机硅酸盐层和有机层，并且具有初始间距在硅酸盐层之间; 使第一混合物暴露于足够强度和持续时间的激励条件以增加无机硅酸盐层的初始间距，以提供第二混合物; 使第二混合物与聚合物组合物接触，使得聚合物组合物填充位于至少一对硅酸盐层之间的至少一个区域，其中聚合物组合物至少部分可溶于溶剂中; 和从第二混合物中除去至少一部分溶剂，其中在除去溶剂后，无机硅酸盐层仍然被聚合物分开。

2. 发明申请

WO2008063207A1 METHOD FOR PURIFYING DIANHYDRIDES 审中-公开
标题翻译：纯化二氢呋喃的方法
公开(公告)号：WO2008063207A1
公开(公告)日：2008-05-29
申请号：PCT/US2007/004982
申请日：2007-02-27
申请人： GENERAL ELECTRIC COMPANY , STELLA, Albert, Santo , HALL, David, Bruce
发明人： STELLA, Albert, Santo , HALL, David, Bruce
IPC分类号： C07D407/12
CPC分类号： C07D407/12
摘要： A method for purifying dianhydrides is provided. In one aspect, purified oxybisphthalic anhydrides, intermediates useful in the preparation of polyetherimides are provided. In one embodiment, a first solution containing a dianhydride compound, a solvent, and a phase transfer catalyst is contacted with a solid inorganic adsorbent material having a total pore volume of about 0.5 milliliters/gram or greater and a cumulative pore volume distribution of about 20 percent or greater of particles having a pore diameter in a range between about 3 nanometers and about 20 nanometers. The solution containing the dianhydride compound is then separated from the solid inorganic adsorbent material to provide a purified dianhydride compound which is substantially free of the phase transfer catalyst. The purification technique is especially valuable for preparing high purity oxybisphthalic anhydrides, such as 4,4'-oxybisphthalic anhydride (4,4'-ODPA), which are substantially free of residual phase transfer catalyst.
摘要翻译：提供了一种纯化二酸酐的方法。在一个方面，提供了纯的氧化双邻苯二甲酸酐，可用于制备聚醚酰亚胺的中间体。在一个实施方案中，将含有二酐化合物，溶剂和相转移催化剂的第一溶液与总孔体积为约0.5毫升/克或更大并且累积孔体积分布约为20的固体无机吸附材料接触百分比或更大的具有在约3纳米和约20纳米之间的孔径的颗粒。然后将含有二酐化合物的溶液与固体无机吸附材料分离，得到基本上不含相转移催化剂的纯化二酐化合物。纯化技术对于制备基本上不含残余相转移催化剂的4,4'-氧双苯二甲酸酐（4,4'-ODPA）的高纯度羟基双苯酐具有特别的价值。

3. 发明申请

WO2008063208A1 METHOD FOR PURIFYING BISIMIDES 审中-公开
标题翻译：纯化双歧杆菌的方法
公开(公告)号：WO2008063208A1
公开(公告)日：2008-05-29
申请号：PCT/US2007/004985
申请日：2007-02-27
申请人： GENERAL ELECTRIC COMPANY , STELLA, Albert, Santo , HALL, David, Bruce
发明人： STELLA, Albert, Santo , HALL, David, Bruce
IPC分类号： C07D209/48 , C07B63/00
CPC分类号： C07D209/48
摘要： A method for purifying bisimides is provided. In one aspect, purified oxybisphthalimides, intermediates useful in the preparation of polyetherimides are provided. In one embodiment, a first solution containing a bisimide compound, a solvent, and a phase transfer catalyst is contacted with a solid inorganic adsorbent material having a total pore volume of about 0.5 milliliters/gram or greater and a cumulative pore volume distribution of about 20 percent or greater of particles having a pore diameter in a range between about 3 nanometers and about 20 nanometers. The solution containing the bisimide compound is then separated from the solid inorganic adsorbent material to provide a purified bisimide compound which is substantially free of the phase transfer catalyst. The purification technique is especially valuable for preparing high purity oxybisphthalimides, such as 4,4'-oxybis(N-methylphthalimide), which are substantially free of residual phase transfer catalyst.
摘要翻译：提供了一种纯化双酰亚胺的方法。一方面，提供了纯化的氧联双苯二酰亚胺，可用于制备聚醚酰亚胺的中间体。在一个实施方案中，将含有双酰亚胺化合物，溶剂和相转移催化剂的第一溶液与总孔体积为约0.5毫升/克或更大并且累积孔体积分布约为20的固体无机吸附材料接触百分比或更大的具有在约3纳米和约20纳米之间的孔径的颗粒。然后将含有双酰亚胺化合物的溶液与固体无机吸附剂材料分离，以提供基本上不含相转移催化剂的纯化双酰亚胺化合物。纯化技术对于制备基本上不含残余相转移催化剂的4,4'-氧双（N-甲基邻苯二甲酰亚胺）的高纯度氧联双苯二酰亚胺是特别有价值的。

4. 发明申请

WO2008063206A1 METHOD FOR MAKING POLYETHERIMIDES 审中-公开
标题翻译：制备聚乙二醇的方法
公开(公告)号：WO2008063206A1
公开(公告)日：2008-05-29
申请号：PCT/US2007/004939
申请日：2007-02-27
申请人： GENERAL ELECTRIC COMPANY , STELLA, Albert, Santo , HALL, David, Bruce
发明人： STELLA, Albert, Santo , HALL, David, Bruce
IPC分类号： C07C51/00 , C07C51/567 , C07C51/573 , C08G73/00 , C08G73/10 , C08G73/12
CPC分类号： C08G73/1007 , C07C51/573 , C08G73/1014 , C08G73/1028 , C08G73/105 , C07C65/24
摘要： A method for making polyetherimides is provided by reacting a high purity dianhydride with an aromatic diamine under condensation polymerization conditions. The dianhydrides employed are purified by a method comprising contacting a first solution containing a dianhydride compound, a solvent, and a phase transfer catalyst, with a solid inorganic adsorbent material having a total pore volume of about 0.5 milliliters/gram or greater and a cumulative pore volume distribution, of about 20 percent or greater of particles having a pore diameter in a range between about 3 nanometers and about 20 nanometers. The solution containing the dianhydride compound is then separated from the solid inorganic adsorbent material to provide a purified dianhydride compound which is substantially free of the phase transfer catalyst. The purified dianhydrides are then condensed with aromatic diamines to provide polyetherimide compositions which are substantially free of residual phase transfer catalyst.
摘要翻译：通过在缩聚条件下使高纯度二酐与芳族二胺反应来提供制备聚醚酰亚胺的方法。所用的二酸酐通过包括将含有二酐化合物，溶剂和相转移催化剂的第一溶液与总孔体积为约0.5毫升/克或更大的固体无机吸附材料和累积孔约20％或更大的孔径在约3纳米至约20纳米之间的颗粒的体积分布。然后将含有二酐化合物的溶液与固体无机吸附材料分离，得到基本上不含相转移催化剂的纯化二酐化合物。然后将纯化的二酸酐与芳族二胺缩合，得到基本上不含残余相转移催化剂的聚醚酰亚胺组合物。

5. 发明申请

WO2006004822A1 METHOD OF MAKING HALOPHTHALIC ACIDS AND HALOPHTHALIC ANHYDRIDES 审中-公开
标题翻译：制备半胱氨酸和半胱氨酸的方法
公开(公告)号：WO2006004822A1
公开(公告)日：2006-01-12
申请号：PCT/US2005/023067
申请日：2005-06-30
申请人： GENERAL ELECTRIC COMPANY , COLBURN, Robert, Edgar , HALL, David, Bruce , KOCH, Peter, Alois , DEMUTH, Bernd, Volker , WESSEL, Thomas , MACK, Karl, Ernst , TATAKE, Prashant, Anil , VAKIL, Uptal, Mahendra , GONDKAR, Shyamal, Bhaskar , PACE, John, Edward , WON, Kwang, Woong
发明人： COLBURN, Robert, Edgar , HALL, David, Bruce , KOCH, Peter, Alois , DEMUTH, Bernd, Volker , WESSEL, Thomas , MACK, Karl, Ernst , TATAKE, Prashant, Anil , VAKIL, Uptal, Mahendra , GONDKAR, Shyamal, Bhaskar , PACE, John, Edward , WON, Kwang, Woong
IPC分类号： C07C51/265
CPC分类号： C07C51/265 , C07C63/68
摘要： A method of preparing a halophthalic acid is disclosed which comprises the steps of contacting in a liquid phase reaction mixture at least one halogen-substituted ortho-xylene with oxygen and acetic acid at a temperature in a range between about 120°C and about 220°C in the presence of a catalyst system yielding a product mixture comprising less than 10 percent halogen-substituted ortho-xylene starting material, a halophthalic acid product, and less than about 10,000 ppm halobenzoic acid and less than about 1000 ppm halophthalide by-products based on a total amount of halophthalic acid present in the product mixture. In addition methods for the preparation of halophthalic anhydride, and recovery of high purity acetic acid from an aqueous acetic acid stream comprising HCI, which is generated during the preparation of the halophthalic acid are also disclosed.
摘要翻译：公开了一种制备卤代邻苯二甲酸的方法，其包括以下步骤：在液相反应混合物中使至少一种卤素取代的邻二甲苯与氧和乙酸在约120℃和约220℃之间的温度下接触在催化剂体系的存在下，产生包含小于10％的卤素取代的邻二甲苯原料，卤代邻苯二甲酸产物和小于约10,000ppm的卤代苯甲酸和小于约1000ppm的卤代烃副产物的产物混合物在产物混合物中存在的卤代邻苯二甲酸的总量。另外还公开了制备卤代邻苯二甲酸酐的方法，以及在制备卤代邻苯二甲酸期间产生的包含HCl的含水乙酸流中回收高纯度乙酸。

6. 发明申请

WO2005066118A1 METHOD FOR REMOVAL OF GUANIDINE COMPOUND FROM AQUEOUS MEDIA 审中-公开
标题翻译：从水性介质中去除胍基化合物的方法
公开(公告)号：WO2005066118A1
公开(公告)日：2005-07-21
申请号：PCT/US2004/039048
申请日：2004-11-19
申请人： GENERAL ELECTRIC COMPANY? , HALL, David, Bruce , GUGGENHEIM, Thomas, Link , SILVA, James, Manio , KHOURI, Farid, Fouad , LITTLEJOHN, Matthew, Hal , GANESAN, Balakrishnan , SHYADLIGERI, Ashok, Shankrappa , NADKARNI, Pradeep, Jeevaji
发明人： HALL, David, Bruce , GUGGENHEIM, Thomas, Link , SILVA, James, Manio , KHOURI, Farid, Fouad , LITTLEJOHN, Matthew, Hal , GANESAN, Balakrishnan , SHYADLIGERI, Ashok, Shankrappa , NADKARNI, Pradeep, Jeevaji
IPC分类号： C07C277/06
CPC分类号： C02F9/00 , B01D61/027 , C02F1/281 , C02F1/283 , C02F1/44 , C02F2101/38 , C07C277/06 , C07C279/04
摘要： Disclosed is a method for removing a neutral or an ionic guanidine compound from an aqueous media optionally comprising an alkali metal halide, wherein the method is selected from the group consisting of (a) adsorption onto a carbonaceous adsorbent, (b) adsorption onto a clay adsorbent, (c) filtration through a nanofiltration membrane, and (d) removal of water and calcination.
摘要翻译：公开了一种从任选地包含碱金属卤化物的水性介质中除去中性或离子胍化合物的方法，其中所述方法选自（a）吸附到碳质吸附剂上，（b）吸附到粘土上吸附剂，（c）通过纳滤膜过滤，和（d）去除水和煅烧。

7. 发明申请

WO2009002779A2 METHOD OF PURIFYING A POLYMER 审中-公开
标题翻译：纯化聚合物的方法
公开(公告)号：WO2009002779A2
公开(公告)日：2008-12-31
申请号：PCT/US2008/067319
申请日：2008-06-18
申请人： SABIC INNOVATIVE PLASTICS IP B.V. , HALL, David, Bruce
发明人： HALL, David, Bruce
IPC分类号： C08G73/00
CPC分类号： C08F6/02 , C08G65/46 , C08G73/1046 , C08G73/105 , C08G73/1064 , C08G75/20 , C08G75/23 , C08L2205/05
摘要： A method for purifying a polymer comprising providing a first mixture comprising at least one solvent and at least one polymeric material, diluting the first mixture with veratrole to produce a second mixture in which the polymeric material is substantially dissolved at a temperature less than 100°C, performing at least one step selected from (i) contacting the second mixture with an aqueous wash solution, and (ii) filtering the second mixture.
摘要翻译：一种纯化聚合物的方法，包括提供包含至少一种溶剂和至少一种聚合物材料的第一混合物，将第一混合物用藜芦醇稀释以产生其中聚合物材料在低于100℃的温度下基本溶解的第二混合物执行选自（i）使第二混合物与水性洗涤溶液接触的至少一个步骤，和（ii）过滤第二混合物。

8. 发明申请

WO2014123530A1 ARTICLES COMPRISING A HYDRATE-INHIBITING SILICONE COATING 审中-公开
标题翻译：包含水合物抑制硅胶涂层的文章
公开(公告)号：WO2014123530A1
公开(公告)日：2014-08-14
申请号：PCT/US2013/025124
申请日：2013-02-07
申请人： GENERAL ELECTRIC COMPANY
发明人： FANG, Biao , WILSON, Paul, Russell , SIVARAMAKRISHNAN, Shyam , SAMUDRALA, Omprakash , WOLFE, Christopher, Edward , HALL, David, Bruce , KULKARNI, Ambarish, Jayant , GIAMMATTEI, Mark, Howard , LUSTED, Roderick, Mark , BUTTS, Matthew, David
IPC分类号： C09D183/04 , F16L9/147
CPC分类号： C09D183/04 , F16L58/1009 , C08L83/00
摘要： This disclosure details methods and techniques for inhibiting natural gas hydrate formation in gas conduits. In one embodiment, an article is provided which comprises (a) a gas conduit defining a gas flow channel; (b) an interior surface of the gas conduit; (c) a hydrate inhibiting coating on the interior surface, wherein the coating comprises: (i) component A, a one- or two-part room temperature vulcanizable polyorganosiloxane composition comprising a surface-treated filler, a condensation catalyst, and a crosslinking agent; and any reaction products thereof; and optionally (ii) component B, a hydrate release-enhancing proportion of at least one polyorganosiloxane comprising one or more silanol or alkoxy-silyl groups and comprising from about 10 weight percent to about 85 weight percent of at least one hydroxy-terminated or alkoxy-terminated polyoxyalkylenealkyl radical; and optionally (iii) any reaction products thereof.
摘要翻译：本公开详细描述了用于抑制气体管道中天然气水合物形成的方法和技术。在一个实施例中，提供了一种制品，其包括（a）限定气体流动通道的气体导管; （b）气体导管的内表面; （c）内表面上的水合物抑制涂层，其中所述涂层包括：（i）组分A，一份或两份室温可硫化聚有机硅氧烷组合物，其包含经表面处理的填料，缩合催化剂和交联剂 ; 及其任何反应产物; 和任选地（ⅱ）组分B，包含一种或多种硅烷醇或烷氧基 - 甲硅烷基的至少一种聚有机硅氧烷的水合物释放增强比例，并且包含约10重量％至约85重量％的至少一个羟基封端或烷氧基终止的聚氧化烯烷基; 和（iii）其任何反应产物。

9. 发明申请

WO2003082791A1 LIQUID PHASE OXIDATION OF HALOGENATED ORTHO-XYLENES 审中-公开
标题翻译：氢化邻苯二甲酸的液相氧化
公开(公告)号：WO2003082791A1
公开(公告)日：2003-10-09
申请号：PCT/US2003/007416
申请日：2003-03-11
申请人： GENERAL ELECTRIC COMPANY
发明人： COLBORN, Robert, Edgar , HALL, David, Bruce , KOCH, Peter , OECKEL, Gerald
IPC分类号： C07C51/265
CPC分类号： C07C51/265 , C07C51/56 , C07C63/68
摘要： A method for the manufacture of halophthalic acid by liquid phase oxidation of haloortho-xylene is disclosed. The halophthalic acid may be dehydrated to form halophthalic anhydride which is useful in the synthesis of polyetherimide.
摘要翻译：公开了通过卤代 - 二甲苯的液相氧化制备卤代邻苯二甲酸的方法。卤代邻苯二甲酸可以被脱水以形成可用于合成聚醚酰亚胺的卤代邻苯二甲酸酐。

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