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1. 发明申请

WO2014145463A3 CATALYST AND PROCESS FOR OXYCHLORINATION OF ETHYLENE TO DICHLOROETHANE 审中-公开
标题翻译：乙烯氧氯化生成二氯乙烷的催化剂和方法
公开(公告)号：WO2014145463A3
公开(公告)日：2014-12-04
申请号：PCT/US2014030233
申请日：2014-03-17
申请人： OCCIDENTAL CHEM CO
发明人： KRAMER KEITH
IPC分类号： B01J27/138 , B01J21/04 , B01J23/83 , B01J35/02 , B01J35/10 , B01J37/02
CPC分类号： B01J23/78 , B01J21/04 , B01J23/83 , B01J27/138 , B01J35/023 , B01J35/1019 , B01J35/1038 , B01J37/0205 , B01J37/024 , C07C17/02 , C07C17/156
摘要： In an oxychlorination process of the type where ethylene is converted to 1,2-dichloroethane in the presence of a supported copper catalyst, the improvement comprising: the use of a supported catalyst prepared by (i) impregnating, within a first step, an alumina support with a first aqueous solution including copper, an alkaline earth metal, and an alkali metal to thereby form a first catalyst component; and (ii) impregnating, within a subsequent step, the first catalyst component with a second aqueous solution including copper and alkaline earth metal, where the second aqueous solution is substantially devoid of alkali metal, to thereby form the supported catalyst.
摘要翻译：在负载型铜催化剂存在下将乙烯转化为1,2-二氯乙烷的类型的氧氯化过程中，改进之处包括：使用负载型催化剂，所述负载型催化剂通过以下步骤制备：（i）在第一步骤中，将氧化铝用包含铜，碱土金属和碱金属的第一水溶液支持，由此形成第一催化剂组分; 和（ii）在随后的步骤中，用包含铜和碱土金属的第二水溶液浸渍第一催化剂组分，其中第二水溶液基本上不含碱金属，从而形成负载型催化剂。

2. 发明申请

WO2014127001A3 METHODS FOR RECOVERING CHLORINATED HYDROCARBONS 审中-公开
标题翻译：回收氯化石油醚的方法
公开(公告)号：WO2014127001A3
公开(公告)日：2014-10-09
申请号：PCT/US2014016026
申请日：2014-02-12
申请人： OCCIDENTAL CHEM CO
发明人： DAWKINS JOHN LEE , HOLLIS DARRELL , KLAUSMEYER RODNEY L , KRAMER KEITH S , GARMON MICHAEL ANDREW
IPC分类号： C07C17/25 , C07C17/38 , C07C17/383 , C07C17/42 , C07C19/01 , C07C21/04
CPC分类号： C07C17/386 , B01D3/009 , B01D3/10 , B01D3/34 , B01D11/04 , C07C17/06 , C07C17/25 , C07C17/278 , C07C17/38 , C07C17/383 , C07C17/395 , C07C17/42 , Y02P20/127 , C07C19/01 , C07C21/04
摘要： Processes for isolating 1,1,1,2,3-pentachloropropane from a crude product stream containing the 1,1,1,2,3-pentachloropropane and ferric chloride. The processes may include deep distillation of the crude, treatment of the crude with a reagent that deactivates the ferric chloride followed by distillation on the deactivated crude stream, aqueous washing of the crude product stream to remove ferric chloride followed by distillation on the deactivated crude stream. Other embodiments simultaneously prepare 1,1,2,3-tetrachloroprene and 1,1,1,2,3-pentachloroprane.
摘要翻译：从含有1,1,1,2,3-五氯丙烷和氯化铁的粗产物流中分离1,1,1,2,3-五氯丙烷的方法。该方法可以包括对粗产物进行深蒸馏，用试剂灭活处理粗产物，然后在失活的粗制物流上进行蒸馏，然后对粗产物流进行水洗，以除去氯化铁，随后在失活的粗产物流。其它实施方案同时制备1,1,2,3-四氯丁二烯和1,1,1,2,3-五氯代。

3. 发明申请

WO0183420A3 METHOD OF MAKING SUBSTITUTED DIHALO AROMATIC ACID CHLORIDES 审中-公开
标题翻译：制备取代二氢芳香酸氯化物的方法
公开(公告)号：WO0183420A3
公开(公告)日：2002-06-13
申请号：PCT/GB0101917
申请日：2001-05-01
申请人： OCCIDENTAL CHEM CO , STEPHENS DINAH
发明人： FIFOLT MICHAEL J , SAVIDAKIS MICHAEL C , THIELEN DANIEL R , SPOHN RONALD F , DERWIN WILLIAM S , JOHNSON DAVID C , MANDAL SANJAY
IPC分类号： C07C51/363 , C07C51/60 , C07C63/04 , C07C63/10 , C07C63/70 , C07C67/307 , C07C67/317
CPC分类号： C07C51/363 , C07C63/04 , C07C63/10
摘要： A three-step method of making a substituted dihalo aromatic acid chloride is disclosed. A substituted aromatic compound having the general formula is halogenated to produce a mixture of corresponding dihalo and trihalo aromatic compounds, where R is COOH or COOR', R' is alkyl from C1 to C6, each R1 is independently selected from alkyl or alkoxy from C1 to C6 with no more than a single R1 group in the ortho position, and n is 1 or 2. Ortho halogens are selectively dehalogenated to produce the corresponding monohalo and dihalo aromatic compounds. The dihalo aromatic compound is converted into the corresponding acid chloride.
摘要翻译：公开了制备取代二卤代芳族酰氯的三步法。具有通式的取代的芳族化合物被卤化以产生相应的二卤代和三卤代芳族化合物的混合物，其中R是COOH或COOR'，R'是C1至C6的烷基，每个R 1独立地选自C 1的烷基或烷氧基至C6，在邻位不超过单个R 1基团，并且n为1或2.选择性地将卤素卤素脱卤以产生相应的单卤素和二卤代芳族化合物。将二卤代芳族化合物转化为相应的酰氯。

4. 发明申请

WO1981000099A1 RECOVERY OF HYDROGEN FLUORIDE FROM METALLIC FLUORIDE SALTS 审中-公开
标题翻译：从金属氟化物盐中回收氟化氢
公开(公告)号：WO1981000099A1
公开(公告)日：1981-01-22
申请号：PCT/US1979000400
申请日：1979-07-06
申请人： OCCIDENTAL CHEM CO
发明人： OCCIDENTAL CHEM CO , HIRKO R , MILLS H
IPC分类号： C01B07/22
CPC分类号： C01B7/196 , C01B7/191
摘要： Anhydrous hydrogen fluoride (44) of low P uO u content is recovered from metallic fluoride salts containing phosphate values by digesting the metallic salts (10) in sulfuric acid (14) at zone (16). Sufficient water and/or steam (12) is introduced into the zone to minimize the evolution of volatile fluophosphates encountered under conventional low humidity reactions. The dilute HF gas evolved (18) is rectified in two or more rectification zones (1, 2, 3) in series, where in at least one rectification zone, the rectification occurs in the presence of sulfuric acid (36). The product HF to P uO u weight ratio is greater than 10,000: 1.
摘要翻译：通过在（16）区域的硫酸（14）中消化金属盐（10），从含有磷酸盐的金属氟化物盐中回收低含量的u u u u的无水氟化氢（44）。将足够的水和/或蒸汽（12）引入该区域以最小化在常规低湿度反应下遇到的挥发性氟磷酸盐的演变。放出的稀释HF气体（18）在两个或更多个串联的精馏区（1,2,3）中进行精馏，其中在至少一个精馏区中，在硫酸存在下进行精馏（36）。产物HF至尿素重量比大于10,000:1。

5. 发明申请

WO0179148A3 METHOD OF MAKING BENZOYL HALIDES AND NITRILES 审中-公开
标题翻译：制备苯甲酸盐和硝酸盐的方法
公开(公告)号：WO0179148A3
公开(公告)日：2002-03-07
申请号：PCT/GB0100938
申请日：2001-03-05
申请人： OCCIDENTAL CHEM CO , STEPHENS DINAH
发明人： LAGERWALL DEAN R , THIELEN DANIEL R , KHANDARE PRAVIN M , LECHNER MARK F
IPC分类号： C07B61/00 , C07C17/18 , C07C25/02 , C07C51/58 , C07C51/64 , C07C63/70 , C07C253/20 , C07C255/50 , C07C63/04
CPC分类号： C07C253/20 , C07C51/58 , C07C51/64 , C07C63/04 , C07C63/70 , C07C255/50
摘要： A method of making a benzoyl halide is disclosed. Into a reactor is placed a reaction mixture of a benzotrihalide and a benzaldehyde having the respective general formulas (1) and (2), where each A is independently selected from halogen, CF3, R, or OR, each B is independently selected from halogen, CF3, or R, R is alkyl from C1 to C10 or aryl from C6 to C12, each X is independently selected from Cl and Br, m is 0 to 3, and n is 0 to 2. Also added is at least about 10 ppm of a catalyst selected from the group consisting of zinc salts and copper salts, and an optional solvent. The addition of an ammonium halide to the product mixture forms the corresponding amide, which can be dehydrated to form the corresponding nitrile.
摘要翻译：公开了制备苯甲酰卤的方法。将具有通式（1）和（2）的苯并三卤化物和苯甲醛的反应混合物放入反应器中，其中每个A独立地选自卤素，CF 3，R或OR，每个B独立地选自卤素，CF 3或R，R为C1至C10的烷基或C6至C12的芳基，每个X独立地选自Cl和Br，m为0至3，n为0至2.还加入至少约10 ppm的选自锌盐和铜盐的催化剂和任选的溶剂。向产物混合物中加入卤化铵形成相应的酰胺，其可以被脱水以形成相应的腈。

6. 发明申请

WO9620223A3 Azametallocene polymerization catalysts 审中-公开
标题翻译：亚甲基茂聚合催化剂
公开(公告)号：WO9620223A3
公开(公告)日：1996-09-06
申请号：PCT/US9516942
申请日：1995-12-18
申请人： OCCIDENTAL CHEM CO
发明人： ETHERTON BRADLEY P , NAGY SANDOR
IPC分类号： C08F4/642 , C07F7/00 , C07F9/572 , C07F17/00 , C08F2/34 , C08F4/64 , C08F4/659 , C08F4/6592 , C08F10/00 , C08F10/02 , C08F10/08
CPC分类号： C07F7/006 , C08F4/65912 , C08F4/6592 , C08F10/00
摘要： Disclosed is an azametallocene polymerization catalyst having the general formula where L is a ligand, or mixture of ligands, each having 4 to 30 carbon atoms and containing at least two fused rings, one of which is a pyrrolyl ring, Cp is a ligand containing a cyclopentadienyl group, B is a Lewis acid, Y is a halogen, alkoxy from C1 to C20, siloxy from C1 to C20, or mixtures thereof, M is titanium, zirconium, or mixtures thereof, m is 1 to 4, and n is 0 to 2, p is 0 to 2, q is 0 to 1, and m+n+q=4. The catalyst is useful in polymerizing unsaturated olefinic monomers such as ethylene.

7. 发明申请

WO0220660A3 POLYVINYL CHLORIDE RESINS AND METHOD OF PREPARATION AND USE IN THE PRODUCTION OF WHITENED POLYVINYL CHLORIDE FOAM 审中-公开
标题翻译：聚氯乙烯树脂及其制备和使用生产白色聚氯乙烯泡沫的方法
公开(公告)号：WO0220660A3
公开(公告)日：2002-07-25
申请号：PCT/GB0104025
申请日：2001-09-07
申请人： OCCIDENTAL CHEM CO , STEPHENS DINAH H
发明人： MORAN MICHAEL T , MOSES THOMAS E , CLANCY SHERRY ROHN
IPC分类号： C08J9/10 , C08J9/00 , C08K5/41 , C08K5/42 , C08L27/06 , C08L101/00 , C08L9/00
CPC分类号： C08J9/0033 , C08J2327/06 , C08J2375/04 , C08L27/06
摘要： Polyvinyl chloride resin compositions and methods of preparation and use thereof for increasing the degree of whiteness in finished polyvinyl chloride foam. The resin compositions contain sulfur compounds selected from sulfonic acid derivatives, sulfinic acid derivatives, and mercapto acetic acid sodium salt, and optionally contain water soluble salts and/or t-butyl hydroperoxide.
摘要翻译：聚氯乙烯树脂组合物及其制备方法以及用于提高成品聚氯乙烯泡沫体中白度的方法。树脂组合物含有选自磺酸衍生物，亚磺酸衍生物和巯基乙酸钠盐的硫化合物，并且任选地含有水溶性盐和/或叔丁基过氧化氢。

8. 发明申请

WO0222537A3 METHOD FOR PRODUCING BENZYL DERIVATIVES OF 2-BUTENE-1,4 DIOLS 审中-公开
标题翻译： 2-丁烯-1,4-二醇的苯甲酸衍生物的制备方法
公开(公告)号：WO0222537A3
公开(公告)日：2002-05-30
申请号：PCT/GB0104036
申请日：2001-09-10
申请人： OCCIDENTAL CHEM CO , STEPHENS DINAH H
发明人： KRISHNAMURTI RAMESH , WANG QI , SMOLKA THOMAS F
IPC分类号： C07C41/16 , C07C43/166 , C07C43/178
CPC分类号： C07C41/16 , C07C43/1787 , C07C43/166
摘要： A method for producing benzyl derivatives of 2-butene-1,4-diols by reacting 2-butene-1,4-diols with benzyl chloride compounds in the presence of an alkali or alkaline earth metal hydroxide or carbonate to produce benzyl derivatives of 2-butene-1,4-diols and recovering at least a portion of at least one such benzene derivative.
摘要翻译：在碱金属或碱土金属氢氧化物或碳酸盐存在下，使2-丁烯-1,4-二醇与苄基氯化合物反应生成2-丁烯-1,4-二醇的苄基衍生物的方法 - 丁烯-1,4-二醇，并回收至少一种这样的苯衍生物的至少一部分。

9. 发明申请

WO0217972A3 PREPARING STERILE ARTICLES FROM POLYMERS CONTAINING A STABILISER BASED ON A POLY(OXYALKYLENE) 审中-公开
标题翻译：基于聚合物（OXYALKYLENE）从含有稳定剂的聚合物制备无菌物品
公开(公告)号：WO0217972A3
公开(公告)日：2002-09-06
申请号：PCT/GB0103889
申请日：2001-08-30
申请人： OCCIDENTAL CHEM CO , STEPHENS DINAH
发明人： WANG QI , NAGY SANDOR
IPC分类号： A61L2/08 , C08F2/46 , C08J7/00 , C08K5/00 , C08L27/06 , C08L71/00 , C08K5/12
CPC分类号： A61L2/081 , A61L2202/24 , C08K5/0008 , C08K5/12 , C08L27/06 , C08L71/02 , C08L2666/14 , C08L2666/22
摘要： A method of preparing a sterile article is disclosed. A polymer having a halogen-containing repeating unit is prepared that contains about 0.005 to about 65 phr of a stabiliser having the general formula TGOT', where each T is independently selected from R-, R-CO-, -P(R)2, -P(OR)2, Si(R)3, or -Si(OR)3, T' is T or A[GOT]n, each A is independently selected from LS-Sn(R)3-q(OLJ)q,(CH2)pS-Sn(R)3-q(S(CH2)p-J)q, LCO2Sn(R)3-q(OLCO-J)q, or LSn(Y)3-q(LJ)q when n is O, from CO, E, CO-E-CO, Si(R)2, Si(OR)2, (Si(R)2G)r, (CO-E-CO-G)r, (CO-G)r, or (E-G)r when n is 1, and from P, PO and trimellitate when n is 2, Y is -SLJ, -SLJ, -SLOR, -OLJ, -OLR, -S(CH2)p, each R is independently selected from R', aralkyl from C6 to C12, and aryl from C6 to C12, E is alkylene from C1 to C12, m is 1 to 20, n is 0 to 2, p is 0 to 10, q is 0 to 3 and r is 1 to 20. An article is made from the polymer and the article is sterilised with ionising radiation. Also disclosed are novel stabilisers for use in this method.
摘要翻译：公开了一种制备无菌制品的方法。制备具有含卤素重复单元的聚合物，其含有约0.005至约65phr具有通式TGOT'的稳定剂，其中每个T独立地选自R-，R-CO-，-P（R）2 ，-P（OR）2，Si（R）3或-Si（OR）3，T'是T或A [GOT] n，每个A独立地选自LS-Sn（R）3-q ）q，（CH 2）p -S-Sn（R）3-q（S（CH 2）pJ）q，LCO 2 Sn（R）3-q（OLCO-J）q或LSn（Y）3-q（LJ）q （CO），CO（CO）2，Si（OR）2，（Si（R）2G）r，（CO-E-CO-G） -G）r或（EG）r，当n为2时，P为PO和偏苯三酸，Y为-SLJ，-SLJ，-SLOR，-OLJ，-OLR，-S（CH2）p 每个R独立地选自R'，C 6至C 12的芳烷基和C 6至C 12的芳基，E为C 1至C 12的亚烷基，m为1至20，n为0至2，p为0至10，q 为0〜3，r为1〜20。由聚合物制成制品，用电离辐射灭菌。还公开了用于该方法的新型稳定剂。

10. 发明申请

WO0109502A2 A PISTON 审中-公开
标题翻译：活塞
公开(公告)号：WO0109502A2
公开(公告)日：2001-02-08
申请号：PCT/GB9902485
申请日：1999-07-29
申请人： OCCIDENTAL CHEM CO , STEPHENS DINAH
发明人： MEYER LEON G
IPC分类号： F16J1/02 , F16D65/14 , F16D65/18 , F16D65/22 , F16J1/00 , F02F
CPC分类号： F16J1/00 , F16D2065/785 , F16D2125/06
摘要： Disclosed is a piston (1) having a cylindrical body made from a thermosetting molding compound. The body has a central well (3) and a molded-on metal cap (2) having sides that extend downward over the exterior of the body and into the well. There is thermal insulation (8, 9) under and in contact with the metal cap.
摘要翻译：公开了一种具有由热固性模塑料制成的圆筒体的活塞（1）。主体具有中心孔（3）和模制的金属盖（2），其具有向下延伸到身体的外部并进入井的侧面。在金属盖下面和与金属盖接触时，有隔热层（8,9）。

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