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31. 发明申请

WO2005090272A1 CYCLONE REACTOR AND ASSOCIATED METHODS 审中-公开
标题翻译：循环反应器和相关方法
公开(公告)号：WO2005090272A1
公开(公告)日：2005-09-29
申请号：PCT/US2005/008316
申请日：2005-03-11
申请人： UNIVERSITY OF UTAH , MILLER, Jan, D. , HUPKA, Jan , WLODZIMIERZ, Zmierczak, W.
发明人： MILLER, Jan, D. , HUPKA, Jan , WLODZIMIERZ, Zmierczak, W.
IPC分类号： C07C27/00
CPC分类号： C07C2/14 , B01J8/0055 , B01J8/20 , B01J8/226 , B01J19/2405 , C07C1/0405 , C07C2/12 , C07C2/58 , C07C2/66 , C07C5/3335 , C07C29/152 , C07C41/01 , C07C45/35 , C07C45/38 , C07C51/215 , C07C51/235 , C07C51/252 , C07C67/055 , C07C253/26 , C07D301/10 , C10G2/34 , C10G49/00 , C10G49/002 , C10G49/02 , Y02P20/52 , C07C11/02 , C07C47/22 , C07C47/04 , C07C57/145 , C07C53/02 , C07C57/04 , C07C69/01 , C07C255/08 , C07C69/15 , C07C31/04 , C07C43/06 , C07C43/043
摘要： A method of synthesizing and reacting compounds in a cyclone reactor (10) is disclosed and described. A liquid carrier can be provided which can include solid catalyst particles, liquid catalysts, and/or liquid reactants. The liquid carrier can be formed into a swirl layer (38) within the cyclone reactor (10). A reactant composition including at least one reactant can also be injected through at least a portion of the swirl layer (38) such that at least a portion of the reactant is converted to a reaction product. The cyclone reactor (10) allows for improved contact of reactants and catalyst, with fine temperature control, thus increasing reaction yields and selectivity.
摘要翻译：公开和描述了在旋流反应器（10）中合成和反应化合物的方法。可以提供液体载体，其可以包括固体催化剂颗粒，液体催化剂和/或液体反应物。液体载体可以形成旋风反应器（10）内的旋流层（38）。包含至少一种反应物的反应物组合物也可以通过旋流层（38）的至少一部分注入，使得至少一部分反应物转化为反应产物。旋风反应器（10）允许改善反应物和催化剂的接触，并具有精细的温度控制，从而提高反应产率和选择性。

32. 发明申请

WO2003033139A1 アンモ酸化用触媒の製造方法审中-公开
标题翻译：生产氧化催化剂的方法
公开(公告)号：WO2003033139A1
公开(公告)日：2003-04-24
申请号：PCT/JP2002/009832
申请日：2002-09-25
申请人：ダイヤニトリックス株式会社 , 宮氣健一 , 柳田元男 , 森邦夫
发明人：宮氣健一 , 柳田元男 , 森邦夫
IPC分类号： B01J23/88
CPC分类号： C07C253/26 , B01J21/08 , B01J23/002 , B01J23/8876 , B01J23/8878 , B01J23/8892 , B01J23/8898 , B01J23/8993 , B01J2523/00 , Y02P20/52 , B01J2523/13 , B01J2523/14 , B01J2523/3706 , B01J2523/3712 , B01J2523/41 , B01J2523/54 , B01J2523/67 , B01J2523/68 , B01J2523/842 , B01J2523/845 , B01J2523/847 , B01J2523/72 , B01J2523/22 , B01J2523/51 , B01J2523/53 , B01J2523/17 , B01J2523/30 , B01J2523/3725 , B01J2523/48 , B01J2523/27 , B01J2523/3718 , B01J2523/69 , B01J2523/55 , B01J2523/15 , B01J2523/3737 , B01J2523/64 , C07C255/08
摘要： A method for producing a catalyst for the ammoxidation of an organic compound which contains molybdenum component 1, bismuth component 2, al least one element selected from the group consisting of nickel, cobalt, zinc, magnesium, manganese and copper component 3, and al least one element selected from the group consisting of lanthanum, cerium, praseodymium and neodymium component 4, characterized in that it comprises a first liquid preparation step of preparing a first liquid which contains at least a part of the material of the component 1, at least a part of the material of the component 2 and at least a part of the material of the component 3 and does not contain the material of the component 4, and a second liquid preparation step of adding at least the material of the component 4 to the first liquid, to thereby prepare a second liquid. A catalyst produced by the method is useful for the ammoxidation of an organic compound, especially for the synthesis of acrylonitrile by the ammoxidation of propylene.
摘要翻译：一种用于制备含有钼组分1，铋组分2，选自镍，钴，锌，镁，锰和铜组分3中的至少一种元素的有机化合物的氨氧化催化剂的方法，以及至少选自镧，铈，镨和钕组分4中的一种元素，其特征在于，其包含第一液体制备步骤，其制备包含至少一部分组分1的材料的第一液体，至少一种组分2的材料的一部分和组分3的材料的至少一部分并且不含有组分4的材料，以及第二液体制备步骤，至少将组分4的材料添加到第一液体，从而制备第二液体。通过该方法制备的催化剂可用于有机化合物的氨氧化，特别是通过丙烯氨氧化合成丙烯腈。

33. 发明申请

WO0213963A3 IMPROVED CATALYST FOR THE MANUFACTURE OF ACRYLONITRILE 审中-公开
标题翻译：改进的催化剂生产丙烯腈
公开(公告)号：WO0213963A3
公开(公告)日：2002-05-02
申请号：PCT/US0124253
申请日：2001-08-02
申请人： STANDARD OIL CO
发明人： PAPARIZOS CHRISTOS , SEELY MICHAEL J , FRIEDRICH MARIA STRADA , SURESH DEV D
IPC分类号： B01J23/88 , B01J23/78 , B01J23/83 , B01J23/84 , B01J23/887 , C07B61/00 , C07C253/24 , C07C253/26 , C07C255/08
CPC分类号： C07C253/26 , B01J23/8876 , Y02P20/52 , C07C255/08
摘要： A catalyst composition comprising a complex of catalytic oxides of iron, bismuth, molybdenum, cobalt, cerium, antimony, at least one of nickel or magnesium, and at least one of lithium, sodium, potassium, rubidium, or thallium, and characterized by the following empirical formula: AaBbCcFedBieCofCegSbhMomOx wherein A is at least one of Cr, P, Sn, Te, B, Ge, Zn, In, Mn, Ca, W, or mixtures thereof, B is at least one of Li, Na, K, Rb, Cs, Tl, or mixtures thereof, C is least one of Ni, Mg or mixtures thereof, a is 0 to 4.0, b is 0.01 to 1.5, c is 1.0 to 10.0, d is 0.1 to 5.0, e is 0.1 to 2.0, f is 0.1 to 10.0, g is 0.1 to 2.0, h is 0.1 to 2.0, m is 12.0 to 18.0 and x is a number determined by the valence requirements of the other elements present. The catalyst is useful in processes for the ammoxidation of an olefin selected from the group consisting of propylene, isobutylene or mixtures thereof, to acrylonitrile, methacrylonitrile and mixtures thereof, respectively.
摘要翻译：一种催化剂组合物，其包含铁，铋，钼，钴，铈，锑，镍或镁中的至少一种以及锂，钠，钾，铷或铊中的至少一种的催化氧化物的络合物，按照经验式：AaBbCcFedBieCofCegSbhMomOx其中A是Cr，P，Sn，Te，B，Ge，Zn，In，Mn，Ca，W或其混合物中的至少一种，B是Li，Na，K， Rb，Cs，Tl或它们的混合物，C为Ni，Mg或其混合物中的至少一种，a为0-4.0，b为0.01-1.5，c为1.0-10.0，d为0.1-5.0，e为0.1-0.5 2.0，f是0.1-10.0，g是0.1-2.0，h是0.1-2.0，m是12.0-18.0，x是由存在的其它元素的化合价要求决定的数。该催化剂可用于将选自丙烯，异丁烯或其混合物的烯烃分别氨氧化成丙烯腈，甲基丙烯腈及其混合物的方法。

34. 发明申请

WO02012174A1 AMELIORATION OF AMMONIA BREAKTHROUGH IN AN ALKANE AMMOXIDATION PROCESS 审中-公开
标题翻译：氨基酸氧化过程中氨基酸突变的研究
公开(公告)号：WO02012174A1
公开(公告)日：2002-02-14
申请号：PCT/US2001/015640
申请日：2001-05-15
IPC分类号： C07B61/00 , C07C253/24 , C07C253/26 , C07C255/08
CPC分类号： C07C253/26 , C07C253/24 , C07C255/08
摘要： The invention is a method for the reduction of ammonia breakthrough during the manufacture of acrylonitrile comprising introducing a hydrocarbon selected from the group consisting of propane and isobutane; ammonia and an oxygen-containing gas into a lower portion of a fluid-bed reactor containing an ammoxidation catalyst to react in the presence of said catalyst to produce acrylonitrile. The method comprises introducing into the reactor at least one C2 to C5 olefin which will react with at least a portion of the unreacted ammonia and oxygen present in the reactor to substantially reduce the amount of ammonia present in the reactor effluent exiting the reactor.
摘要翻译：本发明是一种在制备丙烯腈期间减少氨穿透的方法，包括引入选自丙烷和异丁烷的烃; 氨和含氧气体进入含有氨氧化催化剂的流化床反应器的下部，以在所述催化剂存在下反应生产丙烯腈。该方法包括向反应器中引入至少一种C2至C5烯烃，其将与反应器中存在的至少一部分未反应的氨和氧气反应，以显着减少离开反应器的反应器流出物中存在的氨的量。

35. 发明申请

WO01041924A2 OXIDATIVE REACTIONS USING MEMBRANES THAT SELECTIVELY CONDUCT OXYGEN 审中-公开
标题翻译：氧化反应 - 混合官员，氧选择性膜
公开(公告)号：WO01041924A2
公开(公告)日：2001-06-14
申请号：PCT/EP2000/012497
申请日：2000-12-11
IPC分类号： C07D307/60 , B01D69/04 , B01D69/06 , B01D69/12 , B01D71/02 , B01J20/28 , B01J23/00 , B01J23/34 , B01J27/198 , B01J35/02 , B01J35/06 , C07B41/00 , C07B61/00 , C07C5/48 , C07C45/35 , C07C45/38 , C07C51/215 , C07C51/25 , C07C51/265 , C07C253/24 , C07C253/26 , C07C253/28 , C07D307/89 , B01J35/00
CPC分类号： C07C51/265 , B01J23/002 , B01J23/34 , B01J35/065 , B01J2523/00 , C07B41/00 , C07C5/48 , C07C45/35 , C07C45/38 , C07C51/215 , C07C51/252 , C07C253/24 , C07C253/26 , C07C253/28 , C07C2521/02 , C07C2521/10 , C07C2523/02 , C07C2523/04 , C07C2523/08 , C07C2523/10 , C07C2523/14 , C07C2523/34 , Y02P20/52 , C07C11/02 , C07C47/22 , C07C47/04 , C07C57/145 , C07C57/04 , C07C63/16 , B01J2523/23 , B01J2523/24 , B01J2523/72 , C07C255/51 , C07C255/08
摘要： The invention relates to reaction membranes that contain a selective oxidation catalyst disposed on a ceramic membrane that selectively conducts oxide ions and that is composed of (Sr1-xCax)1-yAyMn1-zBzO3- delta , wherein A represents Ba, Pb, Na, K, Y, an element of the lanthanide group or a combination of these elements, B represents Mg, Al, Ga, In, Sn, an element of the 3d or 4d period or a combination of these elements, x is a number of from 0.2 to 0.8, y is a number of from 0 to 0.4, z is a number of from 0 to 0.6 and delta is a number that results from the principle of electroneutrality on the basis of x, y and z. The inventive reaction membranes are suitable for use in oxidative reactions of hydrocarbons in which oxygen is used.
摘要翻译：本申请描述了包含在混合传导，所述组合物的氧化物离子选择性陶瓷膜的（Sr 1-x的Ca x）的1-yAyMn1-zBzO3-增量，其中A为Ba，铅，钠，钾，Y，镧系元素组或一的元件的选择氧化催化剂反应膜这些元素的组合，B表示镁，铝，镓，铟，锡，所述3D或4D期间或这些元素的组合的元素，x是从0.2到0.8的数，y是一个数字是从0至0.4，z是从0到0.6，和delta是一个数字，这导致的X，Y和z的术语从电中性原则的遵守情况。该反应膜可在其中使用氧的烃的氧化反应是有利的。

36. 发明申请

WO00072962A1 PROCESS FOR IMPROVING ACTIVITY AND SELECTIVITY OF AMMOXIDATION CATALYST 审中-公开
标题翻译：改进活性和选择性的氧化催化剂的方法
公开(公告)号：WO00072962A1
公开(公告)日：2000-12-07
申请号：PCT/US2000/014529
申请日：2000-05-26
IPC分类号： B01J23/887 , B01J37/00 , B01J37/03 , B01J37/08 , C07C45/34 , C07C45/35 , C07C51/25 , C07C253/26 , B01J23/18 , B01J23/74 , B01J23/881 , C07C45/00 , C07C253/00 , C07C255/00
CPC分类号： C07C253/26 , B01J23/002 , B01J23/8871 , B01J23/8876 , B01J37/0036 , B01J37/0045 , B01J37/03 , B01J37/08 , B01J2523/00 , C07C45/34 , C07C45/35 , C07C51/252 , Y02P20/52 , C07C47/22 , C07C57/04 , B01J2523/397 , B01J2523/41 , B01J2523/53 , B01J2523/54 , B01J2523/68 , B01J2523/842 , C07C255/08
摘要： The present invention provides an improved process for producing a catalyst containing the elements iron, antimony, uranium, bismuth and molybdenum in a catalytically active oxidized state, which is useful in the preparation of unsaturated nitriles by ammoxidation of olefins and in the oxidation of olefins to the corresponding unsaturated aldehydes. One embodiment of the process comprises the steps of: (a) forming a mixed oxides component that comprises oxides of antimony, bismuth, iron, and uranium; (b) combining the mixed oxides component with a molybdate; (c) forming the mixed oxides component into particles; (d) heating the particles at a temperature between about 40 DEG C and about 120 DEG C for at least about 1 hour; (e) drying the particles; and (f) calcining the particles.
摘要翻译：本发明提供了一种制备含有催化活性氧化态的铁，锑，铀，铋和钼元素的催化剂的改进方法，其可用于通过烯烃的氨氧化和烯烃氧化制备不饱和腈，相应的不饱和醛。该方法的一个实施方案包括以下步骤：（a）形成包含锑，铋，铁和铀的氧化物的混合氧化物组分; （b）将混合氧化物组分与钼酸盐组合; （c）将所述混合氧化物组分形成颗粒; （d）在约40℃至约120℃的温度下加热颗粒至少约1小时; （e）干燥颗粒; 和（f）煅烧颗粒。

37. 发明申请

WO1998017634A1 PROCESS FOR PURIFYING ACRYLONITRILE 审中-公开
标题翻译：纯化丙烯腈的方法
公开(公告)号：WO1998017634A1
公开(公告)日：1998-04-30
申请号：PCT/US1997018945
申请日：1997-10-17
申请人： SOLUTIA INC.
发明人： SOLUTIA INC. , MONICAL, Valerie, S. , STEINMEYER, Daniel, E. , WARD, Gregory
IPC分类号： C07C253/34
CPC分类号： C07C253/26 , C07C253/34 , C07C255/08
摘要： The fouling rate of quench systems in acrylonitrile manufacturing processes is reduced by maintaining a low level of highboiling organic compounds in aqueous recycle streams to the quench systems.
摘要翻译：丙烯腈制造过程中淬火系统的结垢率通过将水循环物流中的高沸点有机化合物维持在骤冷系统来降低。

38. 发明申请

WO1997025307A1 PROCESS FOR PRODUCING 'alpha'.'beta'-UNSATURATED NITRILE 审中-公开
标题翻译：生产α的方法 beta-UNSATURATED NITRILE
公开(公告)号：WO1997025307A1
公开(公告)日：1997-07-17
申请号：PCT/JP1996000007
申请日：1996-01-05
申请人： ASAHI KASEI KOGYO KABUSHIKI KAISHA , KURIHARA, Shigeru , MUROYA, Hiroaki , SAKAMOTO, Akihiko
发明人： ASAHI KASEI KOGYO KABUSHIKI KAISHA
IPC分类号： C07C255/07
CPC分类号： C07C253/26 , B01J8/1827 , B01J8/34 , B01J2208/00132 , B01J2208/00141 , Y02P20/52 , C07C255/08
摘要： A process for producing an alpha . beta -unsaturated nitrile from propylene, isobutylene or tert-butyl alcohol in an industrial fluidized reactor with the step of feeding methanol and an oxygen-containing gas in the course of the whole contact time of the reactor and reacting unreacted ammonia with the methanol and the oxygen-containing gas, which can reduce the amount of unreacted ammonia without lowering the yield of the nitrile; and an industrial process of conducting the above production in an industrial fluidized reactor having an inner diameter of 3 m or above and filled with a molybdenum-bismuth catalyst supported on silica, which can prevent the feed opening of a dispersing nozzle for the methanol from clogging with molybdenum oxides to attain constant reduction in the amount of unreacted ammonia. The former is a process of catalytically reacting propylene, isobutylene or tert-butyl alcohol with ammonia and an oxygen-containing gas at high temperature in a gas phase by the use of a fluidized bed catalyst to form an alpha . beta -unsaturated nitrile having the same number of carbon atoms as that of the starting propylene, isobutylene or tert-butyl alcohol, wherein methanol and an oxygen-containing gas are fed into the fluidized reactor at the positions corresponding to one-half to nine-tenths of the whole contact time from the point of feeding the starting materials through gas dispersing nozzles respectively and the fluidized reactor has at least one perforated structure having a throat area ratio of at least 60 % set above and/or below the gas dispersing nozzles; and the latter is a process of producing an alpha . beta -unsaturated nitrile as described above, wherein the methanol is fed together with steam through the same gas dispersing nozzle to thereby inhibit the catalyst from adhering to the dispersing nozzle and remove the catalyst adherent thereto.
摘要翻译：一种生产α的方法。在工业流化反应器中，丙烯，异丁烯或叔丁醇的β-不饱和腈，在反应器的整个接触时间和甲醇和未反应的氨反应过程中进料甲醇和含氧气体的步骤含氧气体，其可以在不降低腈的产率的情况下减少未反应的氨的量; 以及在内径为3μm以上的填充有二氧化硅的钼 - 铋催化剂的工业流化反应器中进行上述生产的工业方法，其能够防止用于甲醇的分散喷嘴的进料口堵塞与钼氧化物一起达到未反应氨的量的恒定降低。前者是通过使用流化床催化剂在丙烯，异丁烯或叔丁醇与氨和含氧气体在高温下催化反应形成α的方法。具有与起始丙烯，异丁烯或叔丁醇相同碳原子数的β-不饱和腈，其中甲醇和含氧气体在对应于二分之一至九分之一的位置进料到流化反应器中，从原料通过气体分散喷嘴分别供给点的整个接触时间的十分之一秒，并且流化反应器具有至少一个具有至少60％的喉部面积比设置在气体分散喷嘴上方和/或下方的穿孔结构; 后者是产生α的过程。如上所述的β-不饱和腈，其中甲醇与蒸汽一起通过相同的气体分散喷嘴进料，从而抑制催化剂附着在分散喷嘴上并去除附着在其上的催化剂。

39. 发明申请

WO1991004961A1 APPARATUS FOR PRODUCING 'alpha','beta'-UNSATURATED NITRILE 审中-公开
标题翻译：生产（ALPHA），（BETA） - 饱和硝酸盐的装置
公开(公告)号：WO1991004961A1
公开(公告)日：1991-04-18
申请号：PCT/JP1990001279
申请日：1990-10-04
申请人： ASAHI KASEI KOGYO KABUSHIKI KAISHA , MUROYA, Hiroaki , ISHII, Kanji , OHTA, Masanobu , TANAKA, Tetsuo
发明人： ASAHI KASEI KOGYO KABUSHIKI KAISHA
IPC分类号： C07C255/08
CPC分类号： B01J8/1827 , B01F5/0601 , B01F15/0264 , C07C253/26 , C07C255/08
摘要： An apparatus for producing an alpha , beta -unsaturated nitrile with the same number of carbon atoms as that of an olefin or t-butyl alcohol as the starting material by the reaction of either propylene or isobutylene or t-butyl alcohol with ammonia and an oxygen-containing gas, said apparatus being constituted of a reactor; a starting gas supplier provided horizontally at a lower part of the reactor and equipped with a plurality of starting gas blow nozzles on the lower surface thereof; and an oxygen-containing gas supplier provided beneath the starting gas supplier in parallel therewith and equipped with the same number of oxygen-containing gas blow pipes as that of the starting gas blow nozzles on the upper surface thereof in such a manner that each of said pipes faces each of said nozzles, wherein a relative distance between the pipe and the nozzle ranges from 25 to 300 mm and the pipes are arranged at a distance of 90 to 250 mm from each other with a relative density of distribution of 16 to 120 /m of the cross section of the reactor.
摘要翻译：通过丙烯或异丁烯或叔丁醇与氨和氧气反应制备具有与作为起始原料的烯烃或叔丁醇相同碳原子数的α，β-不饱和腈的装置所述装置由反应器构成; 原料气体供应器水平地设置在反应器的下部，并在其下表面上配备有多个起始气体吹制喷嘴; 以及与原料气体供给体并联设置的含氧气体供给体，并且与上述起始气体吹出喷嘴相同数量的含氧气体吹送管，其上表面上配置有与上述管道面对每个所述喷嘴，其中管道和喷嘴之间的相对距离范围为25至300mm，并且管道彼此相隔90至250mm的距离，分布的相对密度为16至120 / m 2的反应器横截面。

40. 发明申请

WO2017217343A1 アンモ酸化用触媒の製造方法、及びアクリロニトリルの製造方法审中-公开
标题翻译：生产氨氧化催化剂的方法和生产丙烯腈的方法
公开(公告)号：WO2017217343A1
公开(公告)日：2017-12-21
申请号：PCT/JP2017/021543
申请日：2017-06-09
申请人：旭化成株式会社
发明人：相木　彰太 , 福澤　章喜
IPC分类号： B01J37/00 , B01J23/883 , B01J37/04 , B01J37/08 , C07C253/26 , C07C255/08 , C07B61/00
CPC分类号： B01J37/0045 , B01J23/881 , B01J23/883 , B01J23/8872 , B01J23/8876 , B01J37/00 , B01J37/0018 , B01J37/04 , B01J37/08 , B01J37/088 , B01J2523/00 , B01J2523/54 , B01J2523/68 , B01J2523/842 , C07B61/00 , C07C253/26 , C07C255/08 , Y02P20/52 , B01J2523/14 , B01J2523/3712 , B01J2523/845 , B01J2523/847 , B01J2523/22 , B01J2523/13 , B01J2523/67
摘要：モリブデンと、ビスマスと、鉄と、カルボン酸化合物とを含む原料スラリーを調製する工程（ｉ）と、前記原料スラリーを３０～５０℃の温度範囲で２０分～８時間撹拌して前駆体スラリーを調製する工程（ｉｉ）と、前記前駆体スラリーを噴霧乾燥し、乾燥粒子を得る工程と、前記乾燥粒子を焼成する工程と、を有する、アンモ酸化用触媒の製造方法。
摘要翻译：（i）制备含有钼，铋，铁和羧酸化合物的原料浆料;（i）制备含有钼，铋，铁和羧酸化合物的原料浆料，（Ii）通过搅拌前体浆体一段时间来制备前体浆体，喷雾并干燥前体浆体以获得干燥颗粒，并且将干燥颗粒方法。

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