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1. 发明授权

US3890302A Dextro 1-methyl-2-(2-naphthyl) aziridine 失效
标题翻译：右旋1-甲基-2-（2-萘基）氮丙啶
公开(公告)号：US3890302A
公开(公告)日：1975-06-17
申请号：US25983972
申请日：1972-06-05
申请人： KOTERA KATSUMI , KITAHONOKI KEIZO , KIDO RYONOSUKE
发明人： KOTERA KATSUMI , KITAHONOKI KEIZO , KIDO RYONOSUKE
IPC分类号： C07D203/08 , C07D23/06
CPC分类号： C07D203/08
摘要： Racemic 1-methyl-2-(2-naphthyl)aziridine, being useful as a tranquilizer, is prepared via three routes: (a) halogenation of the corresponding aminoalcohol and treatment of the resulting haloamine with an alkali; (b) treatment of the corresponding aminoalcohol with sulfuric acid and treatment of the resulting hydrogen sulfate with an alkali; and (c) treatment of 2-(2naphthyl)aziridine with an oxonium methylating agent. Dextro-1methyl-2-(2-naphthyl)aziridine, being more potent in the tranquilizing activity than the racemate, is prepared by optical resolution of racemic 2-(2-naphthyl)-2-methylaminoethanol with levo-tartaric acid, treatment of the resulting dextro-2-(2naphthyl)-2-methylaminoethanol levo-tartrate with an alkali, treatment of the resulting dextro-2-(2-naphthyl)-2methylaminoethanol with a halogenating agent and treatment of the resulting levo-N-methyl-2-halogeno-1-(2-naphthyl)ethylamine with an alkali.
摘要翻译：通过三种途径制备用作镇定剂的外消旋1-甲基-2-（2-萘基）氮丙啶：（a）卤化相应的氨基醇并用碱处理得到的卤代胺; （b）用硫酸处理相应的氨基醇，用碱处理得到的硫酸氢盐; 和（c）用氧代甲基化剂处理2-（2-萘基）氮丙啶。通过用左旋酒石酸旋光拆分外消旋的2-（2-萘基）-2-甲基氨基乙醇，制备了比外消旋物更有效的镇痛活性的右旋-1-甲基-2-（2-萘基）氮丙啶，用碱处理得到的右旋-2-（2-萘基）-2-甲基氨基乙醇左旋酒石酸盐，用卤化剂处理所得的右旋-2-（2-萘基）-2-甲基氨基乙醇，并处理所得的左旋-N-甲基-2-卤代-1-（2-萘基）乙胺与碱反应。

2. 发明授权

US3855217A Improved process for preparing n-benzylically substituted aziridines 失效
标题翻译：制备N-叔丁基取代的亚胺酯的改进方法
公开(公告)号：US3855217A
公开(公告)日：1974-12-17
申请号：US24687372
申请日：1972-04-24
申请人： DOW CHEMICAL CO
发明人： THILL B
IPC分类号： C07D203/08 , C07D23/06
CPC分类号： C07D203/08
摘要： N-Benzylically substituted aziridines are conventionally prepared by reacting a benzyl halide with aziridine (or other non-N-substituted aziridine) in the presence of an acid acceptor. Product yields are considerably improved by conducting the above process in a liquid aromatic hydrocarbon reaction medium. E.g., N-benzylaziridine is prepared in excellent yields by reacting benzyl chloride with aziridine in the presence of powdered KOH and benzene.
摘要翻译： N-苄基取代的氮丙啶通常在酸受体存在下使苄基卤与氮丙啶（或其它非N-取代的氮丙啶）反应制备。通过在液体芳族烃反应介质中进行上述方法，产物产率显着提高。例如，通过苄基氯与氮丙啶在粉末状KOH和苯的存在下反应制得N-苄基氮丙啶。

3. 发明授权

US3719698A Polyfluorinated esters of acids containing silicon and amino groups 失效
标题翻译：含有硅和氨基团的酸的多元醇酯
公开(公告)号：US3719698A
公开(公告)日：1973-03-06
申请号：US3719698D
申请日：1967-11-27
申请人： STEVENS & CO INC J P
发明人： TESORO G , RING R
IPC分类号： C07D203/08 , C07D213/20 , C07F7/18 , D06M13/342 , D06M13/493 , C07C101/20 , C07D23/06
CPC分类号： C07D203/08 , C07D213/20 , C07F7/1836 , D06M13/342 , D06M13/493
摘要： Polyfluorinated esters of the formula WHEREIN Rf is a polyfluorinated hydrocarbon radical containing at least three fluorine atoms and up to 20 carbon atoms, A is an alkylene radical of up to six carbon atoms, Z is the residue of an amine component selected from the group consisting of amines and amine slats which have had at least one hydrogen atom removed, and q is an integer selected from 1 and 2, useful as textile finishing agents.

4. 发明授权

US3629239A Process for preparing aziridine derivatives 失效
标题翻译：制备亚胺基衍生物的方法
公开(公告)号：US3629239A
公开(公告)日：1971-12-21
申请号：US3629239D
申请日：1969-09-03
申请人： SHIONOGI & CO
发明人： KITAHONOKI KEIZO , KOTERA KATSUMI
IPC分类号： C07D203/08 , C07D203/18 , C07D203/20 , C07D203/22 , C07D203/26 , C07D277/16 , C07D23/02 , C07D23/06 , C07D31/42
CPC分类号： C07D203/08 , C07D203/18 , C07D203/20 , C07D203/22 , C07D203/26 , C07D277/16
摘要： NOVEL PROCESS FOR PREPARING AZIRIDINE DERIVATIVE WHICH COMPRISES REDUCING AN OXIME COMPOUND WITH A METALLIC HYDRIDE COMPLEX IN AN INERT SOLVENT.

5. 发明授权

US3440242A Aromatic polyalkylenamides 失效
标题翻译：芳香聚偏二氟乙烯
公开(公告)号：US3440242A
公开(公告)日：1969-04-22
申请号：US3440242D
申请日：1963-09-12
申请人： MINNESOTA MINING & MFG
发明人： SMITH GEORGE H
IPC分类号： C07D203/18 , C07D23/06
CPC分类号： C07D203/18

6. 发明授权

US3751395A Casting materials for dental purposes containing a bis-ethylene-imene compound capable of being crosslinked 失效
标题翻译：用于含有可交联的双 - 乙烯 - 内酯化合物的牙科用途的铸造材料
公开(公告)号：US3751395A
公开(公告)日：1973-08-07
申请号：US3751395D
申请日：1971-08-18
申请人： ESPE PHARM PRAEP
发明人： SCHMITT W , ZAHLER W , PURRMANN R , JOCHUM P
IPC分类号： A61C9/00 , A61K6/087 , C07D203/18 , C08G73/02 , C07D23/06
CPC分类号： A61K6/087 , A61C9/00 , C07D203/18 , C08G73/024 , Y10S528/92
摘要： THE PRESENT INVENTION RELATES TO MATERIAL FOR MAKING CASTS FOR DENTAL PURPOSES, WHICH MATERIAL SUBSTANTIALLY COMPRISES BIS-ETHYLENE-IMINE COMPOUNDS CAPABLE OF BEING CROSS-LINKED AND HAVING THE FORMULA

((-(CH2)2-)>N-Y-O-R''-O-(1,4-CYCLOHEXYLENE))2-R

WHEREIN R IS AN ALKYLIDENE RADICAL WITH 1-6 CARBON ATOMS, A CYCLOALKYLIDENE RADICAL OR AN SO2 RADICAL; R'' AN ALKYLENE RADICAL HAVING 2-6 CARBON ATOMS OR A CYCLOALKYLENE RADICAL, AND Y AN ACYL RADICAL OF A CARBOXYLIC ACID WITH 2-6 CARBON ATOMS, WHICH MAY ALSO BE SUBSTITUTED BY AN AROMATIC SUBSTITUENT.

7. 发明授权

US3634400A Cross-linkable bis-ethylene imine compound 失效
标题翻译：可交联双乙烯胺化合物
公开(公告)号：US3634400A
公开(公告)日：1972-01-11
申请号：US3634400D
申请日：1967-07-03
申请人： ESPE PHARM PRAEP
发明人： SCHMITT WERNER , PURRMANN ROBERT , JOCHUM PETER , ZAHLER WOLF-DIETRICH
IPC分类号： A61C9/00 , A61C13/00 , A61K6/087 , C07D203/18 , C08G73/02 , C08G73/04 , C07D23/06
CPC分类号： A61C9/00 , A61C13/00 , A61K6/087 , C07D203/18 , C08G73/024 , Y10S528/92
摘要： THE PRESENT INVENTION RELATES TO MATERIAL FOR MAKING CASTS FOR DENTAL PURPOSES, WHICH MATERIAL SUBSTANTIALLY COMPRISES BIS-ETHYLENE-IMINIE COMPOUNDS CAPABLE OF BEING CROSS-LINKED AND HAVING THE FORMULA

1-((4-((AZIRIDIN-1-YL)-Y-O-R''-O-)PHENYL)-R-),4-((AZIRIDIN-

1-YL)-Y-O-R''-O-)BENZENE

WHEREIN R IS AN ALKYLIDENE RADICAL WITH 1-6 CARBON ATOMS, A CYCLOKALKYLIDENE RADICAL OR AN SO2 RADICAL; R'' AN ALKYLENE RADICAL HAVING 2-6 CARBON ATOMS OR A CYCLOALKYLENE RADICAL, AND Y AN ACYL RADICAL OF A CARBOXYLIC ACID WITH 2-6 CARBON ATOMS, WHICH MAY ALSO BE SUBSTITUTED BY AN AROMATIC SUBSTITUENT.

8. 发明授权

US3583977A Hydroxy aziridinyl compounds 失效
标题翻译：羟基亚胺丁基化合物
公开(公告)号：US3583977A
公开(公告)日：1971-06-08
申请号：US3583977D
申请日：1968-06-18
申请人： GEN TIRE & RUBBER CO
发明人： UELZMANN HEINZ
IPC分类号： C07D203/10 , C08G18/10 , C08G18/50 , C08G18/64 , C08G59/10 , C08G59/50 , C08G65/22 , C08G65/26 , C08G73/02 , C08K5/3412 , C08L63/00 , C08L101/08 , C07D23/02 , C07D23/06
CPC分类号： C08L63/00 , C07D203/10 , C08G18/10 , C08G18/5057 , C08G18/6423 , C08G59/10 , C08G59/5066 , C08G65/22 , C08G65/263 , C08G73/0206 , C08G73/0226 , C08K5/3412 , C08L101/08 , Y10S516/06 , C08G18/3293 , C08L2666/20 , C08L2666/02
摘要： AZIRIDINYL COMPOUNDS OF THE FORMULA:

AZ-CH2-CH(-O-R'')-CH2-O-R

WHEREIN

AZ IS AN AZIRIDINO GROUP, R IS HYDROGEN, OR AN ALKENYL, ALKENYL CYCLO ALIPHATIC, ALKENYLARYL, HYDROXYPOLYOXYALKYLENE, OR A HYDROXY POLYOXYALKYLENE (OXYALKYENYL) GROUP, AND R'' IS HYDROGEN, OR A HYDROXYPOLYOXALKYLENE, OR A HYDROXY POLYOXYALKYLENE (OXYALKENYL) GROUP

ARE PREPARED ACCORDING TO THE REACTION ILLUSTRATED BY THE FOLLOWING TYPICAL PREPARATION:

2-(HO-CH2-)-OXIRANE + AZIRIDINE ---->

1-(HO-CH2-CH(-OH)-CH2-)-AZIRIDINE

THE NEW COMPOUNDS CAN BE USED IN FORMING ADHESIVES, COATINGS FOR FABRICS, FOAMS AND SPONGES, BINDERS, EMULSIFIERS AND SURFACTANTS AND AS CROSS-LINKERS FOR POLYMERS.

9. 发明授权

US3520875A Process for preparing n-alkyl aziridines 失效
标题翻译：制备N-烷基亚胺的方法
公开(公告)号：US3520875A
公开(公告)日：1970-07-21
申请号：US3520875D
申请日：1966-08-25
申请人： DOW CHEMICAL CO
发明人： ASHBY THEODORE L , LANE ROBERT E JR
IPC分类号： C07D203/08 , C07D23/06 , C07D23/02
CPC分类号： C07D203/08

10. 发明授权

US3449323A Process for the production of sulfenamides 失效
标题翻译：生产磺胺类的方法
公开(公告)号：US3449323A
公开(公告)日：1969-06-10
申请号：US3449323D
申请日：1965-10-04
申请人： DOW CHEMICAL CO
发明人： DUNBAR JOSEPH E
IPC分类号： C07D295/26 , C07D87/46 , C07C149/24 , C07D23/06
CPC分类号： C07D295/26

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