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    • 8. 发明授权
    • Aligning a featureless thin film in a TEM
    • 在TEM中对齐无特征薄膜
    • US09583303B2
    • 2017-02-28
    • US14878513
    • 2015-10-08
    • FEI Company
    • Bart BuijsseGijs van Duinen
    • H01J37/26H01J37/02H01J37/153
    • H01J37/023H01J37/153H01J37/26H01J37/261H01J2237/024H01J2237/1532H01J2237/1534H01J2237/2602H01J2237/2614
    • When preparing a Hole-Free Phase Plates (HFPP) a preferably featureless thin film should be placed with high accuracy in the diffraction plane of the TEM, or a plane conjugate to it. Two methods for accurately placing the thin film in said plane are described. One method uses a Ronchigram of the thin film while the TEM is in imaging mode, and the magnification of the Ronchigram is tuned so that the magnification in the middle of the Ronchigram is infinite. The second method uses electrons scattered by the thin film while the TEM is in diffraction mode. When the thin film does not coincide with the diffraction plane, electrons scattered by the thin film seem to originate from another location than the cross-over of the zero beam. This is observed as a halo. The absence of the halo is proof that the thin film coincides with the diffraction plane.
    • 当准备无孔相板(HFPP)时,应该在TEM的衍射平面或与其共轭的平面上以高精度放置优选无特征薄膜。 描述了将薄膜准确地放置在所述平面中的两种方法。 当TEM处于成像模式时,一种方法使用薄膜的Ronchigram,并且调整Ronchigram的放大倍率,使得Ronchigram中间的放大倍率是无穷大的。 第二种方法是在TEM处于衍射模式时使用由薄膜散射的电子。 当薄膜与衍射平面不一致时,由薄膜散射的电子似乎源自与零光束交叉的另一位置。 这被观察为光环。 光晕的不存在证明薄膜与衍射平面重合。